Cargando…

Residues and Safety Assessment of Cyantraniliprole and Indoxacarb in Wild Garlic (Allium vineale)

In this study, the residual behavior and safety of cyantraniliprole and indoxacarb applied to wild garlic (Allium vineale) were investigated. Samples were harvested after treatments of 0, 3, 7, and 14 days, then were prepared and extracted following the QuEChERS method and analyzed by UPLC-MS/MS. Th...

Descripción completa

Detalles Bibliográficos
Autores principales: Sardar, Syed Wasim, Choi, Jeong Yoon, Jo, Yeong Ju, Ishag, Abd Elaziz Sulieman Ahmed, Kim, Min-woo, Ham, Hun Ju
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10056846/
https://www.ncbi.nlm.nih.gov/pubmed/36976984
http://dx.doi.org/10.3390/toxics11030219
_version_ 1785016222918639616
author Sardar, Syed Wasim
Choi, Jeong Yoon
Jo, Yeong Ju
Ishag, Abd Elaziz Sulieman Ahmed
Kim, Min-woo
Ham, Hun Ju
author_facet Sardar, Syed Wasim
Choi, Jeong Yoon
Jo, Yeong Ju
Ishag, Abd Elaziz Sulieman Ahmed
Kim, Min-woo
Ham, Hun Ju
author_sort Sardar, Syed Wasim
collection PubMed
description In this study, the residual behavior and safety of cyantraniliprole and indoxacarb applied to wild garlic (Allium vineale) were investigated. Samples were harvested after treatments of 0, 3, 7, and 14 days, then were prepared and extracted following the QuEChERS method and analyzed by UPLC-MS/MS. The linearity (R(2) ≥ 0.99) of the calibration curves was excellent for both compounds. The average recoveries of cyantraniliprole and indoxacarb at two spiking concentrations (0.01 and 0.1 mg/kg) ranged from 94.2% to 111.4%. The relative standard deviation value was below 10%. The initial concentrations of cyantraniliprole and indoxacarb in wild garlic were degraded to 75% and 93% after seven days. The average half-lives were 1.83 and 1.14 days for cyantraniliprole and indoxacarb, respectively. The preharvest intervals (PHIs) for the two pesticides in wild garlic are recommended as two treatments seven days before harvest. The safety assessment data indicated that the percent acceptable daily intakes of cyantraniliprole and indoxacarb were 0.3 × 10(−4)% and 6.7 × 10(−2)%, respectively, in wild garlic. The theoretical maximum daily intake value of cyantraniliprole was 9.80%, and that of indoxacarb was 60.54%. Both compounds’ residues in wild garlic pose low health risks to consumers. The findings of the current investigation provide essential data for the safe use of cyantraniliprole and indoxacarb in wild garlic.
format Online
Article
Text
id pubmed-10056846
institution National Center for Biotechnology Information
language English
publishDate 2023
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-100568462023-03-30 Residues and Safety Assessment of Cyantraniliprole and Indoxacarb in Wild Garlic (Allium vineale) Sardar, Syed Wasim Choi, Jeong Yoon Jo, Yeong Ju Ishag, Abd Elaziz Sulieman Ahmed Kim, Min-woo Ham, Hun Ju Toxics Article In this study, the residual behavior and safety of cyantraniliprole and indoxacarb applied to wild garlic (Allium vineale) were investigated. Samples were harvested after treatments of 0, 3, 7, and 14 days, then were prepared and extracted following the QuEChERS method and analyzed by UPLC-MS/MS. The linearity (R(2) ≥ 0.99) of the calibration curves was excellent for both compounds. The average recoveries of cyantraniliprole and indoxacarb at two spiking concentrations (0.01 and 0.1 mg/kg) ranged from 94.2% to 111.4%. The relative standard deviation value was below 10%. The initial concentrations of cyantraniliprole and indoxacarb in wild garlic were degraded to 75% and 93% after seven days. The average half-lives were 1.83 and 1.14 days for cyantraniliprole and indoxacarb, respectively. The preharvest intervals (PHIs) for the two pesticides in wild garlic are recommended as two treatments seven days before harvest. The safety assessment data indicated that the percent acceptable daily intakes of cyantraniliprole and indoxacarb were 0.3 × 10(−4)% and 6.7 × 10(−2)%, respectively, in wild garlic. The theoretical maximum daily intake value of cyantraniliprole was 9.80%, and that of indoxacarb was 60.54%. Both compounds’ residues in wild garlic pose low health risks to consumers. The findings of the current investigation provide essential data for the safe use of cyantraniliprole and indoxacarb in wild garlic. MDPI 2023-02-25 /pmc/articles/PMC10056846/ /pubmed/36976984 http://dx.doi.org/10.3390/toxics11030219 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Sardar, Syed Wasim
Choi, Jeong Yoon
Jo, Yeong Ju
Ishag, Abd Elaziz Sulieman Ahmed
Kim, Min-woo
Ham, Hun Ju
Residues and Safety Assessment of Cyantraniliprole and Indoxacarb in Wild Garlic (Allium vineale)
title Residues and Safety Assessment of Cyantraniliprole and Indoxacarb in Wild Garlic (Allium vineale)
title_full Residues and Safety Assessment of Cyantraniliprole and Indoxacarb in Wild Garlic (Allium vineale)
title_fullStr Residues and Safety Assessment of Cyantraniliprole and Indoxacarb in Wild Garlic (Allium vineale)
title_full_unstemmed Residues and Safety Assessment of Cyantraniliprole and Indoxacarb in Wild Garlic (Allium vineale)
title_short Residues and Safety Assessment of Cyantraniliprole and Indoxacarb in Wild Garlic (Allium vineale)
title_sort residues and safety assessment of cyantraniliprole and indoxacarb in wild garlic (allium vineale)
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10056846/
https://www.ncbi.nlm.nih.gov/pubmed/36976984
http://dx.doi.org/10.3390/toxics11030219
work_keys_str_mv AT sardarsyedwasim residuesandsafetyassessmentofcyantraniliproleandindoxacarbinwildgarlicalliumvineale
AT choijeongyoon residuesandsafetyassessmentofcyantraniliproleandindoxacarbinwildgarlicalliumvineale
AT joyeongju residuesandsafetyassessmentofcyantraniliproleandindoxacarbinwildgarlicalliumvineale
AT ishagabdelazizsuliemanahmed residuesandsafetyassessmentofcyantraniliproleandindoxacarbinwildgarlicalliumvineale
AT kimminwoo residuesandsafetyassessmentofcyantraniliproleandindoxacarbinwildgarlicalliumvineale
AT hamhunju residuesandsafetyassessmentofcyantraniliproleandindoxacarbinwildgarlicalliumvineale