Photocatalytic setup for in situ and operando ambient-pressure X-ray photoelectron spectroscopy at MAX IV Laboratory

The Ambient-Pressure X-ray Photoelectron Spectroscopy (APXPS) endstation at the SPECIES beamline at MAX IV Laboratory has been improved. The latest upgrades help in performing photo-assisted experiments under operando conditions in the mbar pressure range using gas and vapour mixtures whilst also re...

Descripción completa

Detalles Bibliográficos
Autores principales: Klyushin, Alexander, Ghosalya, Manoj, Kokkonen, Esko, Eads, Calley, Jones, Rosemary, Nalajala, Naresh, Gopinath, Chinnakonda S., Urpelainen, Samuli
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Research Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10161884/
https://www.ncbi.nlm.nih.gov/pubmed/37067260
http://dx.doi.org/10.1107/S1600577523002801
_version_ 1785037588299513856
author Klyushin, Alexander
Ghosalya, Manoj
Kokkonen, Esko
Eads, Calley
Jones, Rosemary
Nalajala, Naresh
Gopinath, Chinnakonda S.
Urpelainen, Samuli
author_facet Klyushin, Alexander
Ghosalya, Manoj
Kokkonen, Esko
Eads, Calley
Jones, Rosemary
Nalajala, Naresh
Gopinath, Chinnakonda S.
Urpelainen, Samuli
author_sort Klyushin, Alexander
collection PubMed
description The Ambient-Pressure X-ray Photoelectron Spectroscopy (APXPS) endstation at the SPECIES beamline at MAX IV Laboratory has been improved. The latest upgrades help in performing photo-assisted experiments under operando conditions in the mbar pressure range using gas and vapour mixtures whilst also reducing beam damage to the sample caused by X-ray irradiation. This article reports on endstation upgrades for APXPS and examples of scientific cases of in situ photocatalysis, photoreduction and photo-assisted atomic layer deposition (photo-ALD).
format Online
Article
Text
id pubmed-10161884
institution National Center for Biotechnology Information
language English
publishDate 2023
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-101618842023-05-06 Photocatalytic setup for in situ and operando ambient-pressure X-ray photoelectron spectroscopy at MAX IV Laboratory Klyushin, Alexander Ghosalya, Manoj Kokkonen, Esko Eads, Calley Jones, Rosemary Nalajala, Naresh Gopinath, Chinnakonda S. Urpelainen, Samuli J Synchrotron Radiat Research Papers The Ambient-Pressure X-ray Photoelectron Spectroscopy (APXPS) endstation at the SPECIES beamline at MAX IV Laboratory has been improved. The latest upgrades help in performing photo-assisted experiments under operando conditions in the mbar pressure range using gas and vapour mixtures whilst also reducing beam damage to the sample caused by X-ray irradiation. This article reports on endstation upgrades for APXPS and examples of scientific cases of in situ photocatalysis, photoreduction and photo-assisted atomic layer deposition (photo-ALD). International Union of Crystallography 2023-04-17 /pmc/articles/PMC10161884/ /pubmed/37067260 http://dx.doi.org/10.1107/S1600577523002801 Text en © Alexander Klyushin et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Klyushin, Alexander
Ghosalya, Manoj
Kokkonen, Esko
Eads, Calley
Jones, Rosemary
Nalajala, Naresh
Gopinath, Chinnakonda S.
Urpelainen, Samuli
Photocatalytic setup for in situ and operando ambient-pressure X-ray photoelectron spectroscopy at MAX IV Laboratory
title Photocatalytic setup for in situ and operando ambient-pressure X-ray photoelectron spectroscopy at MAX IV Laboratory
title_full Photocatalytic setup for in situ and operando ambient-pressure X-ray photoelectron spectroscopy at MAX IV Laboratory
title_fullStr Photocatalytic setup for in situ and operando ambient-pressure X-ray photoelectron spectroscopy at MAX IV Laboratory
title_full_unstemmed Photocatalytic setup for in situ and operando ambient-pressure X-ray photoelectron spectroscopy at MAX IV Laboratory
title_short Photocatalytic setup for in situ and operando ambient-pressure X-ray photoelectron spectroscopy at MAX IV Laboratory
title_sort photocatalytic setup for in situ and operando ambient-pressure x-ray photoelectron spectroscopy at max iv laboratory
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10161884/
https://www.ncbi.nlm.nih.gov/pubmed/37067260
http://dx.doi.org/10.1107/S1600577523002801
work_keys_str_mv AT klyushinalexander photocatalyticsetupforinsituandoperandoambientpressurexrayphotoelectronspectroscopyatmaxivlaboratory
AT ghosalyamanoj photocatalyticsetupforinsituandoperandoambientpressurexrayphotoelectronspectroscopyatmaxivlaboratory
AT kokkonenesko photocatalyticsetupforinsituandoperandoambientpressurexrayphotoelectronspectroscopyatmaxivlaboratory
AT eadscalley photocatalyticsetupforinsituandoperandoambientpressurexrayphotoelectronspectroscopyatmaxivlaboratory
AT jonesrosemary photocatalyticsetupforinsituandoperandoambientpressurexrayphotoelectronspectroscopyatmaxivlaboratory
AT nalajalanaresh photocatalyticsetupforinsituandoperandoambientpressurexrayphotoelectronspectroscopyatmaxivlaboratory
AT gopinathchinnakondas photocatalyticsetupforinsituandoperandoambientpressurexrayphotoelectronspectroscopyatmaxivlaboratory
AT urpelainensamuli photocatalyticsetupforinsituandoperandoambientpressurexrayphotoelectronspectroscopyatmaxivlaboratory

Ejemplares similares