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Demonstration of Gd-GEM detector design for neutron macromolecular crystallography applications

The European Spallation Source (ESS) in Lund, Sweden willbecome the world's most powerful thermal neutron source. TheMacromolecular Diffractometer (NMX) at the ESS requires three51.2 × 51.2 cm$^{2}$ detectors with reasonable detectionefficiency, sub-mm spatial resolution, a narrow point-spreadf...

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Autores principales: Pfeiffer, D., Brunbauer, F., Cristiglio, V., Hall-Wilton, R., Lupbergerf, M., Markó, M., Muller, H., Oksanen, E., Oliveri, E., Ropelewski, L., Rusu, A., Samarati, J., Scharenberg, L., van Stenis, M., Thuiner, P., Veenhof, R.
Lenguaje:eng
Publicado: 2022
Materias:
Acceso en línea:https://dx.doi.org/10.1088/1748-0221/18/04/P04023
http://cds.cern.ch/record/2853503
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author Pfeiffer, D.
Brunbauer, F.
Cristiglio, V.
Hall-Wilton, R.
Lupbergerf, M.
Markó, M.
Muller, H.
Oksanen, E.
Oliveri, E.
Ropelewski, L.
Rusu, A.
Samarati, J.
Scharenberg, L.
van Stenis, M.
Thuiner, P.
Veenhof, R.
author_facet Pfeiffer, D.
Brunbauer, F.
Cristiglio, V.
Hall-Wilton, R.
Lupbergerf, M.
Markó, M.
Muller, H.
Oksanen, E.
Oliveri, E.
Ropelewski, L.
Rusu, A.
Samarati, J.
Scharenberg, L.
van Stenis, M.
Thuiner, P.
Veenhof, R.
author_sort Pfeiffer, D.
collection CERN
description The European Spallation Source (ESS) in Lund, Sweden willbecome the world's most powerful thermal neutron source. TheMacromolecular Diffractometer (NMX) at the ESS requires three51.2 × 51.2 cm$^{2}$ detectors with reasonable detectionefficiency, sub-mm spatial resolution, a narrow point-spreadfunction (PSF), and good time resolution. This work presentsmeasurements with the improved version of the NMX detector prototypeconsisting of a Triple-GEM (Gas Electron Multiplier) detector with anatural Gd converter and a low material budget readout. The detectorwas successfully tested at the neutron reactor of the BudapestNeutron Centre (BNC) and the D16 instrument at the InstitutLaue-Langevin (ILL) in Grenoble. The measurements with Cadmium andGadolinium masks in Budapest demonstrate that the point-spreadfunction of the detector lacks long tails that could impede themeasurement of diffraction spot intensities. On the D16 instrumentat ILL, diffraction spots from Triose phosphate isomerase w/2-phosphoglycolate (PGA) inhibitor were measured both in the MILANDHelium-3 detector and the Gd-GEM. The comparison between the twodetectors shows a similar point-spread function in both detectors,and the expected efficiency ratio compared to the Helium-3detector. Both measurements together thus give good indications thatthe Gd-GEM detector fits the requirements for the NMX instrument atESS.
id cern-2853503
institution Organización Europea para la Investigación Nuclear
language eng
publishDate 2022
record_format invenio
spelling cern-28535032023-06-01T02:27:34Zdoi:10.1088/1748-0221/18/04/P04023http://cds.cern.ch/record/2853503engPfeiffer, D.Brunbauer, F.Cristiglio, V.Hall-Wilton, R.Lupbergerf, M.Markó, M.Muller, H.Oksanen, E.Oliveri, E.Ropelewski, L.Rusu, A.Samarati, J.Scharenberg, L.van Stenis, M.Thuiner, P.Veenhof, R.Demonstration of Gd-GEM detector design for neutron macromolecular crystallography applicationsphysics.ins-detDetectors and Experimental TechniquesThe European Spallation Source (ESS) in Lund, Sweden willbecome the world's most powerful thermal neutron source. TheMacromolecular Diffractometer (NMX) at the ESS requires three51.2 × 51.2 cm$^{2}$ detectors with reasonable detectionefficiency, sub-mm spatial resolution, a narrow point-spreadfunction (PSF), and good time resolution. This work presentsmeasurements with the improved version of the NMX detector prototypeconsisting of a Triple-GEM (Gas Electron Multiplier) detector with anatural Gd converter and a low material budget readout. The detectorwas successfully tested at the neutron reactor of the BudapestNeutron Centre (BNC) and the D16 instrument at the InstitutLaue-Langevin (ILL) in Grenoble. The measurements with Cadmium andGadolinium masks in Budapest demonstrate that the point-spreadfunction of the detector lacks long tails that could impede themeasurement of diffraction spot intensities. On the D16 instrumentat ILL, diffraction spots from Triose phosphate isomerase w/2-phosphoglycolate (PGA) inhibitor were measured both in the MILANDHelium-3 detector and the Gd-GEM. The comparison between the twodetectors shows a similar point-spread function in both detectors,and the expected efficiency ratio compared to the Helium-3detector. Both measurements together thus give good indications thatthe Gd-GEM detector fits the requirements for the NMX instrument atESS.The European Spallation Source (ESS) in Lund, Sweden will become the world's most powerful thermal neutron source. The Macromolecular Diffractometer (NMX) at the ESS requires three 51.2 x 51.2~cm$^{2}$ detectors with reasonable detection efficiency, sub-mm spatial resolution, a narrow point spread function (PSF) and good time resolution. This work presents measurements with the improved version of the NMX detector prototype consisting of a Triple-GEM detector with natural Gd converter and a low material budget readout. The detector was successfully tested at the neutron reactor of the Budapest Neutron Centre (BNC) and at the D16 instrument at the Institut Laue-Langevin (ILL) in Grenoble. The measurements with Cadmium and Gadolinium masks in Budapest demonstrate that the point spread function of the detector lacks long tails that could impede the measurement of diffraction spot intensities. On the D16 instrument at ILL, diffraction spots from Triose phosphate isomerase w/ 2-phosphoglycolate (PGA) inhibitor were measured both in the D16 Helium-3 detector and the Gd-GEM. The comparison between the two detectors show a similar point spread function in both detectors, and the expected efficiency ratio compared to the Helium-3 detector. Both measurements together thus give good indications that the Gd-GEM detector fits the requirements for the NMX instrument at ESS.arXiv:2211.04335oai:cds.cern.ch:28535032022-11-08
spellingShingle physics.ins-det
Detectors and Experimental Techniques
Pfeiffer, D.
Brunbauer, F.
Cristiglio, V.
Hall-Wilton, R.
Lupbergerf, M.
Markó, M.
Muller, H.
Oksanen, E.
Oliveri, E.
Ropelewski, L.
Rusu, A.
Samarati, J.
Scharenberg, L.
van Stenis, M.
Thuiner, P.
Veenhof, R.
Demonstration of Gd-GEM detector design for neutron macromolecular crystallography applications
title Demonstration of Gd-GEM detector design for neutron macromolecular crystallography applications
title_full Demonstration of Gd-GEM detector design for neutron macromolecular crystallography applications
title_fullStr Demonstration of Gd-GEM detector design for neutron macromolecular crystallography applications
title_full_unstemmed Demonstration of Gd-GEM detector design for neutron macromolecular crystallography applications
title_short Demonstration of Gd-GEM detector design for neutron macromolecular crystallography applications
title_sort demonstration of gd-gem detector design for neutron macromolecular crystallography applications
topic physics.ins-det
Detectors and Experimental Techniques
url https://dx.doi.org/10.1088/1748-0221/18/04/P04023
http://cds.cern.ch/record/2853503
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