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Direct Fabrication of a Copper RTD over a Ceramic-Coated Stainless-Steel Tube by Combination of Magnetron Sputtering and Sol–Gel Techniques

Reducing the economic and environmental impact of industrial process may be achieved by the smartisation of different components. In this work, tube smartisation is presented via direct fabrication of a copper (Cu)-based resistive temperature detector (RTD) on their outer surfaces. The testing was c...

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Autores principales: Bikarregi, Aitor, Dominguez, Santiago, Brizuela, Marta, López, Alejandra, Suarez-Vega, Ana, Agustín-Sáenz, Cecilia, Presa, Micael, López, Gabriel A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10301088/
https://www.ncbi.nlm.nih.gov/pubmed/37420609
http://dx.doi.org/10.3390/s23125442
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author Bikarregi, Aitor
Dominguez, Santiago
Brizuela, Marta
López, Alejandra
Suarez-Vega, Ana
Agustín-Sáenz, Cecilia
Presa, Micael
López, Gabriel A.
author_facet Bikarregi, Aitor
Dominguez, Santiago
Brizuela, Marta
López, Alejandra
Suarez-Vega, Ana
Agustín-Sáenz, Cecilia
Presa, Micael
López, Gabriel A.
author_sort Bikarregi, Aitor
collection PubMed
description Reducing the economic and environmental impact of industrial process may be achieved by the smartisation of different components. In this work, tube smartisation is presented via direct fabrication of a copper (Cu)-based resistive temperature detector (RTD) on their outer surfaces. The testing was carried out between room temperature and 250 °C. For this purpose, copper depositions were studied using mid-frequency (MF) and high-power impulse magnetron sputtering (HiPIMS). Stainless steel tubes with an outside inert ceramic coating were used after giving them a shot blasting treatment. The Cu deposition was performed at around 425 °C to improve adhesion as well as the electrical properties of the sensor. To generate the pattern of the Cu RTD, a photolithography process was carried out. The RTD was then protected from external degradation by a silicon oxide film deposited over it by means of two different techniques: sol–gel dipping technique and reactive magnetron sputtering. For the electrical characterisation of the sensor, an ad hoc test bench was used, based on the internal heating and the external temperature measurement with a thermographic camera. The results confirm the linearity (R(2) > 0.999) and repeatability in the electrical properties of the copper RTD (confidence interval < 0.0005).
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spelling pubmed-103010882023-06-29 Direct Fabrication of a Copper RTD over a Ceramic-Coated Stainless-Steel Tube by Combination of Magnetron Sputtering and Sol–Gel Techniques Bikarregi, Aitor Dominguez, Santiago Brizuela, Marta López, Alejandra Suarez-Vega, Ana Agustín-Sáenz, Cecilia Presa, Micael López, Gabriel A. Sensors (Basel) Article Reducing the economic and environmental impact of industrial process may be achieved by the smartisation of different components. In this work, tube smartisation is presented via direct fabrication of a copper (Cu)-based resistive temperature detector (RTD) on their outer surfaces. The testing was carried out between room temperature and 250 °C. For this purpose, copper depositions were studied using mid-frequency (MF) and high-power impulse magnetron sputtering (HiPIMS). Stainless steel tubes with an outside inert ceramic coating were used after giving them a shot blasting treatment. The Cu deposition was performed at around 425 °C to improve adhesion as well as the electrical properties of the sensor. To generate the pattern of the Cu RTD, a photolithography process was carried out. The RTD was then protected from external degradation by a silicon oxide film deposited over it by means of two different techniques: sol–gel dipping technique and reactive magnetron sputtering. For the electrical characterisation of the sensor, an ad hoc test bench was used, based on the internal heating and the external temperature measurement with a thermographic camera. The results confirm the linearity (R(2) > 0.999) and repeatability in the electrical properties of the copper RTD (confidence interval < 0.0005). MDPI 2023-06-08 /pmc/articles/PMC10301088/ /pubmed/37420609 http://dx.doi.org/10.3390/s23125442 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Bikarregi, Aitor
Dominguez, Santiago
Brizuela, Marta
López, Alejandra
Suarez-Vega, Ana
Agustín-Sáenz, Cecilia
Presa, Micael
López, Gabriel A.
Direct Fabrication of a Copper RTD over a Ceramic-Coated Stainless-Steel Tube by Combination of Magnetron Sputtering and Sol–Gel Techniques
title Direct Fabrication of a Copper RTD over a Ceramic-Coated Stainless-Steel Tube by Combination of Magnetron Sputtering and Sol–Gel Techniques
title_full Direct Fabrication of a Copper RTD over a Ceramic-Coated Stainless-Steel Tube by Combination of Magnetron Sputtering and Sol–Gel Techniques
title_fullStr Direct Fabrication of a Copper RTD over a Ceramic-Coated Stainless-Steel Tube by Combination of Magnetron Sputtering and Sol–Gel Techniques
title_full_unstemmed Direct Fabrication of a Copper RTD over a Ceramic-Coated Stainless-Steel Tube by Combination of Magnetron Sputtering and Sol–Gel Techniques
title_short Direct Fabrication of a Copper RTD over a Ceramic-Coated Stainless-Steel Tube by Combination of Magnetron Sputtering and Sol–Gel Techniques
title_sort direct fabrication of a copper rtd over a ceramic-coated stainless-steel tube by combination of magnetron sputtering and sol–gel techniques
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10301088/
https://www.ncbi.nlm.nih.gov/pubmed/37420609
http://dx.doi.org/10.3390/s23125442
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