Cargando…

Vapor phase-grown TiO(2) and ZnO nanoparticles inside electrospun polymer fibers and their calcination-induced organization

The spatial organization of metal oxide nanoparticles represents an important factor in the chemical utilization of resulting structures. For the production of networks that are composed of metal oxide nanoparticle chains, we dispersed vapor phase-grown TiO(2) and ZnO nanoparticles homogeneously in...

Descripción completa

Detalles Bibliográficos
Autores principales: Razouq, Hasan, Berger, Thomas, Hüsing, Nicola, Diwald, Oliver
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Springer Vienna 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10382359/
https://www.ncbi.nlm.nih.gov/pubmed/37521146
http://dx.doi.org/10.1007/s00706-023-03093-0
_version_ 1785080663591878656
author Razouq, Hasan
Berger, Thomas
Hüsing, Nicola
Diwald, Oliver
author_facet Razouq, Hasan
Berger, Thomas
Hüsing, Nicola
Diwald, Oliver
author_sort Razouq, Hasan
collection PubMed
description The spatial organization of metal oxide nanoparticles represents an important factor in the chemical utilization of resulting structures. For the production of networks that are composed of metal oxide nanoparticle chains, we dispersed vapor phase-grown TiO(2) and ZnO nanoparticles homogeneously in an aqueous polyvinyl alcohol solution. After electrospinning, we analyzed the sizes and diameters of the compositionally homogeneous electrospun fibers and discussed the size distribution and morphology of the nanoparticles inside. Calcination-induced polymer removal gives rise to self-supported nanoparticle-based nanofibers. Particle coarsening by a factor of ~ 2 for TiO(2) and ~ 3 for ZnO nanoparticles is observed. GRAPHICAL ABSTRACT: [Image: see text]
format Online
Article
Text
id pubmed-10382359
institution National Center for Biotechnology Information
language English
publishDate 2023
publisher Springer Vienna
record_format MEDLINE/PubMed
spelling pubmed-103823592023-07-30 Vapor phase-grown TiO(2) and ZnO nanoparticles inside electrospun polymer fibers and their calcination-induced organization Razouq, Hasan Berger, Thomas Hüsing, Nicola Diwald, Oliver Monatsh Chem Original Paper The spatial organization of metal oxide nanoparticles represents an important factor in the chemical utilization of resulting structures. For the production of networks that are composed of metal oxide nanoparticle chains, we dispersed vapor phase-grown TiO(2) and ZnO nanoparticles homogeneously in an aqueous polyvinyl alcohol solution. After electrospinning, we analyzed the sizes and diameters of the compositionally homogeneous electrospun fibers and discussed the size distribution and morphology of the nanoparticles inside. Calcination-induced polymer removal gives rise to self-supported nanoparticle-based nanofibers. Particle coarsening by a factor of ~ 2 for TiO(2) and ~ 3 for ZnO nanoparticles is observed. GRAPHICAL ABSTRACT: [Image: see text] Springer Vienna 2023-07-12 2023 /pmc/articles/PMC10382359/ /pubmed/37521146 http://dx.doi.org/10.1007/s00706-023-03093-0 Text en © The Author(s) 2023 https://creativecommons.org/licenses/by/4.0/Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons licence, and indicate if changes were made. The images or other third party material in this article are included in the article's Creative Commons licence, unless indicated otherwise in a credit line to the material. If material is not included in the article's Creative Commons licence and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this licence, visit http://creativecommons.org/licenses/by/4.0/ (https://creativecommons.org/licenses/by/4.0/) .
spellingShingle Original Paper
Razouq, Hasan
Berger, Thomas
Hüsing, Nicola
Diwald, Oliver
Vapor phase-grown TiO(2) and ZnO nanoparticles inside electrospun polymer fibers and their calcination-induced organization
title Vapor phase-grown TiO(2) and ZnO nanoparticles inside electrospun polymer fibers and their calcination-induced organization
title_full Vapor phase-grown TiO(2) and ZnO nanoparticles inside electrospun polymer fibers and their calcination-induced organization
title_fullStr Vapor phase-grown TiO(2) and ZnO nanoparticles inside electrospun polymer fibers and their calcination-induced organization
title_full_unstemmed Vapor phase-grown TiO(2) and ZnO nanoparticles inside electrospun polymer fibers and their calcination-induced organization
title_short Vapor phase-grown TiO(2) and ZnO nanoparticles inside electrospun polymer fibers and their calcination-induced organization
title_sort vapor phase-grown tio(2) and zno nanoparticles inside electrospun polymer fibers and their calcination-induced organization
topic Original Paper
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10382359/
https://www.ncbi.nlm.nih.gov/pubmed/37521146
http://dx.doi.org/10.1007/s00706-023-03093-0
work_keys_str_mv AT razouqhasan vaporphasegrowntio2andznonanoparticlesinsideelectrospunpolymerfibersandtheircalcinationinducedorganization
AT bergerthomas vaporphasegrowntio2andznonanoparticlesinsideelectrospunpolymerfibersandtheircalcinationinducedorganization
AT husingnicola vaporphasegrowntio2andznonanoparticlesinsideelectrospunpolymerfibersandtheircalcinationinducedorganization
AT diwaldoliver vaporphasegrowntio2andznonanoparticlesinsideelectrospunpolymerfibersandtheircalcinationinducedorganization