Synthesis and crystal structure of N-(5-acetyl-4-methyl­pyrimidin-2-yl)benzene­sulfonamide

N-(5-Acetyl-4-methyl­pyrimidin-2-yl)benzene­sulfonamide, C(13)H(13)N(3)O(3)S, was sythesized and characterized by single-crystal X-ray diffraction. In the crystal, π–π inter­actions between the phenyl and pyrimidine groups of neighbouring mol­ecules form mol­ecular chains parallel to [010]. Adjacent...

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Autores principales: Mohamed-Ezzat, Reham A., Kariuki, Benson M., Azzam, Rasha A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10088322/
https://www.ncbi.nlm.nih.gov/pubmed/37057009
http://dx.doi.org/10.1107/S2056989023001871
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author Mohamed-Ezzat, Reham A.
Kariuki, Benson M.
Azzam, Rasha A.
author_facet Mohamed-Ezzat, Reham A.
Kariuki, Benson M.
Azzam, Rasha A.
author_sort Mohamed-Ezzat, Reham A.
collection PubMed
description N-(5-Acetyl-4-methyl­pyrimidin-2-yl)benzene­sulfonamide, C(13)H(13)N(3)O(3)S, was sythesized and characterized by single-crystal X-ray diffraction. In the crystal, π–π inter­actions between the phenyl and pyrimidine groups of neighbouring mol­ecules form mol­ecular chains parallel to [010]. Adjacent mol­ecular chains are linked by N—H⋯N hydrogen-bonding inter­actions between the pyrimidine and amine groups of neighbouring mol­ecules, resulting in a three-dimensional network.
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spelling pubmed-100883222023-04-12 Synthesis and crystal structure of N-(5-acetyl-4-methyl­pyrimidin-2-yl)benzene­sulfonamide Mohamed-Ezzat, Reham A. Kariuki, Benson M. Azzam, Rasha A. Acta Crystallogr E Crystallogr Commun Research Communications N-(5-Acetyl-4-methyl­pyrimidin-2-yl)benzene­sulfonamide, C(13)H(13)N(3)O(3)S, was sythesized and characterized by single-crystal X-ray diffraction. In the crystal, π–π inter­actions between the phenyl and pyrimidine groups of neighbouring mol­ecules form mol­ecular chains parallel to [010]. Adjacent mol­ecular chains are linked by N—H⋯N hydrogen-bonding inter­actions between the pyrimidine and amine groups of neighbouring mol­ecules, resulting in a three-dimensional network. International Union of Crystallography 2023-03-15 /pmc/articles/PMC10088322/ /pubmed/37057009 http://dx.doi.org/10.1107/S2056989023001871 Text en © Mohamed-Ezzat et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Communications
Mohamed-Ezzat, Reham A.
Kariuki, Benson M.
Azzam, Rasha A.
Synthesis and crystal structure of N-(5-acetyl-4-methyl­pyrimidin-2-yl)benzene­sulfonamide
title Synthesis and crystal structure of N-(5-acetyl-4-methyl­pyrimidin-2-yl)benzene­sulfonamide
title_full Synthesis and crystal structure of N-(5-acetyl-4-methyl­pyrimidin-2-yl)benzene­sulfonamide
title_fullStr Synthesis and crystal structure of N-(5-acetyl-4-methyl­pyrimidin-2-yl)benzene­sulfonamide
title_full_unstemmed Synthesis and crystal structure of N-(5-acetyl-4-methyl­pyrimidin-2-yl)benzene­sulfonamide
title_short Synthesis and crystal structure of N-(5-acetyl-4-methyl­pyrimidin-2-yl)benzene­sulfonamide
title_sort synthesis and crystal structure of n-(5-acetyl-4-methyl­pyrimidin-2-yl)benzene­sulfonamide
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10088322/
https://www.ncbi.nlm.nih.gov/pubmed/37057009
http://dx.doi.org/10.1107/S2056989023001871
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