Cargando…

Unequivocal identification of two-bond heteronuclear correlations in natural products at nanomole scale by i-HMBC

HMBC is an essential NMR experiment for determining multiple bond heteronuclear correlations in small to medium-sized organic molecules, including natural products, yet its major limitation is the inability to differentiate two-bond from longer-range correlations. There have been several attempts to...

Descripción completa

Detalles Bibliográficos
Autores principales:	Wang, Yunyi, Fan, Aili, Cohen, Ryan D., Dal Poggetto, Guilherme, Huang, Zheng, Yang, Haifeng, Martin, Gary E., Sherer, Edward C., Reibarkh, Mikhail, Wang, Xiao
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	Nature Publishing Group UK 2023
Materias:	Article
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10070429/ https://www.ncbi.nlm.nih.gov/pubmed/37012241 http://dx.doi.org/10.1038/s41467-023-37289-z

Ejemplares similares

Unequivocal structure confirmation of a breitfussin analog by anisotropic NMR measurements
por: Ndukwe, Ikenna E., et al.
Publicado: (2020)

Rapid Measurement of Heteronuclear Coupling Constants in Complex NMR Spectra
por: Mycroft, Coral, et al.
Publicado: (2023)

Selective Nuclear Magnetic Resonance Experiments for Sign-Sensitive Determination of Heteronuclear Couplings: Expanding the Analysis of Crude Reaction Mixtures
por: Dal Poggetto, Guilherme, et al.
Publicado: (2020)

Optimization of Covalent MKK7 Inhibitors via Crude Nanomole-Scale Libraries
por: Gehrtz, Paul, et al.
Publicado: (2022)

Nanomole-scale Protein Solid-state NMR by Breaking Intrinsic (1)H-T(1) Boundaries
por: Wickramasinghe, Nalinda P., et al.
Publicado: (2009)

A Theoretical Study of the Halogen Bond between Heteronuclear Halogen and Benzene
por: Luo, Jun, et al.
Publicado: (2022)

The unequivocal preponderance of biocomputation in clinical virology
por: Chun, Sechul, et al.
Publicado: (2018)

Incorporation of (4)J-HMBC and NOE Data into Computer-Assisted Structure Elucidation with WebCocon
por: Köck, Matthias, et al.
Publicado: (2021)

HmbC, a Protein of the HMG Family, Participates in the Regulation of Carotenoid Biosynthesis in Fusarium fujikuroi
por: Franco-Losilla, Marta, et al.
Publicado: (2023)

DELTA50: A Highly Accurate Database of Experimental (1)H and (13)C NMR Chemical Shifts Applied to DFT Benchmarking
por: Cohen, Ryan D., et al.
Publicado: (2023)

Quantitative analysis of naphthalene, 1-naphthol and 2-naphthol at nanomol levels in geothermal fluids using SPE with HPLC
por: Sajkowski, Lucjan, et al.
Publicado: (2023)

Heteronuclear soliton molecules in optical microresonators
por: Weng, Wenle, et al.
Publicado: (2020)

Let us be unequivocal about social justice in nursing
por: Abu, Victor Kpandemoi
Publicado: (2020)

The transposed-word effect provides no unequivocal evidence for parallel processing
por: Milledge, Sara V., et al.
Publicado: (2023)

Modeling framework for isotopic labeling of heteronuclear moieties
por: Borkum, Mark I., et al.
Publicado: (2017)

Heteronuclear and homonuclear radio-frequency-driven recoupling
por: Nimerovsky, Evgeny, et al.
Publicado: (2021)

A Distributional Model of Bound Ligand Conformational Strain: From Small Molecules up to Large Peptidic Macrocycles
por: Jain, Ajay N., et al.
Publicado: (2023)

Controlled nano-agglomerates as stabile SERS reporters for unequivocal labelling
por: Xiao, Can, et al.
Publicado: (2022)

Interaction-induced decay of a heteronuclear two-atom system
por: Xu, Peng, et al.
Publicado: (2015)

