A Combined Raman Spectroscopy and Atomic Force Microscopy System for In Situ and Real-Time Measures in Electrochemical Cells

An innovative and versatile set-up for in situ and real time measures in an electrochemical cell is described. An original coupling between micro-Raman spectroscopy and atomic force microscopy enables one to collect data on opaque electrodes. This system allows for the correlation of topographic ima...

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Autores principales: Bussetti, Gianlorenzo, Menegazzo, Marco, Mitko, Sergei, Castiglioni, Chiara, Tommasini, Matteo, Lucotti, Andrea, Magagnin, Luca, Russo, Valeria, Li Bassi, Andrea, Siena, Martina, Guadagnini, Alberto, Grillo, Samuele, Del Curto, Davide, Duò, Lamberto
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10051831/
https://www.ncbi.nlm.nih.gov/pubmed/36984119
http://dx.doi.org/10.3390/ma16062239
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author Bussetti, Gianlorenzo
Menegazzo, Marco
Mitko, Sergei
Castiglioni, Chiara
Tommasini, Matteo
Lucotti, Andrea
Magagnin, Luca
Russo, Valeria
Li Bassi, Andrea
Siena, Martina
Guadagnini, Alberto
Grillo, Samuele
Del Curto, Davide
Duò, Lamberto
author_facet Bussetti, Gianlorenzo
Menegazzo, Marco
Mitko, Sergei
Castiglioni, Chiara
Tommasini, Matteo
Lucotti, Andrea
Magagnin, Luca
Russo, Valeria
Li Bassi, Andrea
Siena, Martina
Guadagnini, Alberto
Grillo, Samuele
Del Curto, Davide
Duò, Lamberto
author_sort Bussetti, Gianlorenzo
collection PubMed
description An innovative and versatile set-up for in situ and real time measures in an electrochemical cell is described. An original coupling between micro-Raman spectroscopy and atomic force microscopy enables one to collect data on opaque electrodes. This system allows for the correlation of topographic images with chemical maps during the charge exchange occurring in oxidation/reduction processes. The proposed set-up plays a crucial role when reactions, both reversible and non-reversible, are studied step by step during electrochemical reactions and/or when local chemical analysis is required.
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spelling pubmed-100518312023-03-30 A Combined Raman Spectroscopy and Atomic Force Microscopy System for In Situ and Real-Time Measures in Electrochemical Cells Bussetti, Gianlorenzo Menegazzo, Marco Mitko, Sergei Castiglioni, Chiara Tommasini, Matteo Lucotti, Andrea Magagnin, Luca Russo, Valeria Li Bassi, Andrea Siena, Martina Guadagnini, Alberto Grillo, Samuele Del Curto, Davide Duò, Lamberto Materials (Basel) Article An innovative and versatile set-up for in situ and real time measures in an electrochemical cell is described. An original coupling between micro-Raman spectroscopy and atomic force microscopy enables one to collect data on opaque electrodes. This system allows for the correlation of topographic images with chemical maps during the charge exchange occurring in oxidation/reduction processes. The proposed set-up plays a crucial role when reactions, both reversible and non-reversible, are studied step by step during electrochemical reactions and/or when local chemical analysis is required. MDPI 2023-03-10 /pmc/articles/PMC10051831/ /pubmed/36984119 http://dx.doi.org/10.3390/ma16062239 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Bussetti, Gianlorenzo
Menegazzo, Marco
Mitko, Sergei
Castiglioni, Chiara
Tommasini, Matteo
Lucotti, Andrea
Magagnin, Luca
Russo, Valeria
Li Bassi, Andrea
Siena, Martina
Guadagnini, Alberto
Grillo, Samuele
Del Curto, Davide
Duò, Lamberto
A Combined Raman Spectroscopy and Atomic Force Microscopy System for In Situ and Real-Time Measures in Electrochemical Cells
title A Combined Raman Spectroscopy and Atomic Force Microscopy System for In Situ and Real-Time Measures in Electrochemical Cells
title_full A Combined Raman Spectroscopy and Atomic Force Microscopy System for In Situ and Real-Time Measures in Electrochemical Cells
title_fullStr A Combined Raman Spectroscopy and Atomic Force Microscopy System for In Situ and Real-Time Measures in Electrochemical Cells
title_full_unstemmed A Combined Raman Spectroscopy and Atomic Force Microscopy System for In Situ and Real-Time Measures in Electrochemical Cells
title_short A Combined Raman Spectroscopy and Atomic Force Microscopy System for In Situ and Real-Time Measures in Electrochemical Cells
title_sort combined raman spectroscopy and atomic force microscopy system for in situ and real-time measures in electrochemical cells
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10051831/
https://www.ncbi.nlm.nih.gov/pubmed/36984119
http://dx.doi.org/10.3390/ma16062239
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