Robust phase determination in complex solid solutions using diffuse multiple scattering

A novel methodology is presented for identifying and distinguishing between structural phases in multi-phasic systems, such as piezoelectric materials like PMN–PT [Pb(Mg(1/3)Nb(2/3))O(3)–PbTiO(3)], PIN–PMN–PT [Pb(In(1/2)Nb(1/2))O(3)–Pb(Mg(1/3)Nb(2/3))O(3)–PbTiO(3)] and PZT [Pb(Zr,Ti)O(3)], using dif...

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Detalles Bibliográficos
Autores principales: Nisbet, A. G. A., Cain, M. G., Hase, T., Finkel, P.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Research Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10405585/
https://www.ncbi.nlm.nih.gov/pubmed/37555228
http://dx.doi.org/10.1107/S1600576723004120
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author Nisbet, A. G. A.
Cain, M. G.
Hase, T.
Finkel, P.
author_facet Nisbet, A. G. A.
Cain, M. G.
Hase, T.
Finkel, P.
author_sort Nisbet, A. G. A.
collection PubMed
description A novel methodology is presented for identifying and distinguishing between structural phases in multi-phasic systems, such as piezoelectric materials like PMN–PT [Pb(Mg(1/3)Nb(2/3))O(3)–PbTiO(3)], PIN–PMN–PT [Pb(In(1/2)Nb(1/2))O(3)–Pb(Mg(1/3)Nb(2/3))O(3)–PbTiO(3)] and PZT [Pb(Zr,Ti)O(3)], using diffuse multiple scattering and Kossel line diffraction techniques. The method exploits the splitting of triple line intersections from special coplanar reflections combined with logical constraints to generate a splitting fingerprint for robust crystallographic phase determination and discrimination.
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spelling pubmed-104055852023-08-08 Robust phase determination in complex solid solutions using diffuse multiple scattering Nisbet, A. G. A. Cain, M. G. Hase, T. Finkel, P. J Appl Crystallogr Research Papers A novel methodology is presented for identifying and distinguishing between structural phases in multi-phasic systems, such as piezoelectric materials like PMN–PT [Pb(Mg(1/3)Nb(2/3))O(3)–PbTiO(3)], PIN–PMN–PT [Pb(In(1/2)Nb(1/2))O(3)–Pb(Mg(1/3)Nb(2/3))O(3)–PbTiO(3)] and PZT [Pb(Zr,Ti)O(3)], using diffuse multiple scattering and Kossel line diffraction techniques. The method exploits the splitting of triple line intersections from special coplanar reflections combined with logical constraints to generate a splitting fingerprint for robust crystallographic phase determination and discrimination. International Union of Crystallography 2023-06-12 /pmc/articles/PMC10405585/ /pubmed/37555228 http://dx.doi.org/10.1107/S1600576723004120 Text en © A. G. A. Nisbet et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Nisbet, A. G. A.
Cain, M. G.
Hase, T.
Finkel, P.
Robust phase determination in complex solid solutions using diffuse multiple scattering
title Robust phase determination in complex solid solutions using diffuse multiple scattering
title_full Robust phase determination in complex solid solutions using diffuse multiple scattering
title_fullStr Robust phase determination in complex solid solutions using diffuse multiple scattering
title_full_unstemmed Robust phase determination in complex solid solutions using diffuse multiple scattering
title_short Robust phase determination in complex solid solutions using diffuse multiple scattering
title_sort robust phase determination in complex solid solutions using diffuse multiple scattering
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10405585/
https://www.ncbi.nlm.nih.gov/pubmed/37555228
http://dx.doi.org/10.1107/S1600576723004120
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