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Ball-milling synthesized Bi(2)VO(5.5) for piezo-photocatalytic assessment
The mechanochemical ball milling followed by heating at 650 °C for 5 h successfully produced the single-phase Bi(2)VO(5.5) powder. Catalytic activity for methylene blue dye degradation was investigated. Raman spectroscopy and X-ray diffraction were used to confirm the phase formation. The sample’s c...
Autores principales: | , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
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Nature Publishing Group UK
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10199923/ https://www.ncbi.nlm.nih.gov/pubmed/37210398 http://dx.doi.org/10.1038/s41598-023-33658-2 |
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author | Kumar, Manish Vaish, Rahul Kebaili, Imen Boukhris, Imed Kwang Benno Park, Hyeong Hwan Joo, Yun Hyun Sung, Tae Kumar, Anuruddh |
author_facet | Kumar, Manish Vaish, Rahul Kebaili, Imen Boukhris, Imed Kwang Benno Park, Hyeong Hwan Joo, Yun Hyun Sung, Tae Kumar, Anuruddh |
author_sort | Kumar, Manish |
collection | PubMed |
description | The mechanochemical ball milling followed by heating at 650 °C for 5 h successfully produced the single-phase Bi(2)VO(5.5) powder. Catalytic activity for methylene blue dye degradation was investigated. Raman spectroscopy and X-ray diffraction were used to confirm the phase formation. The sample’s charge carrier transportation behavior was ascertained using time-dependent photocurrent analysis. The piezo-photocatalysis experiment yielded a 63% degradation efficiency for the ball-milled Bi(2)VO(5.5) sample. The pseudo-first-order kinetics of the piezo-photocatalytic dye degradation are discerned, and the significant k value of 0.00529 min(−1) is achieved. The scavenger test declares the h(+) radical is the predominant active species during the piezo-photocatalysis experiment. Vigna radiata seeds were used in a phytotoxicity test to evaluate the germination index. The mechanochemical activation method facilitates reactions by lowering reaction temperature and time. The effect of improved piezo-photocatalytic efficiency on the ball-milled Bi(2)VO(5.5) powder is an unexplored area, and we have attempted to investigate it. Here, ball-milled Bi(2)VO(5.5) powder achieved improved dye degradation performance. |
format | Online Article Text |
id | pubmed-10199923 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | Nature Publishing Group UK |
record_format | MEDLINE/PubMed |
spelling | pubmed-101999232023-05-22 Ball-milling synthesized Bi(2)VO(5.5) for piezo-photocatalytic assessment Kumar, Manish Vaish, Rahul Kebaili, Imen Boukhris, Imed Kwang Benno Park, Hyeong Hwan Joo, Yun Hyun Sung, Tae Kumar, Anuruddh Sci Rep Article The mechanochemical ball milling followed by heating at 650 °C for 5 h successfully produced the single-phase Bi(2)VO(5.5) powder. Catalytic activity for methylene blue dye degradation was investigated. Raman spectroscopy and X-ray diffraction were used to confirm the phase formation. The sample’s charge carrier transportation behavior was ascertained using time-dependent photocurrent analysis. The piezo-photocatalysis experiment yielded a 63% degradation efficiency for the ball-milled Bi(2)VO(5.5) sample. The pseudo-first-order kinetics of the piezo-photocatalytic dye degradation are discerned, and the significant k value of 0.00529 min(−1) is achieved. The scavenger test declares the h(+) radical is the predominant active species during the piezo-photocatalysis experiment. Vigna radiata seeds were used in a phytotoxicity test to evaluate the germination index. The mechanochemical activation method facilitates reactions by lowering reaction temperature and time. The effect of improved piezo-photocatalytic efficiency on the ball-milled Bi(2)VO(5.5) powder is an unexplored area, and we have attempted to investigate it. Here, ball-milled Bi(2)VO(5.5) powder achieved improved dye degradation performance. Nature Publishing Group UK 2023-05-20 /pmc/articles/PMC10199923/ /pubmed/37210398 http://dx.doi.org/10.1038/s41598-023-33658-2 Text en © The Author(s) 2023 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) . |
spellingShingle | Article Kumar, Manish Vaish, Rahul Kebaili, Imen Boukhris, Imed Kwang Benno Park, Hyeong Hwan Joo, Yun Hyun Sung, Tae Kumar, Anuruddh Ball-milling synthesized Bi(2)VO(5.5) for piezo-photocatalytic assessment |
title | Ball-milling synthesized Bi(2)VO(5.5) for piezo-photocatalytic assessment |
title_full | Ball-milling synthesized Bi(2)VO(5.5) for piezo-photocatalytic assessment |
title_fullStr | Ball-milling synthesized Bi(2)VO(5.5) for piezo-photocatalytic assessment |
title_full_unstemmed | Ball-milling synthesized Bi(2)VO(5.5) for piezo-photocatalytic assessment |
title_short | Ball-milling synthesized Bi(2)VO(5.5) for piezo-photocatalytic assessment |
title_sort | ball-milling synthesized bi(2)vo(5.5) for piezo-photocatalytic assessment |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10199923/ https://www.ncbi.nlm.nih.gov/pubmed/37210398 http://dx.doi.org/10.1038/s41598-023-33658-2 |
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