Cargando…
Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites †
Polyamide 6 (PA6) thermoplastic composites have higher recyclability potential when compared to conventional thermoset composites. A disruptive liquid molding manufacturing technology named Thermoplastic Resin Transfer Molding (T-RTM) can be used for processing composites due to the low viscosity of...
Autores principales: | , , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2023
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10342555/ https://www.ncbi.nlm.nih.gov/pubmed/37444966 http://dx.doi.org/10.3390/ma16134652 |
_version_ | 1785072526948302848 |
---|---|
author | Martins, Filipe P. Santos, Laura Torcato, Ricardo Lima, Paulo S. Oliveira, José M. |
author_facet | Martins, Filipe P. Santos, Laura Torcato, Ricardo Lima, Paulo S. Oliveira, José M. |
author_sort | Martins, Filipe P. |
collection | PubMed |
description | Polyamide 6 (PA6) thermoplastic composites have higher recyclability potential when compared to conventional thermoset composites. A disruptive liquid molding manufacturing technology named Thermoplastic Resin Transfer Molding (T-RTM) can be used for processing composites due to the low viscosity of the monomers and additives. In this process, polymerization, crystallization and shrinkage occur almost at the same time. If these phenomena are not controlled, they can compromise the reproducibility and homogeneity of the parts. This work studied the influence of packing pressure, as a process variable, throughout the filling and polymerization stages. To assess the process reproducibility and parts’ homogeneity, physical, thermal and mechanical properties were analyzed in different areas of neat PA6 and composite parts. This study showed that a two-stage packing pressure can be successfully used to increase parts’ homogeneity and process reproducibility. The use of 3.5 bar packing pressure during the polymerization stage resulted in mechanical properties with lower standard deviations, indicating a higher degree of homogeneity of the manufactured parts and higher process reproducibility. These results will be used for establishing the actual state of the technology and will be a base for future process optimization. |
format | Online Article Text |
id | pubmed-10342555 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-103425552023-07-14 Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites † Martins, Filipe P. Santos, Laura Torcato, Ricardo Lima, Paulo S. Oliveira, José M. Materials (Basel) Article Polyamide 6 (PA6) thermoplastic composites have higher recyclability potential when compared to conventional thermoset composites. A disruptive liquid molding manufacturing technology named Thermoplastic Resin Transfer Molding (T-RTM) can be used for processing composites due to the low viscosity of the monomers and additives. In this process, polymerization, crystallization and shrinkage occur almost at the same time. If these phenomena are not controlled, they can compromise the reproducibility and homogeneity of the parts. This work studied the influence of packing pressure, as a process variable, throughout the filling and polymerization stages. To assess the process reproducibility and parts’ homogeneity, physical, thermal and mechanical properties were analyzed in different areas of neat PA6 and composite parts. This study showed that a two-stage packing pressure can be successfully used to increase parts’ homogeneity and process reproducibility. The use of 3.5 bar packing pressure during the polymerization stage resulted in mechanical properties with lower standard deviations, indicating a higher degree of homogeneity of the manufactured parts and higher process reproducibility. These results will be used for establishing the actual state of the technology and will be a base for future process optimization. MDPI 2023-06-28 /pmc/articles/PMC10342555/ /pubmed/37444966 http://dx.doi.org/10.3390/ma16134652 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Martins, Filipe P. Santos, Laura Torcato, Ricardo Lima, Paulo S. Oliveira, José M. Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites † |
title | Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites † |
title_full | Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites † |
title_fullStr | Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites † |
title_full_unstemmed | Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites † |
title_short | Reproducibility Study of the Thermoplastic Resin Transfer Molding Process for Glass Fiber Reinforced Polyamide 6 Composites † |
title_sort | reproducibility study of the thermoplastic resin transfer molding process for glass fiber reinforced polyamide 6 composites † |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10342555/ https://www.ncbi.nlm.nih.gov/pubmed/37444966 http://dx.doi.org/10.3390/ma16134652 |
work_keys_str_mv | AT martinsfilipep reproducibilitystudyofthethermoplasticresintransfermoldingprocessforglassfiberreinforcedpolyamide6composites AT santoslaura reproducibilitystudyofthethermoplasticresintransfermoldingprocessforglassfiberreinforcedpolyamide6composites AT torcatoricardo reproducibilitystudyofthethermoplasticresintransfermoldingprocessforglassfiberreinforcedpolyamide6composites AT limapaulos reproducibilitystudyofthethermoplasticresintransfermoldingprocessforglassfiberreinforcedpolyamide6composites AT oliveirajosem reproducibilitystudyofthethermoplasticresintransfermoldingprocessforglassfiberreinforcedpolyamide6composites |