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Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines

Photoelectrocatalytic (PEC) strategy has emerged as a promising approach to drive organic reactions under mild conditions. Here, we present a protocol for PEC oxidative coupling of aromatic amines to produce aromatic azo compounds over a porous BiVO(4) nanoarray (BiVO(4)-NA) photoanode. We describe...

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Detalles Bibliográficos
Autores principales: Luo, Lan, Liu, Yuguang, Chen, Wangsong, Zhang, Shanshan, Shao, Mingfei, Li, Zhenhua, Duan, Haohong
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10192644/
https://www.ncbi.nlm.nih.gov/pubmed/37182204
http://dx.doi.org/10.1016/j.xpro.2023.102311
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author Luo, Lan
Liu, Yuguang
Chen, Wangsong
Zhang, Shanshan
Shao, Mingfei
Li, Zhenhua
Duan, Haohong
author_facet Luo, Lan
Liu, Yuguang
Chen, Wangsong
Zhang, Shanshan
Shao, Mingfei
Li, Zhenhua
Duan, Haohong
author_sort Luo, Lan
collection PubMed
description Photoelectrocatalytic (PEC) strategy has emerged as a promising approach to drive organic reactions under mild conditions. Here, we present a protocol for PEC oxidative coupling of aromatic amines to produce aromatic azo compounds over a porous BiVO(4) nanoarray (BiVO(4)-NA) photoanode. We describe the fabrication of BiVO(4)-NA photoanode and the detailed steps for the PEC oxidative coupling reaction, including key performance data of the BiVO(4)-NA photoanode for synthesizing azobenzene from aniline. For complete details on the use and execution of this protocol, please refer to Luo et al. (2022).(1)
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spelling pubmed-101926442023-05-19 Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines Luo, Lan Liu, Yuguang Chen, Wangsong Zhang, Shanshan Shao, Mingfei Li, Zhenhua Duan, Haohong STAR Protoc Protocol Photoelectrocatalytic (PEC) strategy has emerged as a promising approach to drive organic reactions under mild conditions. Here, we present a protocol for PEC oxidative coupling of aromatic amines to produce aromatic azo compounds over a porous BiVO(4) nanoarray (BiVO(4)-NA) photoanode. We describe the fabrication of BiVO(4)-NA photoanode and the detailed steps for the PEC oxidative coupling reaction, including key performance data of the BiVO(4)-NA photoanode for synthesizing azobenzene from aniline. For complete details on the use and execution of this protocol, please refer to Luo et al. (2022).(1) Elsevier 2023-05-13 /pmc/articles/PMC10192644/ /pubmed/37182204 http://dx.doi.org/10.1016/j.xpro.2023.102311 Text en © 2023 The Author(s) https://creativecommons.org/licenses/by-nc-nd/4.0/This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
spellingShingle Protocol
Luo, Lan
Liu, Yuguang
Chen, Wangsong
Zhang, Shanshan
Shao, Mingfei
Li, Zhenhua
Duan, Haohong
Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines
title Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines
title_full Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines
title_fullStr Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines
title_full_unstemmed Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines
title_short Protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines
title_sort protocol for photoelectrocatalytic synthesis of aromatic azo compounds from aromatic amines
topic Protocol
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10192644/
https://www.ncbi.nlm.nih.gov/pubmed/37182204
http://dx.doi.org/10.1016/j.xpro.2023.102311
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