Separation process principles : chemical and biochemical operations /

Detalles Bibliográficos
Autor principal: Seader, J. D.
Otros Autores: Henley, Ernest J., Roper, D. Keith
Formato: Libro
Lenguaje:English
Publicado: Hoboken, NJ : John Wiley & Sons, c2011.
Edición:3rd ed.
Materias:
Separación (Tecnología) > Libros de texto.
Acceso en línea:Cover image
Tabla de Contenidos:
  • 5. Cascades and Hybrid Systems.
  • 5.0 Instructional Objectives.
  • 5.1 Cascade Configurations.
  • 5.2 Solid-Liquid Cascades.
  • 5.3 Single-Section Extraction Cascades.
  • 5.4 Multicomponent Vapor-Liquid Cascades.
  • 5.5 Membrane Cascades.
  • 5.6 Hybrid Systems.
  • 5.7 Degrees of Freedom and Specifications for Cascades.
  • Summary References Study Questions Exercises.
  • PART 2 SEPARATIONS BY PHASE ADDITION OR CREATION.
  • 6. Absorption and Stripping of Dilute Mixtures.
  • 6.0 Instructional Objectives.
  • 6.1 Equipment for Vapor-Liquid Separations.
  • 6.2 General Design Considerations.
  • 6.3 Graphical Method for Trayed Towers.
  • 6.4 Algebraic Method for Determining N.
  • 6.5 Stage Efficiency and Column Height for Trayed Columns.
  • 6.6 Flooding, Column Diameter, Pressure Drop, and Mass Transfer for Trayed Columns.
  • 6.7 Rate-Based Method for Packed Columns.
  • 6.8 Packed-Column Liquid Holdup, Diameter, Flooding, Pressure Drop, and Mass-Transfer
  • Efficiency.
  • 6.9 Concentrated Solutions in Packed Columns.
  • Summary References Study Questions Exercises.
  • 7. Distillation of Binary Mixtures.
  • 7.0 Instructional Objectives.
  • 7.1 Equipment and Design Considerations.
  • 7.2 McCabe-Thiele Graphical Method for Trayed Towers.
  • 7.3 Extensions of the McCabe-Thiele Method.
  • 7.4 Estimation of Stage Efficiency for Distillation.
  • 7.5 Column and Reflux-Drum Diameters.
  • 7.6 Rate-Based Method for Packed Distillation Columns.
  • 7.7 Introduction to the Ponchon-Savarit Graphical Equilibrium-Stage Method for Trayed
  • Towers.
  • Summary References Study Questions Exercises.
  • 8. Liquid-Liquid Extraction with Ternary Systems.
  • 8.0 Instructional Objectives.
  • 8.1 Equipment for Solvent Extraction.
  • 8.2 General Design Considerations.
  • 8.3 Hunter-Nash Graphical Equilibrium-Stage Method.
  • 8.4 Maloney-Schubert Graphical Equilibrium-Stage Method.
  • 8.5 Theory and Scale-up of Extractor Performance.
  • 8.6 Extraction of Bioproducts.
  • Summary References Study Questions Exercises.
  • 9. Approximate Methods for Multicomponent, Multistage Separations.
  • 9.0 Instructional Objectives.
  • 9.1 Fenske-Underwood-Gilliland (FUG) Method.
  • 9.2 Kremser Group Method.
  • Summary References Study Questions Exercises.
  • 10. Equilibrium-Based Methods for Multicomponent Absorption, Stripping,
  • Distillation, and Extraction.
  • 10.0 Instructional Objectives.
  • 10.1 Theoretical Model for an Equilibrium Stage.
  • 10.2 Strategy of Mathematical Solution.
  • 10.3 Equation-Tearing Procedures.
  • 10.4 Newton-Raphson (NR) Method.
  • 10.5 Inside-Out Method.
  • Summary References Study Questions Exercises.
  • 11. Enhanced Distillation and Supercritical Extraction.
  • 11.0 Instructional Objectives.
  • 11.1 Use of Triangular Graphs.
  • 11.2 Extractive Distillation.
  • 11.3 Salt Distillation.
  • 11.4 Pressure-Swing Distillation.
  • 11.5 Homogeneous Azeotropic Distillation.
  • 11.6 Heterogeneous Azeotropic Distillation.
  • 11.7 Reactive Distillation.
  • 11.8 Supercritical-Fluid Extraction.
