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Microstructure and Mechanical Characterization of Novel Al(2)O(3)–(NiAl–Al(2)O(3)) Composites Fabricated via Pulse Plasma Sintering
The scientific goal of this paper is to study and explain the relationship between the microstructure of a ceramic–intermetallic composite fabricated by consolidating a mixture of Al(2)O(3) and NiAl-Al(2)O(3) using the PPS technique and its basic mechanical properties. Six series of composites were...
Autores principales: | , , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10254161/ https://www.ncbi.nlm.nih.gov/pubmed/37297271 http://dx.doi.org/10.3390/ma16114136 |
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author | Zygmuntowicz, Justyna Konopka, Katarzyna Krasnowski, Marek Piotrkiewicz, Paulina Wachowski, Marcin Żurowski, Radosław Cymerman, Konrad Kulikowski, Krzysztof Sobiecki, Robert |
author_facet | Zygmuntowicz, Justyna Konopka, Katarzyna Krasnowski, Marek Piotrkiewicz, Paulina Wachowski, Marcin Żurowski, Radosław Cymerman, Konrad Kulikowski, Krzysztof Sobiecki, Robert |
author_sort | Zygmuntowicz, Justyna |
collection | PubMed |
description | The scientific goal of this paper is to study and explain the relationship between the microstructure of a ceramic–intermetallic composite fabricated by consolidating a mixture of Al(2)O(3) and NiAl-Al(2)O(3) using the PPS technique and its basic mechanical properties. Six series of composites were manufactured. The obtained samples differed in the sintering temperature and content of compo-powder. The base powders, compo-powder, and composites were investigated using SEM equipped with an EDS and XRD. Hardness tests and K(IC) measurements were applied to estimate the mechanical properties of the fabricated composites. The wear resistance was evaluated using a “ball-on-disc” method. The results demonstrate that the density of the obtained composites increases with the increased temperature of the sintering. The content of NiAl + 20 wt.% Al(2)O(3) did not have a determining effect on the hardness of the manufactured composites. The highest hardness, contacting 20.9 ± 0.8 GPa, was found for the composite series sintered at 1300 °C and 2.5 vol.% of compo-powder. The highest K(IC) value from all the studied series equaled 8.13 ± 0.55 MPa·m(0.5) and was also achieved for the series manufactured at 1300 °C (2.5 vol.% of compo-powder). The average friction coefficient during the ball-friction test with the Si(3)N(4) ceramic counter-sample was between 0.8 and 0.95. |
format | Online Article Text |
id | pubmed-10254161 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-102541612023-06-10 Microstructure and Mechanical Characterization of Novel Al(2)O(3)–(NiAl–Al(2)O(3)) Composites Fabricated via Pulse Plasma Sintering Zygmuntowicz, Justyna Konopka, Katarzyna Krasnowski, Marek Piotrkiewicz, Paulina Wachowski, Marcin Żurowski, Radosław Cymerman, Konrad Kulikowski, Krzysztof Sobiecki, Robert Materials (Basel) Article The scientific goal of this paper is to study and explain the relationship between the microstructure of a ceramic–intermetallic composite fabricated by consolidating a mixture of Al(2)O(3) and NiAl-Al(2)O(3) using the PPS technique and its basic mechanical properties. Six series of composites were manufactured. The obtained samples differed in the sintering temperature and content of compo-powder. The base powders, compo-powder, and composites were investigated using SEM equipped with an EDS and XRD. Hardness tests and K(IC) measurements were applied to estimate the mechanical properties of the fabricated composites. The wear resistance was evaluated using a “ball-on-disc” method. The results demonstrate that the density of the obtained composites increases with the increased temperature of the sintering. The content of NiAl + 20 wt.% Al(2)O(3) did not have a determining effect on the hardness of the manufactured composites. The highest hardness, contacting 20.9 ± 0.8 GPa, was found for the composite series sintered at 1300 °C and 2.5 vol.% of compo-powder. The highest K(IC) value from all the studied series equaled 8.13 ± 0.55 MPa·m(0.5) and was also achieved for the series manufactured at 1300 °C (2.5 vol.% of compo-powder). The average friction coefficient during the ball-friction test with the Si(3)N(4) ceramic counter-sample was between 0.8 and 0.95. MDPI 2023-06-01 /pmc/articles/PMC10254161/ /pubmed/37297271 http://dx.doi.org/10.3390/ma16114136 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Zygmuntowicz, Justyna Konopka, Katarzyna Krasnowski, Marek Piotrkiewicz, Paulina Wachowski, Marcin Żurowski, Radosław Cymerman, Konrad Kulikowski, Krzysztof Sobiecki, Robert Microstructure and Mechanical Characterization of Novel Al(2)O(3)–(NiAl–Al(2)O(3)) Composites Fabricated via Pulse Plasma Sintering |
title | Microstructure and Mechanical Characterization of Novel Al(2)O(3)–(NiAl–Al(2)O(3)) Composites Fabricated via Pulse Plasma Sintering |
title_full | Microstructure and Mechanical Characterization of Novel Al(2)O(3)–(NiAl–Al(2)O(3)) Composites Fabricated via Pulse Plasma Sintering |
title_fullStr | Microstructure and Mechanical Characterization of Novel Al(2)O(3)–(NiAl–Al(2)O(3)) Composites Fabricated via Pulse Plasma Sintering |
title_full_unstemmed | Microstructure and Mechanical Characterization of Novel Al(2)O(3)–(NiAl–Al(2)O(3)) Composites Fabricated via Pulse Plasma Sintering |
title_short | Microstructure and Mechanical Characterization of Novel Al(2)O(3)–(NiAl–Al(2)O(3)) Composites Fabricated via Pulse Plasma Sintering |
title_sort | microstructure and mechanical characterization of novel al(2)o(3)–(nial–al(2)o(3)) composites fabricated via pulse plasma sintering |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10254161/ https://www.ncbi.nlm.nih.gov/pubmed/37297271 http://dx.doi.org/10.3390/ma16114136 |
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