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Design of Ti64/Ta Hybrid Materials by Powder Metallurgy Mimicking Bone Structure

This work reports on the fabrication of a novel two-layer material composed of a porous tantalum core and a dense Ti6Al4V (Ti64) shell by powder metallurgy. The porous core was obtained by mixing Ta particles and salt space-holders to create large pores, the green compact was obtained by pressing. T...

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Autores principales: Alvarado-Hernández, Francisco, Mihalcea, Elena, Jimenez, Omar, Macías, Rogelio, Olmos, Luis, López-Baltazar, Enrique A., Guevara-Martinez, Santiago, Lemus-Ruiz, José
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10302576/
https://www.ncbi.nlm.nih.gov/pubmed/37374557
http://dx.doi.org/10.3390/ma16124372
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author Alvarado-Hernández, Francisco
Mihalcea, Elena
Jimenez, Omar
Macías, Rogelio
Olmos, Luis
López-Baltazar, Enrique A.
Guevara-Martinez, Santiago
Lemus-Ruiz, José
author_facet Alvarado-Hernández, Francisco
Mihalcea, Elena
Jimenez, Omar
Macías, Rogelio
Olmos, Luis
López-Baltazar, Enrique A.
Guevara-Martinez, Santiago
Lemus-Ruiz, José
author_sort Alvarado-Hernández, Francisco
collection PubMed
description This work reports on the fabrication of a novel two-layer material composed of a porous tantalum core and a dense Ti6Al4V (Ti64) shell by powder metallurgy. The porous core was obtained by mixing Ta particles and salt space-holders to create large pores, the green compact was obtained by pressing. The sintering behavior of the two-layer sample was studied by dilatometry. The interface bonding between the Ti64 and Ta layers was analyzed by SEM, and the pore characteristics were analyzed by computed microtomography. Images showed that two distinct layers were obtained with a bonding achieved by the solid-state diffusion of Ta particles into Ti64 during sintering. The formation of β-Ti and α′ martensitic phases confirmed the diffusion of Ta. The pore size distribution was in the size range of 80 to 500 µm, and a permeability value of 6 × 10(−10) m(2) was close to the trabecular bones one. The mechanical properties of the component were dominated mainly by the porous layer, and Young’s modulus of 16 GPa was in the range of bones. Additionally, the density of this material (6 g/cm(3)) was much lower than the one of pure Ta, which helps to reduce the weight for the desired applications. These results indicate that structurally hybridized materials, also known as composites, with specific property profiles can improve the response to osseointegration for bone implant applications.
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spelling pubmed-103025762023-06-29 Design of Ti64/Ta Hybrid Materials by Powder Metallurgy Mimicking Bone Structure Alvarado-Hernández, Francisco Mihalcea, Elena Jimenez, Omar Macías, Rogelio Olmos, Luis López-Baltazar, Enrique A. Guevara-Martinez, Santiago Lemus-Ruiz, José Materials (Basel) Article This work reports on the fabrication of a novel two-layer material composed of a porous tantalum core and a dense Ti6Al4V (Ti64) shell by powder metallurgy. The porous core was obtained by mixing Ta particles and salt space-holders to create large pores, the green compact was obtained by pressing. The sintering behavior of the two-layer sample was studied by dilatometry. The interface bonding between the Ti64 and Ta layers was analyzed by SEM, and the pore characteristics were analyzed by computed microtomography. Images showed that two distinct layers were obtained with a bonding achieved by the solid-state diffusion of Ta particles into Ti64 during sintering. The formation of β-Ti and α′ martensitic phases confirmed the diffusion of Ta. The pore size distribution was in the size range of 80 to 500 µm, and a permeability value of 6 × 10(−10) m(2) was close to the trabecular bones one. The mechanical properties of the component were dominated mainly by the porous layer, and Young’s modulus of 16 GPa was in the range of bones. Additionally, the density of this material (6 g/cm(3)) was much lower than the one of pure Ta, which helps to reduce the weight for the desired applications. These results indicate that structurally hybridized materials, also known as composites, with specific property profiles can improve the response to osseointegration for bone implant applications. MDPI 2023-06-14 /pmc/articles/PMC10302576/ /pubmed/37374557 http://dx.doi.org/10.3390/ma16124372 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Alvarado-Hernández, Francisco
Mihalcea, Elena
Jimenez, Omar
Macías, Rogelio
Olmos, Luis
López-Baltazar, Enrique A.
Guevara-Martinez, Santiago
Lemus-Ruiz, José
Design of Ti64/Ta Hybrid Materials by Powder Metallurgy Mimicking Bone Structure
title Design of Ti64/Ta Hybrid Materials by Powder Metallurgy Mimicking Bone Structure
title_full Design of Ti64/Ta Hybrid Materials by Powder Metallurgy Mimicking Bone Structure
title_fullStr Design of Ti64/Ta Hybrid Materials by Powder Metallurgy Mimicking Bone Structure
title_full_unstemmed Design of Ti64/Ta Hybrid Materials by Powder Metallurgy Mimicking Bone Structure
title_short Design of Ti64/Ta Hybrid Materials by Powder Metallurgy Mimicking Bone Structure
title_sort design of ti64/ta hybrid materials by powder metallurgy mimicking bone structure
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10302576/
https://www.ncbi.nlm.nih.gov/pubmed/37374557
http://dx.doi.org/10.3390/ma16124372
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