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Investigation on the Microstructure and Mechanical Properties of the Ti-Ta Alloy with Unmelted Ta Particles by Laser Powder Bed Fusion

Titanium-tantalum (Ti-Ta) alloy has excellent biomechanical properties with high strength and low Young’s modulus, showing great application potential in the biomedical industry. In this study, Ti-Ta alloy samples were prepared by laser powder bed fusion (LPBF) technology with mixed pure 75 wt.% Ti...

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Autores principales: Gao, Mu, He, Dingyong, Cui, Li, Ma, Lixia, Tan, Zhen, Zhou, Zheng, Guo, Xingye
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10051491/
https://www.ncbi.nlm.nih.gov/pubmed/36984086
http://dx.doi.org/10.3390/ma16062208
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author Gao, Mu
He, Dingyong
Cui, Li
Ma, Lixia
Tan, Zhen
Zhou, Zheng
Guo, Xingye
author_facet Gao, Mu
He, Dingyong
Cui, Li
Ma, Lixia
Tan, Zhen
Zhou, Zheng
Guo, Xingye
author_sort Gao, Mu
collection PubMed
description Titanium-tantalum (Ti-Ta) alloy has excellent biomechanical properties with high strength and low Young’s modulus, showing great application potential in the biomedical industry. In this study, Ti-Ta alloy samples were prepared by laser powder bed fusion (LPBF) technology with mixed pure 75 wt.% Ti and 25 wt.% Ta powders as the feedstock. The maximum relative density of Ti-Ta samples prepared by LPBF reached 99.9%. It is well-accepted that four nonequilibrium phases, namely, α′, α″ and metastable β phase exist in Ti-Ta alloys. The structure of α′, α″ and β are hexagonal close-packed (HCP), base-centered orthorhombic (BCO) and body-centered cubic (BCC), respectively. X-ray Diffraction (XRD) analysis showed that the α′ phase transformed to the α″ phase with the increase of energy density. The lamellar α′/α″ phases and the α″ twins were generated in the prior β phase. The microstructure and mechanical properties of the Ti-Ta alloy were optimized with different LPBF processing parameters. The samples prepared by LPBF energy density of 381 J/mm(3) had a favorable ultimate strength (UTS) of 1076 ± 2 MPa and yield strength of 795 ± 16 MPa. The samples prepared by LPBF energy density of 76 had excellent ductility, with an elongation of 31% at fracture.
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spelling pubmed-100514912023-03-30 Investigation on the Microstructure and Mechanical Properties of the Ti-Ta Alloy with Unmelted Ta Particles by Laser Powder Bed Fusion Gao, Mu He, Dingyong Cui, Li Ma, Lixia Tan, Zhen Zhou, Zheng Guo, Xingye Materials (Basel) Article Titanium-tantalum (Ti-Ta) alloy has excellent biomechanical properties with high strength and low Young’s modulus, showing great application potential in the biomedical industry. In this study, Ti-Ta alloy samples were prepared by laser powder bed fusion (LPBF) technology with mixed pure 75 wt.% Ti and 25 wt.% Ta powders as the feedstock. The maximum relative density of Ti-Ta samples prepared by LPBF reached 99.9%. It is well-accepted that four nonequilibrium phases, namely, α′, α″ and metastable β phase exist in Ti-Ta alloys. The structure of α′, α″ and β are hexagonal close-packed (HCP), base-centered orthorhombic (BCO) and body-centered cubic (BCC), respectively. X-ray Diffraction (XRD) analysis showed that the α′ phase transformed to the α″ phase with the increase of energy density. The lamellar α′/α″ phases and the α″ twins were generated in the prior β phase. The microstructure and mechanical properties of the Ti-Ta alloy were optimized with different LPBF processing parameters. The samples prepared by LPBF energy density of 381 J/mm(3) had a favorable ultimate strength (UTS) of 1076 ± 2 MPa and yield strength of 795 ± 16 MPa. The samples prepared by LPBF energy density of 76 had excellent ductility, with an elongation of 31% at fracture. MDPI 2023-03-09 /pmc/articles/PMC10051491/ /pubmed/36984086 http://dx.doi.org/10.3390/ma16062208 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Gao, Mu
He, Dingyong
Cui, Li
Ma, Lixia
Tan, Zhen
Zhou, Zheng
Guo, Xingye
Investigation on the Microstructure and Mechanical Properties of the Ti-Ta Alloy with Unmelted Ta Particles by Laser Powder Bed Fusion
title Investigation on the Microstructure and Mechanical Properties of the Ti-Ta Alloy with Unmelted Ta Particles by Laser Powder Bed Fusion
title_full Investigation on the Microstructure and Mechanical Properties of the Ti-Ta Alloy with Unmelted Ta Particles by Laser Powder Bed Fusion
title_fullStr Investigation on the Microstructure and Mechanical Properties of the Ti-Ta Alloy with Unmelted Ta Particles by Laser Powder Bed Fusion
title_full_unstemmed Investigation on the Microstructure and Mechanical Properties of the Ti-Ta Alloy with Unmelted Ta Particles by Laser Powder Bed Fusion
title_short Investigation on the Microstructure and Mechanical Properties of the Ti-Ta Alloy with Unmelted Ta Particles by Laser Powder Bed Fusion
title_sort investigation on the microstructure and mechanical properties of the ti-ta alloy with unmelted ta particles by laser powder bed fusion
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10051491/
https://www.ncbi.nlm.nih.gov/pubmed/36984086
http://dx.doi.org/10.3390/ma16062208
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