  • Summary References Study Questions Exercises.
  • 12. Rate-Based Models for Vapor-Liquid Separation Operations.
  • 12.0 Instructional Objectives.
  • 12.1 Rate-Based Model.
  • 12.2 Thermodynamic Properties and Transport-Rate Expressions.
  • 12.3 Methods for Estimating Transport Coefficients and Interfacial Area.
  • 12.4 Vapor and Liquid Flow Patterns.
  • 12.5 Method of Calculation.
  • Summary References Study Questions Exercises.
  • 13. Batch Distillation.
  • 13.0 Instructional Objectives.
  • 13.1 Differential Distillation.
  • 13.2 Binary Batch Rectification.
  • 13.3 Batch Stripping and Complex Batch Distillation.
  • 13.4 Effect of Liquid Holdup.
  • 13.5 Shortcut Method for Batch Rectification.
  • 13.6 Stage-by-Stage Methods for Batch Rectification.
  • 13.7 Intermediate-cut Strategy.
  • 13.8 Optimal Control by Variation of Reflux Ratio.
  • Summary References Study Questions Exercises.
  • PART 3 SEPARATIONS BY BARRIERS AND SOLID AGENTS.
  • 14. Membrane Separations.
  • 14.0 Instructional Objectives.
  • 14.1 Membrane Materials.
  • 14.2 Membrane Modules.
  • 14.3 Transport in Membranes.
  • 14.4 Dialysis.
  • 14.5 Electrodialysis.
  • 14.6 Reverse Osmosis.
  • 14.7 Gas Permeation.
  • 14.8 Pervaporation.
  • 14.9 Membranes in Bioprocessing.
  • Summary References Study Questions Exercises.
  • 15. Adsorption, Ion Exchange, Chromatography, and Electrophoresis.
  • 15.0 Instructional Objectives.
  • 15.1 Sorbents.
  • 15.2 Equilibrium Considerations.
  • 15.3_ Kinetic and Transport Considerations.
  • 15.4 Equipment for Sorption Systems.
  • 15.5_ Slurry and Fixed-Bed Adsorption Systems.
  • 15.6 Continuous, Countercurrent Adsorption Systems.
  • 15.7 Ion-Exchange Cycle.
  • 15.8 Electrophoresis.
  • Summary References Study Questions Exercises.
  • PART 4 SEPARATIONS THAT INVOLVE A SOLID PHASE.
  • 16. Leaching and Washing.
  • 16.0 Instructional Objectives.
  • 16.1 Equipment for Leaching.
  • 16.2 Equilibrium-Stage Model for Leaching and Washing.
  • 16.3 Rate-Based Model for Leaching.
  • Summary References Study Questions Exercises.
  • 17. Crystallization, Desublimation, and Evaporation.
  • 17.0 Instructional Objectives.
  • 17.1 Crystal Geometry.
  • 17.2 Thermodynamic Considerations.
  • 17.3 Kinetics and Mass Transfer.
  • 17.4 Equipment for Solution Crystallization.
  • 17.5 The MSMPR Crystallization Model.
  • 17.6 Precipitation.
  • 17.7 Melt Crystallization.
  • 17.8 Zone Melting.
  • 17.9 Desublimation.
  • 17.10 Evaporation.
  • 17.11 Bioproduct Crystallization.
  • Summary References Study Questions Exercises
  • 18. Drying of Solids.
  • 18.0_ Instructional Objectives.
  • 18.1 Drying Equipment.
  • 18.2 Psychrometry.
  • 18.3 Equilibrium-Moisture Content of Solids.
  • 18.4 Drying Periods.
  • 18.5 Dryer Models.
  • 18.6 Drying of Bioproducts.
  • Summary References Study Questions Exercises.
  • PART 5 MECHANICAL SEPARATION OF PHASES.
  • 19. Mechanical Phase Separations.
  • 19.0 Instructional Objectives.
  • 19.1 Separation-Device Selection.
  • 19.2 Industrial Particle-Separator Devices.
  • 19.3 Design of Particle Separators.
  • 19.4 Design of Solid-Liquid Cake-Filtration Devices Based on Pressure Gradients.
  • 19.5 Centrifuge Devices for Solid-Liquid Separations.
  • 19.6 Wash Cycles.
  • 19.7 Mechanical Separations in Biotechnology.
  • Summary References Study Questions Exercises.
  • Answers to Selected Exercises.
  • Index.

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