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An efficient protocol for the synthesis of pyridines and hydroquinolones using IRMOF-3/GO/CuFe(2)O(4) composite as a magnetically separable heterogeneous catalyst

This study reports a facile and cost-effective technique for preparing magnetic copper ferrite nanoparticles supported on IRMOF-3/GO [IRMOF-3/GO/CuFe(2)O(4)]. The synthesized IRMOF-3/GO/CuFe(2)O(4) was characterized with IR, SEM, TGA, XRD, BET, EDX, VSM, and elemental mapping. The prepared catalyst...

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Autores principales: Ghasemzadeh, Mohammad Ali, Mirhosseini-Eshkevari, Boshra, Dadashi, Jaber
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10241797/
https://www.ncbi.nlm.nih.gov/pubmed/37277460
http://dx.doi.org/10.1038/s41598-023-36115-2
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author Ghasemzadeh, Mohammad Ali
Mirhosseini-Eshkevari, Boshra
Dadashi, Jaber
author_facet Ghasemzadeh, Mohammad Ali
Mirhosseini-Eshkevari, Boshra
Dadashi, Jaber
author_sort Ghasemzadeh, Mohammad Ali
collection PubMed
description This study reports a facile and cost-effective technique for preparing magnetic copper ferrite nanoparticles supported on IRMOF-3/GO [IRMOF-3/GO/CuFe(2)O(4)]. The synthesized IRMOF-3/GO/CuFe(2)O(4) was characterized with IR, SEM, TGA, XRD, BET, EDX, VSM, and elemental mapping. The prepared catalyst revealed higher catalytic behavior in synthesizing heterocyclic compounds through a one-pot reaction between various aromatic aldehydes, diverse primary amines, malononitrile, and dimedone under ultrasound irradiations. Among the notable features of this technique are higher efficiency, easy recovery from the reaction mixture, removal of a heterogeneous catalyst, and uncomplicated route. In this catalytic system, the activity level was almost constant after various stages of reuse and recovery.
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spelling pubmed-102417972023-06-07 An efficient protocol for the synthesis of pyridines and hydroquinolones using IRMOF-3/GO/CuFe(2)O(4) composite as a magnetically separable heterogeneous catalyst Ghasemzadeh, Mohammad Ali Mirhosseini-Eshkevari, Boshra Dadashi, Jaber Sci Rep Article This study reports a facile and cost-effective technique for preparing magnetic copper ferrite nanoparticles supported on IRMOF-3/GO [IRMOF-3/GO/CuFe(2)O(4)]. The synthesized IRMOF-3/GO/CuFe(2)O(4) was characterized with IR, SEM, TGA, XRD, BET, EDX, VSM, and elemental mapping. The prepared catalyst revealed higher catalytic behavior in synthesizing heterocyclic compounds through a one-pot reaction between various aromatic aldehydes, diverse primary amines, malononitrile, and dimedone under ultrasound irradiations. Among the notable features of this technique are higher efficiency, easy recovery from the reaction mixture, removal of a heterogeneous catalyst, and uncomplicated route. In this catalytic system, the activity level was almost constant after various stages of reuse and recovery. Nature Publishing Group UK 2023-06-05 /pmc/articles/PMC10241797/ /pubmed/37277460 http://dx.doi.org/10.1038/s41598-023-36115-2 Text en © The Author(s) 2023 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Article
Ghasemzadeh, Mohammad Ali
Mirhosseini-Eshkevari, Boshra
Dadashi, Jaber
An efficient protocol for the synthesis of pyridines and hydroquinolones using IRMOF-3/GO/CuFe(2)O(4) composite as a magnetically separable heterogeneous catalyst
title An efficient protocol for the synthesis of pyridines and hydroquinolones using IRMOF-3/GO/CuFe(2)O(4) composite as a magnetically separable heterogeneous catalyst
title_full An efficient protocol for the synthesis of pyridines and hydroquinolones using IRMOF-3/GO/CuFe(2)O(4) composite as a magnetically separable heterogeneous catalyst
title_fullStr An efficient protocol for the synthesis of pyridines and hydroquinolones using IRMOF-3/GO/CuFe(2)O(4) composite as a magnetically separable heterogeneous catalyst
title_full_unstemmed An efficient protocol for the synthesis of pyridines and hydroquinolones using IRMOF-3/GO/CuFe(2)O(4) composite as a magnetically separable heterogeneous catalyst
title_short An efficient protocol for the synthesis of pyridines and hydroquinolones using IRMOF-3/GO/CuFe(2)O(4) composite as a magnetically separable heterogeneous catalyst
title_sort efficient protocol for the synthesis of pyridines and hydroquinolones using irmof-3/go/cufe(2)o(4) composite as a magnetically separable heterogeneous catalyst
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10241797/
https://www.ncbi.nlm.nih.gov/pubmed/37277460
http://dx.doi.org/10.1038/s41598-023-36115-2
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