Application of Heteronuclear NMR Spectroscopy to Bioinorganic and Medicinal Chemistry
por: Fotopoulou, Eirini, et al.
Publicado: (2018)

Ligand‐stabilized heteronuclear diatomics of group 13 and 15
por: Kaur, Aishvaryadeep, et al.
Publicado: (2022)

Solution structure of Gaussia Luciferase with five disulfide bonds and identification of a putative coelenterazine binding cavity by heteronuclear NMR
por: Wu, Nan, et al.
Publicado: (2020)

Evaluation of Band-Selective HSQC and HMBC: Methodological Validation on the Cyclosporin Cyclic Peptide and Application for Poly(3-hydroxyalkanoate)s Stereoregularity Determination
por: Caytan, Elsa, et al.
Publicado: (2018)

(11)B and (1)H–(11)B HMBC NMR as a Tool for Identification of a Boron-Containing Nucleoside Dimer
por: Blue, Riley M., et al.
Publicado: (2022)

Making the equivocal unequivocal: standardization of clean margins in diabetic foot osteomyelitis
por: Schmidt, Brian M., et al.
Publicado: (2020)

Complex macrocycle exploration: parallel, heuristic, and constraint-based conformer generation using ForceGen
por: Jain, Ajay N., et al.
Publicado: (2019)

Direct Detection of Hydrogen Bonds in Supramolecular Systems Using (1)H–(15)N Heteronuclear Multiple Quantum Coherence Spectroscopy
por: Jinks, Michael A., et al.
Publicado: (2022)

Applications of heteronuclear NMR spectroscopy in biological and medicinal inorganic chemistry
por: Ronconi, Luca, et al.
Publicado: (2008)

Intra-residue methyl–methyl correlations for valine and leucine residues in large proteins from a 3D-HMBC-HMQC experiment
por: Siemons, Lucas, et al.
Publicado: (2019)

Highly Coordinated Heteronuclear Calcium–Iron Carbonyl Cation Complexes [CaFe(CO)(n)](+) (n=5–12) with d−d Bonding
por: Jin, Xiaoyang, et al.
Publicado: (2021)

Unequivocal imaging of aluminium in human cells and tissues by an improved method using morin
por: Mold, Matthew J., et al.
Publicado: (2019)

Inflammation Beats Cholesterol: A Comment on the Unequivocal Driver of Cardiovascular Disease Risk
por: Vaccarezza, Mauro, et al.
Publicado: (2023)

Earliest known unequivocal rhinocerotoid sheds new light on the origin of Giant Rhinos and phylogeny of early rhinocerotoids
por: Wang, Haibing, et al.
Publicado: (2016)

Chromatographic Study of Novel Heteronuclear Complexes with Schiff Base as Main Ligand
por: Wronka, Agnieszka, et al.
Publicado: (2014)

Simultaneously Enhancing Spectral Resolution and Sensitivity in Heteronuclear Correlation NMR Spectroscopy**
por: Paudel, Liladhar, et al.
Publicado: (2013)

Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation
por: Gyöngyösi, Tamás, et al.
Publicado: (2019)

Rationalising Heteronuclear Decoupling in Refocussing Applications of Solid‐State NMR Spectroscopy
por: Frantsuzov, Ilya, et al.
Publicado: (2017)

Heteronuclear Dirhodium-Gold Anionic Complexes: Polymeric Chains and Discrete Units
por: Fernandez-Bartolome, Estefania, et al.
Publicado: (2020)

The protecting-group free selective 3′-functionalization of nucleosides
por: McCabe Dunn, Jamie M., et al.
Publicado: (2017)

Unequivocal identification of intracellular aluminium adjuvant in a monocytic THP-1 cell line
por: Mold, Matthew, et al.
Publicado: (2014)

Cannot write session to /tmp/vufind_sessions/sess_tb55tqj33ol357to9k0b21nrlu