Influence of bimetal interface confinement on the Hall-petch slope of multiscale Cu/Nb multilayer composites

Heterostructured materials afford a new way to improve the mechanical properties, which has become vital in both materials science and engineering applications. In the present research, Cu/Nb multilayer composites with layer thicknesses from the micrometer to nanometer were fabricated by accumulative roll bonding and the microstructure and mechanical properties of the Cu/Nb multilayer composites were then investigated. The yield strength and ultimate tensile strength of these composites increase with decreasing layer thickness. Moreover, the relationship between yield strength and (layer thickness)(−1/2) approximately accords with the conventional Hall-Petch equation but with a decrease in the Hall-Petch slope when the layer thickness decreases from the micrometer to nanometer scales. The deformation microstructure of these Cu/Nb multilayer composites clearly exhibit dislocations glide in the layers, which reduces the stacking of dislocations at the Cu–Nb interface and thereby weakens the strengthening effect of the interface.