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Aluminium Matrix Composite Materials Reinforced by 3D-Printed Ceramic Preforms

This article employed the fused deposition modelling (FDM) method and gas-pressure infiltration to manufacture alumina/AlSi12 composites. Porous ceramic skeletons were prepared by FDM 3D printing of two different alumina powder-filed filaments. The organic component was removed using a combination o...

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Autores principales: Kremzer, Marek, Tomiczek, Błażej, Matula, Grzegorz, Gocki, Michał, Krzemiński, Łukasz
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10420023/
https://www.ncbi.nlm.nih.gov/pubmed/37570177
http://dx.doi.org/10.3390/ma16155473
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author Kremzer, Marek
Tomiczek, Błażej
Matula, Grzegorz
Gocki, Michał
Krzemiński, Łukasz
author_facet Kremzer, Marek
Tomiczek, Błażej
Matula, Grzegorz
Gocki, Michał
Krzemiński, Łukasz
author_sort Kremzer, Marek
collection PubMed
description This article employed the fused deposition modelling (FDM) method and gas-pressure infiltration to manufacture alumina/AlSi12 composites. Porous ceramic skeletons were prepared by FDM 3D printing of two different alumina powder-filed filaments. The organic component was removed using a combination of solvent and heat debinding, and the materials were then sintered at 1500 °C to complete the process. Thermogravimetric tests and DTA analysis were performed to develop an appropriate degradation and sintering program. Manufactured skeletons were subjected to microstructure analysis, porosity analysis, and bending test. The sintering process produced porous alumina ceramic samples with no residual carbon content. Open porosity could occur due to the binder’s degradation. Liquid metal was infiltrated into the ceramic, efficiently filling any open pores and forming a three-dimensional network of the aluminium phase. The microstructure and characteristics of the fabricated materials were investigated using high-resolution scanning electron microscopy, computer tomography, hardness testing, and bending strength testing. The developed composite materials are characterized by the required structure—low porosity and homogenous distribution of the reinforcing phase, better mechanical properties than their matrix and more than twice as high hardness. Hence, the developed innovative technology of their manufacturing can be used in practice.
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spelling pubmed-104200232023-08-12 Aluminium Matrix Composite Materials Reinforced by 3D-Printed Ceramic Preforms Kremzer, Marek Tomiczek, Błażej Matula, Grzegorz Gocki, Michał Krzemiński, Łukasz Materials (Basel) Article This article employed the fused deposition modelling (FDM) method and gas-pressure infiltration to manufacture alumina/AlSi12 composites. Porous ceramic skeletons were prepared by FDM 3D printing of two different alumina powder-filed filaments. The organic component was removed using a combination of solvent and heat debinding, and the materials were then sintered at 1500 °C to complete the process. Thermogravimetric tests and DTA analysis were performed to develop an appropriate degradation and sintering program. Manufactured skeletons were subjected to microstructure analysis, porosity analysis, and bending test. The sintering process produced porous alumina ceramic samples with no residual carbon content. Open porosity could occur due to the binder’s degradation. Liquid metal was infiltrated into the ceramic, efficiently filling any open pores and forming a three-dimensional network of the aluminium phase. The microstructure and characteristics of the fabricated materials were investigated using high-resolution scanning electron microscopy, computer tomography, hardness testing, and bending strength testing. The developed composite materials are characterized by the required structure—low porosity and homogenous distribution of the reinforcing phase, better mechanical properties than their matrix and more than twice as high hardness. Hence, the developed innovative technology of their manufacturing can be used in practice. MDPI 2023-08-04 /pmc/articles/PMC10420023/ /pubmed/37570177 http://dx.doi.org/10.3390/ma16155473 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Kremzer, Marek
Tomiczek, Błażej
Matula, Grzegorz
Gocki, Michał
Krzemiński, Łukasz
Aluminium Matrix Composite Materials Reinforced by 3D-Printed Ceramic Preforms
title Aluminium Matrix Composite Materials Reinforced by 3D-Printed Ceramic Preforms
title_full Aluminium Matrix Composite Materials Reinforced by 3D-Printed Ceramic Preforms
title_fullStr Aluminium Matrix Composite Materials Reinforced by 3D-Printed Ceramic Preforms
title_full_unstemmed Aluminium Matrix Composite Materials Reinforced by 3D-Printed Ceramic Preforms
title_short Aluminium Matrix Composite Materials Reinforced by 3D-Printed Ceramic Preforms
title_sort aluminium matrix composite materials reinforced by 3d-printed ceramic preforms
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10420023/
https://www.ncbi.nlm.nih.gov/pubmed/37570177
http://dx.doi.org/10.3390/ma16155473
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