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Utilization of optimized microwave sintering to produce safe and sustainable one-part alkali-activated materials

Sodium hydroxide (NaOH) as an alkaline activator presents a vital limitation in the mass production of alkali-activated binders due to its severe effect on users’ safety. In this study, safe and sustainable one-part alkali-activated slag mixes (OP-AAS) were prepared through an efficient microwave si...

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Autores principales: Refaat, Moataz, Mohsen, Alaa, Nasr, El-Sayed A. R., Kohail, Mohamed
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10030970/
https://www.ncbi.nlm.nih.gov/pubmed/36944693
http://dx.doi.org/10.1038/s41598-023-31581-0
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author Refaat, Moataz
Mohsen, Alaa
Nasr, El-Sayed A. R.
Kohail, Mohamed
author_facet Refaat, Moataz
Mohsen, Alaa
Nasr, El-Sayed A. R.
Kohail, Mohamed
author_sort Refaat, Moataz
collection PubMed
description Sodium hydroxide (NaOH) as an alkaline activator presents a vital limitation in the mass production of alkali-activated binders due to its severe effect on users’ safety. In this study, safe and sustainable one-part alkali-activated slag mixes (OP-AAS) were prepared through an efficient microwave sintering for a mixture of active amorphous ground granulated blast furnace slag (GGBFS) and sodium hydroxide powder (NaOH). Different microwave-sintered powders were prepared using microwave energy of power 900 W for the mixture at different treatment periods (10, 20, and 30 min). Fresh and hardened properties of different OP-AAS mixes were studied. Moreover, the phase composition and microstructure were investigated using X-ray diffraction (XRD) analysis and scanning electron microscope (SEM). Cytotoxicity/viability testing was performed to evaluate the cell death induced by the developed materials to measure their safety for the user. According to compressive strength, cytotoxicity/viability analysis, environmental impact and cost calculation of developed OP-AAS, it is concluded that employing microwave sintering for a short duration is sufficient to produce safe binding materials with adequate mechanical properties suitable for commercial applications in the construction sector.
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spelling pubmed-100309702023-03-23 Utilization of optimized microwave sintering to produce safe and sustainable one-part alkali-activated materials Refaat, Moataz Mohsen, Alaa Nasr, El-Sayed A. R. Kohail, Mohamed Sci Rep Article Sodium hydroxide (NaOH) as an alkaline activator presents a vital limitation in the mass production of alkali-activated binders due to its severe effect on users’ safety. In this study, safe and sustainable one-part alkali-activated slag mixes (OP-AAS) were prepared through an efficient microwave sintering for a mixture of active amorphous ground granulated blast furnace slag (GGBFS) and sodium hydroxide powder (NaOH). Different microwave-sintered powders were prepared using microwave energy of power 900 W for the mixture at different treatment periods (10, 20, and 30 min). Fresh and hardened properties of different OP-AAS mixes were studied. Moreover, the phase composition and microstructure were investigated using X-ray diffraction (XRD) analysis and scanning electron microscope (SEM). Cytotoxicity/viability testing was performed to evaluate the cell death induced by the developed materials to measure their safety for the user. According to compressive strength, cytotoxicity/viability analysis, environmental impact and cost calculation of developed OP-AAS, it is concluded that employing microwave sintering for a short duration is sufficient to produce safe binding materials with adequate mechanical properties suitable for commercial applications in the construction sector. Nature Publishing Group UK 2023-03-21 /pmc/articles/PMC10030970/ /pubmed/36944693 http://dx.doi.org/10.1038/s41598-023-31581-0 Text en © The Author(s) 2023 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Refaat, Moataz
Mohsen, Alaa
Nasr, El-Sayed A. R.
Kohail, Mohamed
Utilization of optimized microwave sintering to produce safe and sustainable one-part alkali-activated materials
title Utilization of optimized microwave sintering to produce safe and sustainable one-part alkali-activated materials
title_full Utilization of optimized microwave sintering to produce safe and sustainable one-part alkali-activated materials
title_fullStr Utilization of optimized microwave sintering to produce safe and sustainable one-part alkali-activated materials
title_full_unstemmed Utilization of optimized microwave sintering to produce safe and sustainable one-part alkali-activated materials
title_short Utilization of optimized microwave sintering to produce safe and sustainable one-part alkali-activated materials
title_sort utilization of optimized microwave sintering to produce safe and sustainable one-part alkali-activated materials
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10030970/
https://www.ncbi.nlm.nih.gov/pubmed/36944693
http://dx.doi.org/10.1038/s41598-023-31581-0
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