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Homogenization of Extrusion Billets of a Novel Al-Mg-Si-Cu Alloy with Increased Copper Content

Within the present work the homogenization of DC-cast (direct chill-cast) extrusion billets of Al-Mg-Si-Cu alloy was investigated. The alloy is characterized by higher Cu content than currently applied in 6xxx series. The aim of the work was analysis of billets homogenization conditions enabling max...

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Autores principales: Woźnicki, Antoni, Leszczyńska-Madej, Beata, Włoch, Grzegorz, Madura, Jacek, Bogusz, Marek, Leśniak, Dariusz
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10004725/
https://www.ncbi.nlm.nih.gov/pubmed/36903206
http://dx.doi.org/10.3390/ma16052091
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author Woźnicki, Antoni
Leszczyńska-Madej, Beata
Włoch, Grzegorz
Madura, Jacek
Bogusz, Marek
Leśniak, Dariusz
author_facet Woźnicki, Antoni
Leszczyńska-Madej, Beata
Włoch, Grzegorz
Madura, Jacek
Bogusz, Marek
Leśniak, Dariusz
author_sort Woźnicki, Antoni
collection PubMed
description Within the present work the homogenization of DC-cast (direct chill-cast) extrusion billets of Al-Mg-Si-Cu alloy was investigated. The alloy is characterized by higher Cu content than currently applied in 6xxx series. The aim of the work was analysis of billets homogenization conditions enabling maximum dissolution of soluble phases during heating and soaking as well as their re-precipitation during cooling in form of particles capable for rapid dissolution during subsequent processes. The material was subjected to laboratory homogenization and the microstructural effects were assessed on the basis of DSC (differential scanning calorimetry) tests, SEM/EDS (scanning electron microscopy/energy-dispersive spectroscopy) investigations and XRD (X-ray diffraction) analyses. The proposed homogenization scheme with three soaking stages enabled full dissolution of Q-Al(5)Cu(2)Mg(8)Si(6) and θ-Al(2)Cu phases. The β-Mg(2)Si phase was not dissolved completely during soaking, but its amount was significantly reduced. Fast cooling from homogenization was needed to refine β-Mg(2)Si phase particles, but despite this in the microstructure coarse Q-Al(5)Cu(2)Mg(8)Si(6) phase particles were found. Thus, rapid billets heating may lead to incipient melting at the temperature of about 545 °C and the careful selection of billets preheating and extrusion conditions was found necessary.
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spelling pubmed-100047252023-03-11 Homogenization of Extrusion Billets of a Novel Al-Mg-Si-Cu Alloy with Increased Copper Content Woźnicki, Antoni Leszczyńska-Madej, Beata Włoch, Grzegorz Madura, Jacek Bogusz, Marek Leśniak, Dariusz Materials (Basel) Article Within the present work the homogenization of DC-cast (direct chill-cast) extrusion billets of Al-Mg-Si-Cu alloy was investigated. The alloy is characterized by higher Cu content than currently applied in 6xxx series. The aim of the work was analysis of billets homogenization conditions enabling maximum dissolution of soluble phases during heating and soaking as well as their re-precipitation during cooling in form of particles capable for rapid dissolution during subsequent processes. The material was subjected to laboratory homogenization and the microstructural effects were assessed on the basis of DSC (differential scanning calorimetry) tests, SEM/EDS (scanning electron microscopy/energy-dispersive spectroscopy) investigations and XRD (X-ray diffraction) analyses. The proposed homogenization scheme with three soaking stages enabled full dissolution of Q-Al(5)Cu(2)Mg(8)Si(6) and θ-Al(2)Cu phases. The β-Mg(2)Si phase was not dissolved completely during soaking, but its amount was significantly reduced. Fast cooling from homogenization was needed to refine β-Mg(2)Si phase particles, but despite this in the microstructure coarse Q-Al(5)Cu(2)Mg(8)Si(6) phase particles were found. Thus, rapid billets heating may lead to incipient melting at the temperature of about 545 °C and the careful selection of billets preheating and extrusion conditions was found necessary. MDPI 2023-03-03 /pmc/articles/PMC10004725/ /pubmed/36903206 http://dx.doi.org/10.3390/ma16052091 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Woźnicki, Antoni
Leszczyńska-Madej, Beata
Włoch, Grzegorz
Madura, Jacek
Bogusz, Marek
Leśniak, Dariusz
Homogenization of Extrusion Billets of a Novel Al-Mg-Si-Cu Alloy with Increased Copper Content
title Homogenization of Extrusion Billets of a Novel Al-Mg-Si-Cu Alloy with Increased Copper Content
title_full Homogenization of Extrusion Billets of a Novel Al-Mg-Si-Cu Alloy with Increased Copper Content
title_fullStr Homogenization of Extrusion Billets of a Novel Al-Mg-Si-Cu Alloy with Increased Copper Content
title_full_unstemmed Homogenization of Extrusion Billets of a Novel Al-Mg-Si-Cu Alloy with Increased Copper Content
title_short Homogenization of Extrusion Billets of a Novel Al-Mg-Si-Cu Alloy with Increased Copper Content
title_sort homogenization of extrusion billets of a novel al-mg-si-cu alloy with increased copper content
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10004725/
https://www.ncbi.nlm.nih.gov/pubmed/36903206
http://dx.doi.org/10.3390/ma16052091
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