Design, Construction, and Concept Validation of a Laboratory-Scale Two-phase Reactor to Valorize Whiskey Distillery By-products

[Image: see text] The by-products generated from the whiskey distillation process consist of organic liquids with a high chemical oxygen demand (COD) and residues with a high solid content. Low-carbon strategies that repurpose and valorize such by-products are now imperative to reduce the carbon footprint of the food and beverage industries. The operation of a two-phase anaerobic digester to produce volatile fatty acids (VFAs) and biogas may enable distilleries to transition toward a low-carbon bioeconomy. An example of such a system is a leach bed reactor connected to an expanded granular sludge bed (LBR-EGSB) which was designed, commissioned, and conceptually validated in this paper. Several design improvements progress the LBR-EGSB beyond previous reactor designs. An external gas–liquid–solid separator in the EGSB was used to capture any residual gases produced by the effluent and may reduce the amount of methane slippage and biomass washout. The implementation of a siphon-actuated leachate cup is a low-cost alternative that is less prone to actuation malfunction as compared to electrically actuated solenoid valves in previous reactor designs. Furthermore, replacing fresh water with distillery’s liquid by-products as leachate promotes a circular repurpose and reuse philosophy. The system proved to be effective in generating VFAs (10.3 g VFAs L(–1)(Leachate)), in EGSB COD removal (96%), and in producing methane-rich biogas (75%(vol)), which is higher than the values achieved by traditional anaerobic digestion systems. The LBR-EGSB could ultimately provide more by-product valorization and decarbonization opportunities than traditional anaerobic digestion systems for a whiskey distillery.