Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines

Photoelectrocatalytic (PEC) strategy has emerged as a promising approach to drive organic reactions under mild conditions. Here, we present a protocol for PEC oxidative coupling of aromatic amines to produce aromatic azo compounds over a porous BiVO(4) nanoarray (BiVO(4)-NA) photoanode. We describe...

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Detalles Bibliográficos
Autores principales: Luo, Lan, Liu, Yuguang, Chen, Wangsong, Zhang, Shanshan, Shao, Mingfei, Li, Zhenhua, Duan, Haohong
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2023
Materias:
Protocol
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10192644/
https://www.ncbi.nlm.nih.gov/pubmed/37182204
http://dx.doi.org/10.1016/j.xpro.2023.102311
Descripción
Sumario:Photoelectrocatalytic (PEC) strategy has emerged as a promising approach to drive organic reactions under mild conditions. Here, we present a protocol for PEC oxidative coupling of aromatic amines to produce aromatic azo compounds over a porous BiVO(4) nanoarray (BiVO(4)-NA) photoanode. We describe the fabrication of BiVO(4)-NA photoanode and the detailed steps for the PEC oxidative coupling reaction, including key performance data of the BiVO(4)-NA photoanode for synthesizing azobenzene from aniline. For complete details on the use and execution of this protocol, please refer to Luo et al. (2022).(1)

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