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Multi-Objective Optimization of Epoxy Resin Adhesive for Pavement Toughened by Self-Made Toughening Agent

Epoxy resin adhesive for pavement is often insufficient in flexibility and toughness. Therefore, a new type of toughening agent was prepared to overcome this shortcoming. To achieve the best toughening effect of a self-made toughening agent on an epoxy resin adhesive, its ratio to the epoxy resin ne...

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Autores principales: Ba, Huaiqiang, Guo, Luxin, Huan, Haiyang, Zhang, Shibo, Lin, Zhiwei
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10146785/
https://www.ncbi.nlm.nih.gov/pubmed/37112093
http://dx.doi.org/10.3390/polym15081946
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author Ba, Huaiqiang
Guo, Luxin
Huan, Haiyang
Zhang, Shibo
Lin, Zhiwei
author_facet Ba, Huaiqiang
Guo, Luxin
Huan, Haiyang
Zhang, Shibo
Lin, Zhiwei
author_sort Ba, Huaiqiang
collection PubMed
description Epoxy resin adhesive for pavement is often insufficient in flexibility and toughness. Therefore, a new type of toughening agent was prepared to overcome this shortcoming. To achieve the best toughening effect of a self-made toughening agent on an epoxy resin adhesive, its ratio to the epoxy resin needs to be optimally selected. A curing agent, a toughening agent, and an accelerator dosage were chosen as independent variables. The epoxy resin’s adhesive tensile strength, elongation at break, flexural strength, and flexural deflection were used as response values to establish a single-objective prediction model of epoxy resin mechanical property indexes. Response surface methodology (RSM) was used to determine the single-objective optimal ratio and analyze the effect of factor interaction on epoxy resin adhesive’s performance indexes. Based on principal component analysis (PCA), multi-objective optimization was performed using gray relational analysis (GRA) to construct a second-order regression prediction model between the ratio and gray relational grade (GRG) to determine the optimal ratio and to validate it. The results showed that the multi-objective optimization using response surface methodology and gray relational analysis (RSM-GRA) was more effective than the single-objective optimization model. The optimal ratio of epoxy resin adhesive was 100 parts of epoxy resin, 160.7 parts curing agent, 16.1 parts toughening agent, and 3.0 parts accelerator. The measured tensile strength was 10.75 MPa, elongation at break was 23.54%, the bending strength was 6.16 MPa, and the bending deflection was 7.15 mm. RSM-GRA has excellent accuracy for epoxy resin adhesive ratio optimization and can provide a reference for the epoxy resin system ratio optimization design of complex components.
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spelling pubmed-101467852023-04-29 Multi-Objective Optimization of Epoxy Resin Adhesive for Pavement Toughened by Self-Made Toughening Agent Ba, Huaiqiang Guo, Luxin Huan, Haiyang Zhang, Shibo Lin, Zhiwei Polymers (Basel) Article Epoxy resin adhesive for pavement is often insufficient in flexibility and toughness. Therefore, a new type of toughening agent was prepared to overcome this shortcoming. To achieve the best toughening effect of a self-made toughening agent on an epoxy resin adhesive, its ratio to the epoxy resin needs to be optimally selected. A curing agent, a toughening agent, and an accelerator dosage were chosen as independent variables. The epoxy resin’s adhesive tensile strength, elongation at break, flexural strength, and flexural deflection were used as response values to establish a single-objective prediction model of epoxy resin mechanical property indexes. Response surface methodology (RSM) was used to determine the single-objective optimal ratio and analyze the effect of factor interaction on epoxy resin adhesive’s performance indexes. Based on principal component analysis (PCA), multi-objective optimization was performed using gray relational analysis (GRA) to construct a second-order regression prediction model between the ratio and gray relational grade (GRG) to determine the optimal ratio and to validate it. The results showed that the multi-objective optimization using response surface methodology and gray relational analysis (RSM-GRA) was more effective than the single-objective optimization model. The optimal ratio of epoxy resin adhesive was 100 parts of epoxy resin, 160.7 parts curing agent, 16.1 parts toughening agent, and 3.0 parts accelerator. The measured tensile strength was 10.75 MPa, elongation at break was 23.54%, the bending strength was 6.16 MPa, and the bending deflection was 7.15 mm. RSM-GRA has excellent accuracy for epoxy resin adhesive ratio optimization and can provide a reference for the epoxy resin system ratio optimization design of complex components. MDPI 2023-04-19 /pmc/articles/PMC10146785/ /pubmed/37112093 http://dx.doi.org/10.3390/polym15081946 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Ba, Huaiqiang
Guo, Luxin
Huan, Haiyang
Zhang, Shibo
Lin, Zhiwei
Multi-Objective Optimization of Epoxy Resin Adhesive for Pavement Toughened by Self-Made Toughening Agent
title Multi-Objective Optimization of Epoxy Resin Adhesive for Pavement Toughened by Self-Made Toughening Agent
title_full Multi-Objective Optimization of Epoxy Resin Adhesive for Pavement Toughened by Self-Made Toughening Agent
title_fullStr Multi-Objective Optimization of Epoxy Resin Adhesive for Pavement Toughened by Self-Made Toughening Agent
title_full_unstemmed Multi-Objective Optimization of Epoxy Resin Adhesive for Pavement Toughened by Self-Made Toughening Agent
title_short Multi-Objective Optimization of Epoxy Resin Adhesive for Pavement Toughened by Self-Made Toughening Agent
title_sort multi-objective optimization of epoxy resin adhesive for pavement toughened by self-made toughening agent
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10146785/
https://www.ncbi.nlm.nih.gov/pubmed/37112093
http://dx.doi.org/10.3390/polym15081946
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