Synthesis and crystal structures of (E)-N′-(4-chloro-3-nitro­benzyl­idene)acetohydrazide and (E)-2-(4-chloro­benzyl­idene)-1-(quinolin-8-yl)hydrazine

The syntheses of two benzyl­idenehydrazine derivatives, namely, (E)-N′-(4-chloro-3-nitro­benzyl­idene)acetohydrazide, C(9)H(8)ClN(3)O(3), and (E)-2-(4-chloro­benzyl­idene)-1-(quinolin-8-yl)hydrazine, C(16)H(12)ClN(3), are reported. The mol­ecules have been characterized using IR, (1)H NMR, (13)C NMR...

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Autores principales: Nasr, Tamer, Kariuki, Benson M., Elansary, Mai M., Elhaggar, Radwan, Zaghary, Wafaa
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10439415/
https://www.ncbi.nlm.nih.gov/pubmed/37601392
http://dx.doi.org/10.1107/S2056989023006412
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author Nasr, Tamer
Kariuki, Benson M.
Elansary, Mai M.
Elhaggar, Radwan
Zaghary, Wafaa
author_facet Nasr, Tamer
Kariuki, Benson M.
Elansary, Mai M.
Elhaggar, Radwan
Zaghary, Wafaa
author_sort Nasr, Tamer
collection PubMed
description The syntheses of two benzyl­idenehydrazine derivatives, namely, (E)-N′-(4-chloro-3-nitro­benzyl­idene)acetohydrazide, C(9)H(8)ClN(3)O(3), and (E)-2-(4-chloro­benzyl­idene)-1-(quinolin-8-yl)hydrazine, C(16)H(12)ClN(3), are reported. The mol­ecules have been characterized using IR, (1)H NMR, (13)C NMR and mass spectro­scopic and elemental analysis techniques, and their structures have been determined by single-crystal X-ray diffraction.
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spelling pubmed-104394152023-08-20 Synthesis and crystal structures of (E)-N′-(4-chloro-3-nitro­benzyl­idene)acetohydrazide and (E)-2-(4-chloro­benzyl­idene)-1-(quinolin-8-yl)hydrazine Nasr, Tamer Kariuki, Benson M. Elansary, Mai M. Elhaggar, Radwan Zaghary, Wafaa Acta Crystallogr E Crystallogr Commun Research Communications The syntheses of two benzyl­idenehydrazine derivatives, namely, (E)-N′-(4-chloro-3-nitro­benzyl­idene)acetohydrazide, C(9)H(8)ClN(3)O(3), and (E)-2-(4-chloro­benzyl­idene)-1-(quinolin-8-yl)hydrazine, C(16)H(12)ClN(3), are reported. The mol­ecules have been characterized using IR, (1)H NMR, (13)C NMR and mass spectro­scopic and elemental analysis techniques, and their structures have been determined by single-crystal X-ray diffraction. International Union of Crystallography 2023-07-28 /pmc/articles/PMC10439415/ /pubmed/37601392 http://dx.doi.org/10.1107/S2056989023006412 Text en © Nasr et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Communications
Nasr, Tamer
Kariuki, Benson M.
Elansary, Mai M.
Elhaggar, Radwan
Zaghary, Wafaa
Synthesis and crystal structures of (E)-N′-(4-chloro-3-nitro­benzyl­idene)acetohydrazide and (E)-2-(4-chloro­benzyl­idene)-1-(quinolin-8-yl)hydrazine
title Synthesis and crystal structures of (E)-N′-(4-chloro-3-nitro­benzyl­idene)acetohydrazide and (E)-2-(4-chloro­benzyl­idene)-1-(quinolin-8-yl)hydrazine
title_full Synthesis and crystal structures of (E)-N′-(4-chloro-3-nitro­benzyl­idene)acetohydrazide and (E)-2-(4-chloro­benzyl­idene)-1-(quinolin-8-yl)hydrazine
title_fullStr Synthesis and crystal structures of (E)-N′-(4-chloro-3-nitro­benzyl­idene)acetohydrazide and (E)-2-(4-chloro­benzyl­idene)-1-(quinolin-8-yl)hydrazine
title_full_unstemmed Synthesis and crystal structures of (E)-N′-(4-chloro-3-nitro­benzyl­idene)acetohydrazide and (E)-2-(4-chloro­benzyl­idene)-1-(quinolin-8-yl)hydrazine
title_short Synthesis and crystal structures of (E)-N′-(4-chloro-3-nitro­benzyl­idene)acetohydrazide and (E)-2-(4-chloro­benzyl­idene)-1-(quinolin-8-yl)hydrazine
title_sort synthesis and crystal structures of (e)-n′-(4-chloro-3-nitro­benzyl­idene)acetohydrazide and (e)-2-(4-chloro­benzyl­idene)-1-(quinolin-8-yl)hydrazine
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10439415/
https://www.ncbi.nlm.nih.gov/pubmed/37601392
http://dx.doi.org/10.1107/S2056989023006412
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