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Fe(3)O(4)@iron-based metal–organic framework nanocomposite [Fe(3)O(4)@MOF (Fe) NC] as a recyclable magnetic nano-organocatalyst for the environment-friendly synthesis of pyrano[2,3-d]pyrimidine derivatives
Various pyrano[2,3-d]pyrimidines were synthesized by the multicomponent reaction of aldehydes, malononitrile, and acidic C–H compounds such as barbituric acid through the tandem Knoevenagel–Michael cyclocondensation pathway in an environmentally friendly reactive medium in the presence of a recovera...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
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Frontiers Media S.A.
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10225664/ https://www.ncbi.nlm.nih.gov/pubmed/37255544 http://dx.doi.org/10.3389/fchem.2023.1193080 |
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author | Hootifard, Ghader Sheikhhosseini, Enayatollah Ahmadi, Sayed Ali Yahyazadehfar, Mahdieh |
author_facet | Hootifard, Ghader Sheikhhosseini, Enayatollah Ahmadi, Sayed Ali Yahyazadehfar, Mahdieh |
author_sort | Hootifard, Ghader |
collection | PubMed |
description | Various pyrano[2,3-d]pyrimidines were synthesized by the multicomponent reaction of aldehydes, malononitrile, and acidic C–H compounds such as barbituric acid through the tandem Knoevenagel–Michael cyclocondensation pathway in an environmentally friendly reactive medium in the presence of a recoverable nanocomposite. This nanocomposite includes Fe(3)O(4) nanoparticles placed on an organometallic framework. The synthesized Fe(3)O(4)@iron-based metal–organic framework nanocomposite was characterized using scanning electron microscopy, energy dispersive X-ray spectroscopy, X-ray powder diffraction, a vibrating sample magnetometer, and thermogravimetric analysis. |
format | Online Article Text |
id | pubmed-10225664 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | Frontiers Media S.A. |
record_format | MEDLINE/PubMed |
spelling | pubmed-102256642023-05-30 Fe(3)O(4)@iron-based metal–organic framework nanocomposite [Fe(3)O(4)@MOF (Fe) NC] as a recyclable magnetic nano-organocatalyst for the environment-friendly synthesis of pyrano[2,3-d]pyrimidine derivatives Hootifard, Ghader Sheikhhosseini, Enayatollah Ahmadi, Sayed Ali Yahyazadehfar, Mahdieh Front Chem Chemistry Various pyrano[2,3-d]pyrimidines were synthesized by the multicomponent reaction of aldehydes, malononitrile, and acidic C–H compounds such as barbituric acid through the tandem Knoevenagel–Michael cyclocondensation pathway in an environmentally friendly reactive medium in the presence of a recoverable nanocomposite. This nanocomposite includes Fe(3)O(4) nanoparticles placed on an organometallic framework. The synthesized Fe(3)O(4)@iron-based metal–organic framework nanocomposite was characterized using scanning electron microscopy, energy dispersive X-ray spectroscopy, X-ray powder diffraction, a vibrating sample magnetometer, and thermogravimetric analysis. Frontiers Media S.A. 2023-05-15 /pmc/articles/PMC10225664/ /pubmed/37255544 http://dx.doi.org/10.3389/fchem.2023.1193080 Text en Copyright © 2023 Hootifard, Sheikhhosseini, Ahmadi and Yahyazadehfar. https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution License (CC BY). The use, distribution or reproduction in other forums is permitted, provided the original author(s) and the copyright owner(s) are credited and that the original publication in this journal is cited, in accordance with accepted academic practice. No use, distribution or reproduction is permitted which does not comply with these terms. |
spellingShingle | Chemistry Hootifard, Ghader Sheikhhosseini, Enayatollah Ahmadi, Sayed Ali Yahyazadehfar, Mahdieh Fe(3)O(4)@iron-based metal–organic framework nanocomposite [Fe(3)O(4)@MOF (Fe) NC] as a recyclable magnetic nano-organocatalyst for the environment-friendly synthesis of pyrano[2,3-d]pyrimidine derivatives |
title | Fe(3)O(4)@iron-based metal–organic framework nanocomposite [Fe(3)O(4)@MOF (Fe) NC] as a recyclable magnetic nano-organocatalyst for the environment-friendly synthesis of pyrano[2,3-d]pyrimidine derivatives |
title_full | Fe(3)O(4)@iron-based metal–organic framework nanocomposite [Fe(3)O(4)@MOF (Fe) NC] as a recyclable magnetic nano-organocatalyst for the environment-friendly synthesis of pyrano[2,3-d]pyrimidine derivatives |
title_fullStr | Fe(3)O(4)@iron-based metal–organic framework nanocomposite [Fe(3)O(4)@MOF (Fe) NC] as a recyclable magnetic nano-organocatalyst for the environment-friendly synthesis of pyrano[2,3-d]pyrimidine derivatives |
title_full_unstemmed | Fe(3)O(4)@iron-based metal–organic framework nanocomposite [Fe(3)O(4)@MOF (Fe) NC] as a recyclable magnetic nano-organocatalyst for the environment-friendly synthesis of pyrano[2,3-d]pyrimidine derivatives |
title_short | Fe(3)O(4)@iron-based metal–organic framework nanocomposite [Fe(3)O(4)@MOF (Fe) NC] as a recyclable magnetic nano-organocatalyst for the environment-friendly synthesis of pyrano[2,3-d]pyrimidine derivatives |
title_sort | fe(3)o(4)@iron-based metal–organic framework nanocomposite [fe(3)o(4)@mof (fe) nc] as a recyclable magnetic nano-organocatalyst for the environment-friendly synthesis of pyrano[2,3-d]pyrimidine derivatives |
topic | Chemistry |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10225664/ https://www.ncbi.nlm.nih.gov/pubmed/37255544 http://dx.doi.org/10.3389/fchem.2023.1193080 |
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