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Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines
Photoelectrocatalytic (PEC) strategy has emerged as a promising approach to drive organic reactions under mild conditions. Here, we present a protocol for PEC oxidative coupling of aromatic amines to produce aromatic azo compounds over a porous BiVO(4) nanoarray (BiVO(4)-NA) photoanode. We describe...
Autores principales: | , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Elsevier
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10192644/ https://www.ncbi.nlm.nih.gov/pubmed/37182204 http://dx.doi.org/10.1016/j.xpro.2023.102311 |
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author | Luo, Lan Liu, Yuguang Chen, Wangsong Zhang, Shanshan Shao, Mingfei Li, Zhenhua Duan, Haohong |
author_facet | Luo, Lan Liu, Yuguang Chen, Wangsong Zhang, Shanshan Shao, Mingfei Li, Zhenhua Duan, Haohong |
author_sort | Luo, Lan |
collection | PubMed |
description | Photoelectrocatalytic (PEC) strategy has emerged as a promising approach to drive organic reactions under mild conditions. Here, we present a protocol for PEC oxidative coupling of aromatic amines to produce aromatic azo compounds over a porous BiVO(4) nanoarray (BiVO(4)-NA) photoanode. We describe the fabrication of BiVO(4)-NA photoanode and the detailed steps for the PEC oxidative coupling reaction, including key performance data of the BiVO(4)-NA photoanode for synthesizing azobenzene from aniline. For complete details on the use and execution of this protocol, please refer to Luo et al. (2022).(1) |
format | Online Article Text |
id | pubmed-10192644 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | Elsevier |
record_format | MEDLINE/PubMed |
spelling | pubmed-101926442023-05-19 Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines Luo, Lan Liu, Yuguang Chen, Wangsong Zhang, Shanshan Shao, Mingfei Li, Zhenhua Duan, Haohong STAR Protoc Protocol Photoelectrocatalytic (PEC) strategy has emerged as a promising approach to drive organic reactions under mild conditions. Here, we present a protocol for PEC oxidative coupling of aromatic amines to produce aromatic azo compounds over a porous BiVO(4) nanoarray (BiVO(4)-NA) photoanode. We describe the fabrication of BiVO(4)-NA photoanode and the detailed steps for the PEC oxidative coupling reaction, including key performance data of the BiVO(4)-NA photoanode for synthesizing azobenzene from aniline. For complete details on the use and execution of this protocol, please refer to Luo et al. (2022).(1) Elsevier 2023-05-13 /pmc/articles/PMC10192644/ /pubmed/37182204 http://dx.doi.org/10.1016/j.xpro.2023.102311 Text en © 2023 The Author(s) https://creativecommons.org/licenses/by-nc-nd/4.0/This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/). |
spellingShingle | Protocol Luo, Lan Liu, Yuguang Chen, Wangsong Zhang, Shanshan Shao, Mingfei Li, Zhenhua Duan, Haohong Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines |
title | Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines |
title_full | Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines |
title_fullStr | Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines |
title_full_unstemmed | Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines |
title_short | Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines |
title_sort | protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines |
topic | Protocol |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10192644/ https://www.ncbi.nlm.nih.gov/pubmed/37182204 http://dx.doi.org/10.1016/j.xpro.2023.102311 |
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