Mapping the 3D position of battery cathode particles in Bragg coherent diffractive imaging

In Bragg coherent diffractive imaging, the precise location of the measured crystals in the interior of the sample is usually missing. Obtaining this information would help the study of the spatially dependent behavior of particles in the bulk of inhomogeneous samples, such as extra-thick battery ca...

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Autores principales: Shabalin, A. G., Zhang, M., Yao, W., Rysov, R., Ren, Z., Lapkin, D., Kim, Y.-Y., Assalauova, D., Mukharamova, N., Sprung, M., Vartanyants, I. A., Meng, Y. S., Shpyrko, O. G.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Short Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10000792/
https://www.ncbi.nlm.nih.gov/pubmed/36891858
http://dx.doi.org/10.1107/S1600577523000814
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author Shabalin, A. G.
Zhang, M.
Yao, W.
Rysov, R.
Ren, Z.
Lapkin, D.
Kim, Y.-Y.
Assalauova, D.
Mukharamova, N.
Sprung, M.
Vartanyants, I. A.
Meng, Y. S.
Shpyrko, O. G.
author_facet Shabalin, A. G.
Zhang, M.
Yao, W.
Rysov, R.
Ren, Z.
Lapkin, D.
Kim, Y.-Y.
Assalauova, D.
Mukharamova, N.
Sprung, M.
Vartanyants, I. A.
Meng, Y. S.
Shpyrko, O. G.
author_sort Shabalin, A. G.
collection PubMed
description In Bragg coherent diffractive imaging, the precise location of the measured crystals in the interior of the sample is usually missing. Obtaining this information would help the study of the spatially dependent behavior of particles in the bulk of inhomogeneous samples, such as extra-thick battery cathodes. This work presents an approach to determine the 3D position of particles by precisely aligning them at the instrument axis of rotation. In the test experiment reported here, with a 60 µm-thick LiNi(0.5)Mn(1.5)O(4) battery cathode, the particles were located with a precision of 20 µm in the out-of-plane direction, and the in-plane coordinates were determined with a precision of 1 µm.
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spelling pubmed-100007922023-03-11 Mapping the 3D position of battery cathode particles in Bragg coherent diffractive imaging Shabalin, A. G. Zhang, M. Yao, W. Rysov, R. Ren, Z. Lapkin, D. Kim, Y.-Y. Assalauova, D. Mukharamova, N. Sprung, M. Vartanyants, I. A. Meng, Y. S. Shpyrko, O. G. J Synchrotron Radiat Short Communications In Bragg coherent diffractive imaging, the precise location of the measured crystals in the interior of the sample is usually missing. Obtaining this information would help the study of the spatially dependent behavior of particles in the bulk of inhomogeneous samples, such as extra-thick battery cathodes. This work presents an approach to determine the 3D position of particles by precisely aligning them at the instrument axis of rotation. In the test experiment reported here, with a 60 µm-thick LiNi(0.5)Mn(1.5)O(4) battery cathode, the particles were located with a precision of 20 µm in the out-of-plane direction, and the in-plane coordinates were determined with a precision of 1 µm. International Union of Crystallography 2023-02-16 /pmc/articles/PMC10000792/ /pubmed/36891858 http://dx.doi.org/10.1107/S1600577523000814 Text en © A. G. Shabalin et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Short Communications
Shabalin, A. G.
Zhang, M.
Yao, W.
Rysov, R.
Ren, Z.
Lapkin, D.
Kim, Y.-Y.
Assalauova, D.
Mukharamova, N.
Sprung, M.
Vartanyants, I. A.
Meng, Y. S.
Shpyrko, O. G.
Mapping the 3D position of battery cathode particles in Bragg coherent diffractive imaging
title Mapping the 3D position of battery cathode particles in Bragg coherent diffractive imaging
title_full Mapping the 3D position of battery cathode particles in Bragg coherent diffractive imaging
title_fullStr Mapping the 3D position of battery cathode particles in Bragg coherent diffractive imaging
title_full_unstemmed Mapping the 3D position of battery cathode particles in Bragg coherent diffractive imaging
title_short Mapping the 3D position of battery cathode particles in Bragg coherent diffractive imaging
title_sort mapping the 3d position of battery cathode particles in bragg coherent diffractive imaging
topic Short Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10000792/
https://www.ncbi.nlm.nih.gov/pubmed/36891858
http://dx.doi.org/10.1107/S1600577523000814
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