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Ball-milling synthesized Bi(2)VO(5.5) for piezo-photocatalytic assessment
The mechanochemical ball milling followed by heating at 650 °C for 5 h successfully produced the single-phase Bi(2)VO(5.5) powder. Catalytic activity for methylene blue dye degradation was investigated. Raman spectroscopy and X-ray diffraction were used to confirm the phase formation. The sample’s c...
Autores principales: | , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Nature Publishing Group UK
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10199923/ https://www.ncbi.nlm.nih.gov/pubmed/37210398 http://dx.doi.org/10.1038/s41598-023-33658-2 |
Sumario: | The mechanochemical ball milling followed by heating at 650 °C for 5 h successfully produced the single-phase Bi(2)VO(5.5) powder. Catalytic activity for methylene blue dye degradation was investigated. Raman spectroscopy and X-ray diffraction were used to confirm the phase formation. The sample’s charge carrier transportation behavior was ascertained using time-dependent photocurrent analysis. The piezo-photocatalysis experiment yielded a 63% degradation efficiency for the ball-milled Bi(2)VO(5.5) sample. The pseudo-first-order kinetics of the piezo-photocatalytic dye degradation are discerned, and the significant k value of 0.00529 min(−1) is achieved. The scavenger test declares the h(+) radical is the predominant active species during the piezo-photocatalysis experiment. Vigna radiata seeds were used in a phytotoxicity test to evaluate the germination index. The mechanochemical activation method facilitates reactions by lowering reaction temperature and time. The effect of improved piezo-photocatalytic efficiency on the ball-milled Bi(2)VO(5.5) powder is an unexplored area, and we have attempted to investigate it. Here, ball-milled Bi(2)VO(5.5) powder achieved improved dye degradation performance. |
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