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Fiber Orientation Estimation from X-ray Dark Field Images of Fiber Reinforced Polymers Using Constrained Spherical Deconvolution

The properties of fiber reinforced polymers are strongly related to the length and orientation of the fibers within the polymer matrix, the latter of which can be studied using X-ray computed tomography (XCT). Unfortunately, resolving individual fibers is challenging because they are small compared...

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Autores principales: Huyge, Ben, Sanctorum, Jonathan, Jeurissen, Ben, De Beenhouwer, Jan, Sijbers, Jan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10347038/
https://www.ncbi.nlm.nih.gov/pubmed/37447531
http://dx.doi.org/10.3390/polym15132887
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author Huyge, Ben
Sanctorum, Jonathan
Jeurissen, Ben
De Beenhouwer, Jan
Sijbers, Jan
author_facet Huyge, Ben
Sanctorum, Jonathan
Jeurissen, Ben
De Beenhouwer, Jan
Sijbers, Jan
author_sort Huyge, Ben
collection PubMed
description The properties of fiber reinforced polymers are strongly related to the length and orientation of the fibers within the polymer matrix, the latter of which can be studied using X-ray computed tomography (XCT). Unfortunately, resolving individual fibers is challenging because they are small compared to the XCT voxel resolution and because of the low attenuation contrast between the fibers and the surrounding resin. To alleviate both problems, anisotropic dark field tomography via grating based interferometry (GBI) has been proposed. Here, the fiber orientations are extracted by applying a Funk-Radon transform (FRT) to the local scatter function. However, the FRT suffers from a low angular resolution, which complicates estimating fiber orientations for small fiber crossing angles. We propose constrained spherical deconvolution (CSD) as an alternative to the FRT to resolve fiber orientations. Instead of GBI, edge illumination phase contrast imaging is used because estimating fiber orientations with this technique has not yet been explored. Dark field images are generated by a Monte Carlo simulation framework. It is shown that the FRT cannot estimate the fiber orientation accurately for crossing angles smaller than 70 [Formula: see text] , while CSD performs well down to a crossing angle of 50 [Formula: see text]. In general, CSD outperforms the FRT in estimating fiber orientations.
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spelling pubmed-103470382023-07-15 Fiber Orientation Estimation from X-ray Dark Field Images of Fiber Reinforced Polymers Using Constrained Spherical Deconvolution Huyge, Ben Sanctorum, Jonathan Jeurissen, Ben De Beenhouwer, Jan Sijbers, Jan Polymers (Basel) Article The properties of fiber reinforced polymers are strongly related to the length and orientation of the fibers within the polymer matrix, the latter of which can be studied using X-ray computed tomography (XCT). Unfortunately, resolving individual fibers is challenging because they are small compared to the XCT voxel resolution and because of the low attenuation contrast between the fibers and the surrounding resin. To alleviate both problems, anisotropic dark field tomography via grating based interferometry (GBI) has been proposed. Here, the fiber orientations are extracted by applying a Funk-Radon transform (FRT) to the local scatter function. However, the FRT suffers from a low angular resolution, which complicates estimating fiber orientations for small fiber crossing angles. We propose constrained spherical deconvolution (CSD) as an alternative to the FRT to resolve fiber orientations. Instead of GBI, edge illumination phase contrast imaging is used because estimating fiber orientations with this technique has not yet been explored. Dark field images are generated by a Monte Carlo simulation framework. It is shown that the FRT cannot estimate the fiber orientation accurately for crossing angles smaller than 70 [Formula: see text] , while CSD performs well down to a crossing angle of 50 [Formula: see text]. In general, CSD outperforms the FRT in estimating fiber orientations. MDPI 2023-06-29 /pmc/articles/PMC10347038/ /pubmed/37447531 http://dx.doi.org/10.3390/polym15132887 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Huyge, Ben
Sanctorum, Jonathan
Jeurissen, Ben
De Beenhouwer, Jan
Sijbers, Jan
Fiber Orientation Estimation from X-ray Dark Field Images of Fiber Reinforced Polymers Using Constrained Spherical Deconvolution
title Fiber Orientation Estimation from X-ray Dark Field Images of Fiber Reinforced Polymers Using Constrained Spherical Deconvolution
title_full Fiber Orientation Estimation from X-ray Dark Field Images of Fiber Reinforced Polymers Using Constrained Spherical Deconvolution
title_fullStr Fiber Orientation Estimation from X-ray Dark Field Images of Fiber Reinforced Polymers Using Constrained Spherical Deconvolution
title_full_unstemmed Fiber Orientation Estimation from X-ray Dark Field Images of Fiber Reinforced Polymers Using Constrained Spherical Deconvolution
title_short Fiber Orientation Estimation from X-ray Dark Field Images of Fiber Reinforced Polymers Using Constrained Spherical Deconvolution
title_sort fiber orientation estimation from x-ray dark field images of fiber reinforced polymers using constrained spherical deconvolution
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10347038/
https://www.ncbi.nlm.nih.gov/pubmed/37447531
http://dx.doi.org/10.3390/polym15132887
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