The Intracavity Extension of 28-Hetero-2,7-naphthiporphyrins in Reactions with Alkylamines

[Image: see text] The 28-hetero-2,7-naphthiporphyrins reacted with triethylamine and diethylamine to form nonaromatic intracavity-extended macrocycles incorporating naphthodihydro-2H-pyran, naphthotetrahydropyridine, and naphthopyrrolotetrahydro-1H-azepine moieties. The new macrocycles were characte...

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Autores principales: Ślusarek, Katarzyna, Perdek, Jędrzej P., Białońska, Agata, Grzelczak, Rafał A., Szyszko, Bartosz
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2023
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10324391/
https://www.ncbi.nlm.nih.gov/pubmed/37345966
http://dx.doi.org/10.1021/acs.orglett.3c01715
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author Ślusarek, Katarzyna
Perdek, Jędrzej P.
Białońska, Agata
Grzelczak, Rafał A.
Szyszko, Bartosz
author_facet Ślusarek, Katarzyna
Perdek, Jędrzej P.
Białońska, Agata
Grzelczak, Rafał A.
Szyszko, Bartosz
author_sort Ślusarek, Katarzyna
collection PubMed
description [Image: see text] The 28-hetero-2,7-naphthiporphyrins reacted with triethylamine and diethylamine to form nonaromatic intracavity-extended macrocycles incorporating naphthodihydro-2H-pyran, naphthotetrahydropyridine, and naphthopyrrolotetrahydro-1H-azepine moieties. The new macrocycles were characterized in solution by means of NMR and UV–vis spectroscopy and in the solid state by XRD.
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spelling pubmed-103243912023-07-07 The Intracavity Extension of 28-Hetero-2,7-naphthiporphyrins in Reactions with Alkylamines Ślusarek, Katarzyna Perdek, Jędrzej P. Białońska, Agata Grzelczak, Rafał A. Szyszko, Bartosz Org Lett [Image: see text] The 28-hetero-2,7-naphthiporphyrins reacted with triethylamine and diethylamine to form nonaromatic intracavity-extended macrocycles incorporating naphthodihydro-2H-pyran, naphthotetrahydropyridine, and naphthopyrrolotetrahydro-1H-azepine moieties. The new macrocycles were characterized in solution by means of NMR and UV–vis spectroscopy and in the solid state by XRD. American Chemical Society 2023-06-22 /pmc/articles/PMC10324391/ /pubmed/37345966 http://dx.doi.org/10.1021/acs.orglett.3c01715 Text en © 2023 The Authors. Published by American Chemical Society https://creativecommons.org/licenses/by/4.0/Permits the broadest form of re-use including for commercial purposes, provided that author attribution and integrity are maintained (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Ślusarek, Katarzyna
Perdek, Jędrzej P.
Białońska, Agata
Grzelczak, Rafał A.
Szyszko, Bartosz
The Intracavity Extension of 28-Hetero-2,7-naphthiporphyrins in Reactions with Alkylamines
title The Intracavity Extension of 28-Hetero-2,7-naphthiporphyrins in Reactions with Alkylamines
title_full The Intracavity Extension of 28-Hetero-2,7-naphthiporphyrins in Reactions with Alkylamines
title_fullStr The Intracavity Extension of 28-Hetero-2,7-naphthiporphyrins in Reactions with Alkylamines
title_full_unstemmed The Intracavity Extension of 28-Hetero-2,7-naphthiporphyrins in Reactions with Alkylamines
title_short The Intracavity Extension of 28-Hetero-2,7-naphthiporphyrins in Reactions with Alkylamines
title_sort intracavity extension of 28-hetero-2,7-naphthiporphyrins in reactions with alkylamines
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10324391/
https://www.ncbi.nlm.nih.gov/pubmed/37345966
http://dx.doi.org/10.1021/acs.orglett.3c01715
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