Mapping the 3D position of battery cathode particles in Bragg coherent diffractive imaging

In Bragg coherent diffractive imaging, the precise location of the measured crystals in the interior of the sample is usually missing. Obtaining this information would help the study of the spatially dependent behavior of particles in the bulk of inhomogeneous samples, such as extra-thick battery ca...

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Detalles Bibliográficos
Autores principales: Shabalin, A. G., Zhang, M., Yao, W., Rysov, R., Ren, Z., Lapkin, D., Kim, Y.-Y., Assalauova, D., Mukharamova, N., Sprung, M., Vartanyants, I. A., Meng, Y. S., Shpyrko, O. G.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Short Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10000792/
https://www.ncbi.nlm.nih.gov/pubmed/36891858
http://dx.doi.org/10.1107/S1600577523000814
Descripción
Sumario:In Bragg coherent diffractive imaging, the precise location of the measured crystals in the interior of the sample is usually missing. Obtaining this information would help the study of the spatially dependent behavior of particles in the bulk of inhomogeneous samples, such as extra-thick battery cathodes. This work presents an approach to determine the 3D position of particles by precisely aligning them at the instrument axis of rotation. In the test experiment reported here, with a 60 µm-thick LiNi(0.5)Mn(1.5)O(4) battery cathode, the particles were located with a precision of 20 µm in the out-of-plane direction, and the in-plane coordinates were determined with a precision of 1 µm.

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