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Isolation of the isopropanol extract components of the leaves of Ailanthus glandulosa by a new method

The leaves of Ailanthus glandulosa were extracted with the Soxhlet apparatus using isopropanol. A new method was used to separate and isolate eleven chemical compounds present in the leaves of bird's tongue. The separation was carried out by column chromatography using displacement solvents (pe...

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Autor principal: Saad, Sawsan Youseff
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10192775/
https://www.ncbi.nlm.nih.gov/pubmed/37215867
http://dx.doi.org/10.1016/j.heliyon.2023.e15881
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author Saad, Sawsan Youseff
author_facet Saad, Sawsan Youseff
author_sort Saad, Sawsan Youseff
collection PubMed
description The leaves of Ailanthus glandulosa were extracted with the Soxhlet apparatus using isopropanol. A new method was used to separate and isolate eleven chemical compounds present in the leaves of bird's tongue. The separation was carried out by column chromatography using displacement solvents (petroleum ether, chloroform, dichloromethane, methanol) and four eluates were obtained. The four eluates were treated with a number of solvents, yielding thirty-four compounds. The chemical content of the mordants was determined using GC/MS technology. The samples tested contained six ester compounds, three aldehyde compounds, three ketone compounds, two alcoholic compounds, eight carboxylic acid compounds, five silicone compounds, five aromatic compounds and one phosphate compound. Eleven compounds were isolated, the most important of which are: 2-naphthoxyacetic acid, 2,6-bis (1,1-dimethylethyl)-4-ethylphenol, 2,5-tert-butylnitrobenzene, 5-hexyl-2-furaldehyde, 16-nitrobicyclo [10.4.0] hexadecan-1-ol-13-one, cyclooctasiloxan hexadecamethyl.
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spelling pubmed-101927752023-05-19 Isolation of the isopropanol extract components of the leaves of Ailanthus glandulosa by a new method Saad, Sawsan Youseff Heliyon Research Article The leaves of Ailanthus glandulosa were extracted with the Soxhlet apparatus using isopropanol. A new method was used to separate and isolate eleven chemical compounds present in the leaves of bird's tongue. The separation was carried out by column chromatography using displacement solvents (petroleum ether, chloroform, dichloromethane, methanol) and four eluates were obtained. The four eluates were treated with a number of solvents, yielding thirty-four compounds. The chemical content of the mordants was determined using GC/MS technology. The samples tested contained six ester compounds, three aldehyde compounds, three ketone compounds, two alcoholic compounds, eight carboxylic acid compounds, five silicone compounds, five aromatic compounds and one phosphate compound. Eleven compounds were isolated, the most important of which are: 2-naphthoxyacetic acid, 2,6-bis (1,1-dimethylethyl)-4-ethylphenol, 2,5-tert-butylnitrobenzene, 5-hexyl-2-furaldehyde, 16-nitrobicyclo [10.4.0] hexadecan-1-ol-13-one, cyclooctasiloxan hexadecamethyl. Elsevier 2023-04-30 /pmc/articles/PMC10192775/ /pubmed/37215867 http://dx.doi.org/10.1016/j.heliyon.2023.e15881 Text en © 2023 The Author https://creativecommons.org/licenses/by/4.0/This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Research Article
Saad, Sawsan Youseff
Isolation of the isopropanol extract components of the leaves of Ailanthus glandulosa by a new method
title Isolation of the isopropanol extract components of the leaves of Ailanthus glandulosa by a new method
title_full Isolation of the isopropanol extract components of the leaves of Ailanthus glandulosa by a new method
title_fullStr Isolation of the isopropanol extract components of the leaves of Ailanthus glandulosa by a new method
title_full_unstemmed Isolation of the isopropanol extract components of the leaves of Ailanthus glandulosa by a new method
title_short Isolation of the isopropanol extract components of the leaves of Ailanthus glandulosa by a new method
title_sort isolation of the isopropanol extract components of the leaves of ailanthus glandulosa by a new method
topic Research Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10192775/
https://www.ncbi.nlm.nih.gov/pubmed/37215867
http://dx.doi.org/10.1016/j.heliyon.2023.e15881
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