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Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites †

Polyamide 6 (PA6) thermoplastic composites have higher recyclability potential when compared to conventional thermoset composites. A disruptive liquid molding manufacturing technology named Thermoplastic Resin Transfer Molding (T-RTM) can be used for processing composites due to the low viscosity of...

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Autores principales: Martins, Filipe P., Santos, Laura, Torcato, Ricardo, Lima, Paulo S., Oliveira, José M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10342555/
https://www.ncbi.nlm.nih.gov/pubmed/37444966
http://dx.doi.org/10.3390/ma16134652
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author Martins, Filipe P.
Santos, Laura
Torcato, Ricardo
Lima, Paulo S.
Oliveira, José M.
author_facet Martins, Filipe P.
Santos, Laura
Torcato, Ricardo
Lima, Paulo S.
Oliveira, José M.
author_sort Martins, Filipe P.
collection PubMed
description Polyamide 6 (PA6) thermoplastic composites have higher recyclability potential when compared to conventional thermoset composites. A disruptive liquid molding manufacturing technology named Thermoplastic Resin Transfer Molding (T-RTM) can be used for processing composites due to the low viscosity of the monomers and additives. In this process, polymerization, crystallization and shrinkage occur almost at the same time. If these phenomena are not controlled, they can compromise the reproducibility and homogeneity of the parts. This work studied the influence of packing pressure, as a process variable, throughout the filling and polymerization stages. To assess the process reproducibility and parts’ homogeneity, physical, thermal and mechanical properties were analyzed in different areas of neat PA6 and composite parts. This study showed that a two-stage packing pressure can be successfully used to increase parts’ homogeneity and process reproducibility. The use of 3.5 bar packing pressure during the polymerization stage resulted in mechanical properties with lower standard deviations, indicating a higher degree of homogeneity of the manufactured parts and higher process reproducibility. These results will be used for establishing the actual state of the technology and will be a base for future process optimization.
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spelling pubmed-103425552023-07-14 Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites † Martins, Filipe P. Santos, Laura Torcato, Ricardo Lima, Paulo S. Oliveira, José M. Materials (Basel) Article Polyamide 6 (PA6) thermoplastic composites have higher recyclability potential when compared to conventional thermoset composites. A disruptive liquid molding manufacturing technology named Thermoplastic Resin Transfer Molding (T-RTM) can be used for processing composites due to the low viscosity of the monomers and additives. In this process, polymerization, crystallization and shrinkage occur almost at the same time. If these phenomena are not controlled, they can compromise the reproducibility and homogeneity of the parts. This work studied the influence of packing pressure, as a process variable, throughout the filling and polymerization stages. To assess the process reproducibility and parts’ homogeneity, physical, thermal and mechanical properties were analyzed in different areas of neat PA6 and composite parts. This study showed that a two-stage packing pressure can be successfully used to increase parts’ homogeneity and process reproducibility. The use of 3.5 bar packing pressure during the polymerization stage resulted in mechanical properties with lower standard deviations, indicating a higher degree of homogeneity of the manufactured parts and higher process reproducibility. These results will be used for establishing the actual state of the technology and will be a base for future process optimization. MDPI 2023-06-28 /pmc/articles/PMC10342555/ /pubmed/37444966 http://dx.doi.org/10.3390/ma16134652 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Martins, Filipe P.
Santos, Laura
Torcato, Ricardo
Lima, Paulo S.
Oliveira, José M.
Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites †
title Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites †
title_full Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites †
title_fullStr Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites †
title_full_unstemmed Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites †
title_short Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites †
title_sort reproducibility study of the thermoplastic resin transfer molding process for glass fiber reinforced polyamide 6 composites †
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10342555/
https://www.ncbi.nlm.nih.gov/pubmed/37444966
http://dx.doi.org/10.3390/ma16134652
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