Cargando…

Meniscus-Corrected Method for Broadband Liquid Permittivity Measurements with an Uncalibrated Vector Network Analyzer

We present a novel broadband permittivity characterization method for liquids measured in a semi-open vertically oriented test cell with an uncalibrated vector network analyzer. For this goal, we utilize three scattering matrices measured at different levels of liquid in the cell. With mathematical...

Descripción completa

Detalles Bibliográficos
Autores principales: Kalisiak, Michał, Lewandowski, Arkadiusz, Wiatr, Wojciech
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10302224/
https://www.ncbi.nlm.nih.gov/pubmed/37420567
http://dx.doi.org/10.3390/s23125401
_version_ 1785064996290428928
author Kalisiak, Michał
Lewandowski, Arkadiusz
Wiatr, Wojciech
author_facet Kalisiak, Michał
Lewandowski, Arkadiusz
Wiatr, Wojciech
author_sort Kalisiak, Michał
collection PubMed
description We present a novel broadband permittivity characterization method for liquids measured in a semi-open vertically oriented test cell with an uncalibrated vector network analyzer. For this goal, we utilize three scattering matrices measured at different levels of liquid in the cell. With mathematical operations, we remove the effects of systematic measurement errors caused by both the vector network analyzer and a meniscus shaping the top of the liquid samples in such a type of test cell. To the best authors’ knowledge, this is the first of such a calibration-independent method dealing with meniscus. We verify its validity by comparing our results with the data available in the literature and with the outcomes of our previously published calibration-dependent meniscus removal method (MR) for propan-2-ol (IPA), a 50% aqueous solution of IPA and distilled water. The new method yields results comparable with the MR method, at least for IPA and the IPA solution, revealing, however some problems when testing high-loss water samples. Nevertheless, it allows one to cut down on expenditures in the system calibration engaging skilled labor and expensive standards.
format Online
Article
Text
id pubmed-10302224
institution National Center for Biotechnology Information
language English
publishDate 2023
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-103022242023-06-29 Meniscus-Corrected Method for Broadband Liquid Permittivity Measurements with an Uncalibrated Vector Network Analyzer Kalisiak, Michał Lewandowski, Arkadiusz Wiatr, Wojciech Sensors (Basel) Article We present a novel broadband permittivity characterization method for liquids measured in a semi-open vertically oriented test cell with an uncalibrated vector network analyzer. For this goal, we utilize three scattering matrices measured at different levels of liquid in the cell. With mathematical operations, we remove the effects of systematic measurement errors caused by both the vector network analyzer and a meniscus shaping the top of the liquid samples in such a type of test cell. To the best authors’ knowledge, this is the first of such a calibration-independent method dealing with meniscus. We verify its validity by comparing our results with the data available in the literature and with the outcomes of our previously published calibration-dependent meniscus removal method (MR) for propan-2-ol (IPA), a 50% aqueous solution of IPA and distilled water. The new method yields results comparable with the MR method, at least for IPA and the IPA solution, revealing, however some problems when testing high-loss water samples. Nevertheless, it allows one to cut down on expenditures in the system calibration engaging skilled labor and expensive standards. MDPI 2023-06-07 /pmc/articles/PMC10302224/ /pubmed/37420567 http://dx.doi.org/10.3390/s23125401 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Kalisiak, Michał
Lewandowski, Arkadiusz
Wiatr, Wojciech
Meniscus-Corrected Method for Broadband Liquid Permittivity Measurements with an Uncalibrated Vector Network Analyzer
title Meniscus-Corrected Method for Broadband Liquid Permittivity Measurements with an Uncalibrated Vector Network Analyzer
title_full Meniscus-Corrected Method for Broadband Liquid Permittivity Measurements with an Uncalibrated Vector Network Analyzer
title_fullStr Meniscus-Corrected Method for Broadband Liquid Permittivity Measurements with an Uncalibrated Vector Network Analyzer
title_full_unstemmed Meniscus-Corrected Method for Broadband Liquid Permittivity Measurements with an Uncalibrated Vector Network Analyzer
title_short Meniscus-Corrected Method for Broadband Liquid Permittivity Measurements with an Uncalibrated Vector Network Analyzer
title_sort meniscus-corrected method for broadband liquid permittivity measurements with an uncalibrated vector network analyzer
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10302224/
https://www.ncbi.nlm.nih.gov/pubmed/37420567
http://dx.doi.org/10.3390/s23125401
work_keys_str_mv AT kalisiakmichał meniscuscorrectedmethodforbroadbandliquidpermittivitymeasurementswithanuncalibratedvectornetworkanalyzer
AT lewandowskiarkadiusz meniscuscorrectedmethodforbroadbandliquidpermittivitymeasurementswithanuncalibratedvectornetworkanalyzer
AT wiatrwojciech meniscuscorrectedmethodforbroadbandliquidpermittivitymeasurementswithanuncalibratedvectornetworkanalyzer