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Analysis of diffuse scattering in electron diffraction data for the crystal structure determination of Pigment Orange 13, C(32)H(24)Cl(2)N(8)O(2)

The crystallographic study of two polymorphs of the industrial pyrazolone Pigment Orange 13 (P.O.13) is reported. The crystal structure of the β phase was determined using single-crystal X-ray analysis of a tiny needle. The α phase was investigated using three-dimensional electron diffraction. The e...

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Detalles Bibliográficos
Autores principales: Gorelik, Tatiana E., Bekő, Sàndor L., Teteruk, Jaroslav, Heyse, Winfried, Schmidt, Martin U.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10088482/
https://www.ncbi.nlm.nih.gov/pubmed/36920875
http://dx.doi.org/10.1107/S2052520623000720