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Effects of K(2)TiF(6) and Electrolyte Temperatures on Energy Consumption and Properties of MAO Coatings on 6063 Aluminum Alloy

To decrease energy consumption and improve the performance of micro-arc oxidation (MAO) films on 6063 Al alloy, a policy of K(2)TiF(6) additive and electrolyte temperature control was adapted. The specific energy consumption relied on the K(2)TiF(6) additive and more particularly on the electrolyte...

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Autores principales: Xie, Xiaomeng, Yang, Erhui, Zhang, Ziying, Wei, Wu, Li, Dong, Zhao, Xiaolian, Yang, Ruixia, Li, Weizhou
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10004693/
https://www.ncbi.nlm.nih.gov/pubmed/36902945
http://dx.doi.org/10.3390/ma16051830
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author Xie, Xiaomeng
Yang, Erhui
Zhang, Ziying
Wei, Wu
Li, Dong
Zhao, Xiaolian
Yang, Ruixia
Li, Weizhou
author_facet Xie, Xiaomeng
Yang, Erhui
Zhang, Ziying
Wei, Wu
Li, Dong
Zhao, Xiaolian
Yang, Ruixia
Li, Weizhou
author_sort Xie, Xiaomeng
collection PubMed
description To decrease energy consumption and improve the performance of micro-arc oxidation (MAO) films on 6063 Al alloy, a policy of K(2)TiF(6) additive and electrolyte temperature control was adapted. The specific energy consumption relied on the K(2)TiF(6) additive and more particularly on the electrolyte temperatures. Scanning electron microscopy demonstrates that electrolytes with 5 g/L K(2)TiF(6) can effectively seal the surface pores and increase the thickness of the compact inner layer. Spectral analysis shows that the surface oxide coating consists of γ-Al(2)O(3) phase. Following 336 h of the total immersion process, the impedance modulus of the oxidation film, prepared at 25 °C (Ti5-25), remained 1.08 × 10(6) Ω·cm(2). Moreover, Ti5-25 has the best performance/energy-consumption ratio with a compact inner layer (2.5 ± 0.3 μm). This research found that the time of the big arc stage increased with the temperature, resulting in producing more internal defects in the film. In this work, we employ a dual-track strategy of additive and temperature providing an avenue to reduce the energy consumption of MAO on alloys.
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spelling pubmed-100046932023-03-11 Effects of K(2)TiF(6) and Electrolyte Temperatures on Energy Consumption and Properties of MAO Coatings on 6063 Aluminum Alloy Xie, Xiaomeng Yang, Erhui Zhang, Ziying Wei, Wu Li, Dong Zhao, Xiaolian Yang, Ruixia Li, Weizhou Materials (Basel) Article To decrease energy consumption and improve the performance of micro-arc oxidation (MAO) films on 6063 Al alloy, a policy of K(2)TiF(6) additive and electrolyte temperature control was adapted. The specific energy consumption relied on the K(2)TiF(6) additive and more particularly on the electrolyte temperatures. Scanning electron microscopy demonstrates that electrolytes with 5 g/L K(2)TiF(6) can effectively seal the surface pores and increase the thickness of the compact inner layer. Spectral analysis shows that the surface oxide coating consists of γ-Al(2)O(3) phase. Following 336 h of the total immersion process, the impedance modulus of the oxidation film, prepared at 25 °C (Ti5-25), remained 1.08 × 10(6) Ω·cm(2). Moreover, Ti5-25 has the best performance/energy-consumption ratio with a compact inner layer (2.5 ± 0.3 μm). This research found that the time of the big arc stage increased with the temperature, resulting in producing more internal defects in the film. In this work, we employ a dual-track strategy of additive and temperature providing an avenue to reduce the energy consumption of MAO on alloys. MDPI 2023-02-23 /pmc/articles/PMC10004693/ /pubmed/36902945 http://dx.doi.org/10.3390/ma16051830 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Xie, Xiaomeng
Yang, Erhui
Zhang, Ziying
Wei, Wu
Li, Dong
Zhao, Xiaolian
Yang, Ruixia
Li, Weizhou
Effects of K(2)TiF(6) and Electrolyte Temperatures on Energy Consumption and Properties of MAO Coatings on 6063 Aluminum Alloy
title Effects of K(2)TiF(6) and Electrolyte Temperatures on Energy Consumption and Properties of MAO Coatings on 6063 Aluminum Alloy
title_full Effects of K(2)TiF(6) and Electrolyte Temperatures on Energy Consumption and Properties of MAO Coatings on 6063 Aluminum Alloy
title_fullStr Effects of K(2)TiF(6) and Electrolyte Temperatures on Energy Consumption and Properties of MAO Coatings on 6063 Aluminum Alloy
title_full_unstemmed Effects of K(2)TiF(6) and Electrolyte Temperatures on Energy Consumption and Properties of MAO Coatings on 6063 Aluminum Alloy
title_short Effects of K(2)TiF(6) and Electrolyte Temperatures on Energy Consumption and Properties of MAO Coatings on 6063 Aluminum Alloy
title_sort effects of k(2)tif(6) and electrolyte temperatures on energy consumption and properties of mao coatings on 6063 aluminum alloy
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10004693/
https://www.ncbi.nlm.nih.gov/pubmed/36902945
http://dx.doi.org/10.3390/ma16051830
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