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Characterization of New Polymer Material of Amino-β-Cyclodextrin and Sodium Alginate for Environmental Purposes

The β-cyclodextrin polymer (PβCD) cross-linked with pyromellitic dianhydride (PD) and functionalized with an amino group (PAβCD) was introduced into a matrix made of sodium alginate (SA). Scanning electron microscopy (SEM) images showed a homogeneous surface of the composite material. Infrared spect...

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Autores principales: Kozieł-Trąbska, Kinga, Żarska, Sandra, Girek, Tomasz, Ciesielski, Wojciech
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10143267/
https://www.ncbi.nlm.nih.gov/pubmed/37103874
http://dx.doi.org/10.3390/membranes13040447
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author Kozieł-Trąbska, Kinga
Żarska, Sandra
Girek, Tomasz
Ciesielski, Wojciech
author_facet Kozieł-Trąbska, Kinga
Żarska, Sandra
Girek, Tomasz
Ciesielski, Wojciech
author_sort Kozieł-Trąbska, Kinga
collection PubMed
description The β-cyclodextrin polymer (PβCD) cross-linked with pyromellitic dianhydride (PD) and functionalized with an amino group (PAβCD) was introduced into a matrix made of sodium alginate (SA). Scanning electron microscopy (SEM) images showed a homogeneous surface of the composite material. Infrared spectroscopy (FTIR) testing of the PAβCD confirmed polymer formation. The tested polymer increased its solubility relative to the polymer without the amino group. Thermogravimetric analysis (TGA) confirmed the stability of the system. Differential scanning calorimetry (DSC) showed the chemical binding of PAβCD and SA. Gel permeation chromatography (GPC-SEC) showed high cross-linking of PAβCD and allowed for accurate determination of its weight. The formation of the composite material such as PAβCD introduced into a matrix made of sodium alginate (SA) has several potential environmental implications, including the use of sustainable materials, reduced waste generation, reduced toxicity, and improved solubility.
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spelling pubmed-101432672023-04-29 Characterization of New Polymer Material of Amino-β-Cyclodextrin and Sodium Alginate for Environmental Purposes Kozieł-Trąbska, Kinga Żarska, Sandra Girek, Tomasz Ciesielski, Wojciech Membranes (Basel) Article The β-cyclodextrin polymer (PβCD) cross-linked with pyromellitic dianhydride (PD) and functionalized with an amino group (PAβCD) was introduced into a matrix made of sodium alginate (SA). Scanning electron microscopy (SEM) images showed a homogeneous surface of the composite material. Infrared spectroscopy (FTIR) testing of the PAβCD confirmed polymer formation. The tested polymer increased its solubility relative to the polymer without the amino group. Thermogravimetric analysis (TGA) confirmed the stability of the system. Differential scanning calorimetry (DSC) showed the chemical binding of PAβCD and SA. Gel permeation chromatography (GPC-SEC) showed high cross-linking of PAβCD and allowed for accurate determination of its weight. The formation of the composite material such as PAβCD introduced into a matrix made of sodium alginate (SA) has several potential environmental implications, including the use of sustainable materials, reduced waste generation, reduced toxicity, and improved solubility. MDPI 2023-04-19 /pmc/articles/PMC10143267/ /pubmed/37103874 http://dx.doi.org/10.3390/membranes13040447 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Kozieł-Trąbska, Kinga
Żarska, Sandra
Girek, Tomasz
Ciesielski, Wojciech
Characterization of New Polymer Material of Amino-β-Cyclodextrin and Sodium Alginate for Environmental Purposes
title Characterization of New Polymer Material of Amino-β-Cyclodextrin and Sodium Alginate for Environmental Purposes
title_full Characterization of New Polymer Material of Amino-β-Cyclodextrin and Sodium Alginate for Environmental Purposes
title_fullStr Characterization of New Polymer Material of Amino-β-Cyclodextrin and Sodium Alginate for Environmental Purposes
title_full_unstemmed Characterization of New Polymer Material of Amino-β-Cyclodextrin and Sodium Alginate for Environmental Purposes
title_short Characterization of New Polymer Material of Amino-β-Cyclodextrin and Sodium Alginate for Environmental Purposes
title_sort characterization of new polymer material of amino-β-cyclodextrin and sodium alginate for environmental purposes
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10143267/
https://www.ncbi.nlm.nih.gov/pubmed/37103874
http://dx.doi.org/10.3390/membranes13040447
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