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Fabrication of Ultra-Sharp Tips by Dynamic Chemical Etching Process for Scanning Near-Field Microwave Microscopy

This work details an effective dynamic chemical etching technique to fabricate ultra-sharp tips for Scanning Near-Field Microwave Microscopy (SNMM). The protruded cylindrical part of the inner conductor in a commercial SMA (Sub Miniature A) coaxial connector is tapered by a dynamic chemical etching...

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Detalles Bibliográficos
Autores principales: Joseph, C. H., Capoccia, Giovanni, Lucibello, Andrea, Proietti, Emanuela, Sardi, Giovanni Maria, Bartolucci, Giancarlo, Marcelli, Romolo
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10056389/
https://www.ncbi.nlm.nih.gov/pubmed/36992071
http://dx.doi.org/10.3390/s23063360
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author Joseph, C. H.
Capoccia, Giovanni
Lucibello, Andrea
Proietti, Emanuela
Sardi, Giovanni Maria
Bartolucci, Giancarlo
Marcelli, Romolo
author_facet Joseph, C. H.
Capoccia, Giovanni
Lucibello, Andrea
Proietti, Emanuela
Sardi, Giovanni Maria
Bartolucci, Giancarlo
Marcelli, Romolo
author_sort Joseph, C. H.
collection PubMed
description This work details an effective dynamic chemical etching technique to fabricate ultra-sharp tips for Scanning Near-Field Microwave Microscopy (SNMM). The protruded cylindrical part of the inner conductor in a commercial SMA (Sub Miniature A) coaxial connector is tapered by a dynamic chemical etching process using ferric chloride. The technique is optimized to fabricate ultra-sharp probe tips with controllable shapes and tapered down to have a radius of tip apex around ∼1 [Formula: see text] m. The detailed optimization facilitated the fabrication of reproducible high-quality probes suitable for non-contact SNMM operation. A simple analytical model is also presented to better describe the dynamics of the tip formation. The near-field characteristics of the tips are evaluated by finite element method (FEM) based electromagnetic simulations and the performance of the probes has been validated experimentally by means of imaging a metal-dielectric sample using the in-house scanning near-field microwave microscopy system.
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spelling pubmed-100563892023-03-30 Fabrication of Ultra-Sharp Tips by Dynamic Chemical Etching Process for Scanning Near-Field Microwave Microscopy Joseph, C. H. Capoccia, Giovanni Lucibello, Andrea Proietti, Emanuela Sardi, Giovanni Maria Bartolucci, Giancarlo Marcelli, Romolo Sensors (Basel) Article This work details an effective dynamic chemical etching technique to fabricate ultra-sharp tips for Scanning Near-Field Microwave Microscopy (SNMM). The protruded cylindrical part of the inner conductor in a commercial SMA (Sub Miniature A) coaxial connector is tapered by a dynamic chemical etching process using ferric chloride. The technique is optimized to fabricate ultra-sharp probe tips with controllable shapes and tapered down to have a radius of tip apex around ∼1 [Formula: see text] m. The detailed optimization facilitated the fabrication of reproducible high-quality probes suitable for non-contact SNMM operation. A simple analytical model is also presented to better describe the dynamics of the tip formation. The near-field characteristics of the tips are evaluated by finite element method (FEM) based electromagnetic simulations and the performance of the probes has been validated experimentally by means of imaging a metal-dielectric sample using the in-house scanning near-field microwave microscopy system. MDPI 2023-03-22 /pmc/articles/PMC10056389/ /pubmed/36992071 http://dx.doi.org/10.3390/s23063360 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Joseph, C. H.
Capoccia, Giovanni
Lucibello, Andrea
Proietti, Emanuela
Sardi, Giovanni Maria
Bartolucci, Giancarlo
Marcelli, Romolo
Fabrication of Ultra-Sharp Tips by Dynamic Chemical Etching Process for Scanning Near-Field Microwave Microscopy
title Fabrication of Ultra-Sharp Tips by Dynamic Chemical Etching Process for Scanning Near-Field Microwave Microscopy
title_full Fabrication of Ultra-Sharp Tips by Dynamic Chemical Etching Process for Scanning Near-Field Microwave Microscopy
title_fullStr Fabrication of Ultra-Sharp Tips by Dynamic Chemical Etching Process for Scanning Near-Field Microwave Microscopy
title_full_unstemmed Fabrication of Ultra-Sharp Tips by Dynamic Chemical Etching Process for Scanning Near-Field Microwave Microscopy
title_short Fabrication of Ultra-Sharp Tips by Dynamic Chemical Etching Process for Scanning Near-Field Microwave Microscopy
title_sort fabrication of ultra-sharp tips by dynamic chemical etching process for scanning near-field microwave microscopy
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10056389/
https://www.ncbi.nlm.nih.gov/pubmed/36992071
http://dx.doi.org/10.3390/s23063360
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