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Optimization of the Electrochemical Method of Obtaining Graphene Nanoplatelets (GNPs)
Graphene nanoplatelets (GNPs) were prepared using the electrolytic exfoliation method on graphite foil in an ammonium sulfate solution. A series of experiments were conducted in order to optimize the production of the flakes by varying the pH of the solution, applied voltage and current, duration of...
| Autores principales: | , , , , , , , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
| Publicado: |
MDPI
2023
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| Materias: | |
| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10057930/ https://www.ncbi.nlm.nih.gov/pubmed/36984068 http://dx.doi.org/10.3390/ma16062188 |
| _version_ | 1785016493070614528 |
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| author | Grabowska, Adrianna Kowalczyk, Jerzy Tomala, Robert Ptak, Maciej Małecka, Małgorzata Wędzyńska, Anna Stefanski, Mariusz Stręk, Wiesław Głuchowski, Paweł |
| author_facet | Grabowska, Adrianna Kowalczyk, Jerzy Tomala, Robert Ptak, Maciej Małecka, Małgorzata Wędzyńska, Anna Stefanski, Mariusz Stręk, Wiesław Głuchowski, Paweł |
| author_sort | Grabowska, Adrianna |
| collection | PubMed |
| description | Graphene nanoplatelets (GNPs) were prepared using the electrolytic exfoliation method on graphite foil in an ammonium sulfate solution. A series of experiments were conducted in order to optimize the production of the flakes by varying the pH of the solution, applied voltage and current, duration of electrolysis, temperature in the electrolytic system, and type and duration of the ultrasound interaction. The quality of the produced graphene nanoplatelets was analyzed using X-ray diffraction, Raman and IR spectroscopy, and TEM. |
| format | Online Article Text |
| id | pubmed-10057930 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2023 |
| publisher | MDPI |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-100579302023-03-30 Optimization of the Electrochemical Method of Obtaining Graphene Nanoplatelets (GNPs) Grabowska, Adrianna Kowalczyk, Jerzy Tomala, Robert Ptak, Maciej Małecka, Małgorzata Wędzyńska, Anna Stefanski, Mariusz Stręk, Wiesław Głuchowski, Paweł Materials (Basel) Article Graphene nanoplatelets (GNPs) were prepared using the electrolytic exfoliation method on graphite foil in an ammonium sulfate solution. A series of experiments were conducted in order to optimize the production of the flakes by varying the pH of the solution, applied voltage and current, duration of electrolysis, temperature in the electrolytic system, and type and duration of the ultrasound interaction. The quality of the produced graphene nanoplatelets was analyzed using X-ray diffraction, Raman and IR spectroscopy, and TEM. MDPI 2023-03-09 /pmc/articles/PMC10057930/ /pubmed/36984068 http://dx.doi.org/10.3390/ma16062188 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
| spellingShingle | Article Grabowska, Adrianna Kowalczyk, Jerzy Tomala, Robert Ptak, Maciej Małecka, Małgorzata Wędzyńska, Anna Stefanski, Mariusz Stręk, Wiesław Głuchowski, Paweł Optimization of the Electrochemical Method of Obtaining Graphene Nanoplatelets (GNPs) |
| title | Optimization of the Electrochemical Method of Obtaining Graphene Nanoplatelets (GNPs) |
| title_full | Optimization of the Electrochemical Method of Obtaining Graphene Nanoplatelets (GNPs) |
| title_fullStr | Optimization of the Electrochemical Method of Obtaining Graphene Nanoplatelets (GNPs) |
| title_full_unstemmed | Optimization of the Electrochemical Method of Obtaining Graphene Nanoplatelets (GNPs) |
| title_short | Optimization of the Electrochemical Method of Obtaining Graphene Nanoplatelets (GNPs) |
| title_sort | optimization of the electrochemical method of obtaining graphene nanoplatelets (gnps) |
| topic | Article |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10057930/ https://www.ncbi.nlm.nih.gov/pubmed/36984068 http://dx.doi.org/10.3390/ma16062188 |
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