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A Novel Atomically Resolved Scanning Tunneling Microscope Capable of Working in Cryogen-Free Superconducting Magnet

We present a novel homebuilt scanning tunneling microscope (STM) with atomic resolution integrated into a cryogen-free superconducting magnet system with a variable temperature insert. The STM head is designed as a nested structure of double piezoelectric tubes (PTs), which are connected coaxially t...

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Detalles Bibliográficos
Autores principales: Geng, Tao, Wang, Jihao, Meng, Wenjie, Zhang, Jing, Feng, Qiyuan, Hou, Yubin, Lu, Qingyou
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10059664/
https://www.ncbi.nlm.nih.gov/pubmed/36985044
http://dx.doi.org/10.3390/mi14030637
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author Geng, Tao
Wang, Jihao
Meng, Wenjie
Zhang, Jing
Feng, Qiyuan
Hou, Yubin
Lu, Qingyou
author_facet Geng, Tao
Wang, Jihao
Meng, Wenjie
Zhang, Jing
Feng, Qiyuan
Hou, Yubin
Lu, Qingyou
author_sort Geng, Tao
collection PubMed
description We present a novel homebuilt scanning tunneling microscope (STM) with atomic resolution integrated into a cryogen-free superconducting magnet system with a variable temperature insert. The STM head is designed as a nested structure of double piezoelectric tubes (PTs), which are connected coaxially through a sapphire frame whose top has a sample stage. A single shaft made of tantalum, with the STM tip on top, is held firmly by a spring strip inside the internal PT. The external PT drives the shaft to the tip–sample junction based on the SpiderDrive principle, and the internal PT completes the subsequent scanning and imaging work. The STM head is simple, compact, and easy to assemble. The excellent performance of the device was demonstrated by obtaining atomic-resolution images of graphite and low drift rates of 30.2 pm/min and 41.4 pm/min in the X–Y plane and Z direction, respectively, at 300K. In addition, we cooled the sample to 1.6 K and took atomic-resolution images of graphite and NbSe(2). Finally, we performed a magnetic field sweep test from 0 T to 9 T at 70 K, obtaining distinct graphite images with atomic resolution under varying magnetic fields. These experiments show our newly developed STM’s high stability, vibration resistance, and immunity to high magnetic fields.
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spelling pubmed-100596642023-03-30 A Novel Atomically Resolved Scanning Tunneling Microscope Capable of Working in Cryogen-Free Superconducting Magnet Geng, Tao Wang, Jihao Meng, Wenjie Zhang, Jing Feng, Qiyuan Hou, Yubin Lu, Qingyou Micromachines (Basel) Article We present a novel homebuilt scanning tunneling microscope (STM) with atomic resolution integrated into a cryogen-free superconducting magnet system with a variable temperature insert. The STM head is designed as a nested structure of double piezoelectric tubes (PTs), which are connected coaxially through a sapphire frame whose top has a sample stage. A single shaft made of tantalum, with the STM tip on top, is held firmly by a spring strip inside the internal PT. The external PT drives the shaft to the tip–sample junction based on the SpiderDrive principle, and the internal PT completes the subsequent scanning and imaging work. The STM head is simple, compact, and easy to assemble. The excellent performance of the device was demonstrated by obtaining atomic-resolution images of graphite and low drift rates of 30.2 pm/min and 41.4 pm/min in the X–Y plane and Z direction, respectively, at 300K. In addition, we cooled the sample to 1.6 K and took atomic-resolution images of graphite and NbSe(2). Finally, we performed a magnetic field sweep test from 0 T to 9 T at 70 K, obtaining distinct graphite images with atomic resolution under varying magnetic fields. These experiments show our newly developed STM’s high stability, vibration resistance, and immunity to high magnetic fields. MDPI 2023-03-11 /pmc/articles/PMC10059664/ /pubmed/36985044 http://dx.doi.org/10.3390/mi14030637 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Geng, Tao
Wang, Jihao
Meng, Wenjie
Zhang, Jing
Feng, Qiyuan
Hou, Yubin
Lu, Qingyou
A Novel Atomically Resolved Scanning Tunneling Microscope Capable of Working in Cryogen-Free Superconducting Magnet
title A Novel Atomically Resolved Scanning Tunneling Microscope Capable of Working in Cryogen-Free Superconducting Magnet
title_full A Novel Atomically Resolved Scanning Tunneling Microscope Capable of Working in Cryogen-Free Superconducting Magnet
title_fullStr A Novel Atomically Resolved Scanning Tunneling Microscope Capable of Working in Cryogen-Free Superconducting Magnet
title_full_unstemmed A Novel Atomically Resolved Scanning Tunneling Microscope Capable of Working in Cryogen-Free Superconducting Magnet
title_short A Novel Atomically Resolved Scanning Tunneling Microscope Capable of Working in Cryogen-Free Superconducting Magnet
title_sort novel atomically resolved scanning tunneling microscope capable of working in cryogen-free superconducting magnet
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10059664/
https://www.ncbi.nlm.nih.gov/pubmed/36985044
http://dx.doi.org/10.3390/mi14030637
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