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Structural Analysis of Cu(+) and Cu(2+) Ions in Zeolite as a Nanoreactor with Antibacterial Applications

[Image: see text] In this work, we report the structural analysis of Cu(+) and Cu(2+) ions in zeolite as a nanoreactor with antibacterial applications. A simple one-step process was implemented to obtain Cu ions in zeolite A (ZA4) by controlling the temperature in the solutions to guarantee the ions...

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Autores principales: Flores-Valenzuela, J., Leal-Perez, J. E., Almaral-Sanchez, J. L., Hurtado-Macias, A., Borquez-Mendivil, A., Vargas-Ortiz, R. A., Garcia-Grajeda, B. A., Duran-Perez, S. A., Cortez-Valadez, Manuel
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2023
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10448675/
https://www.ncbi.nlm.nih.gov/pubmed/37636981
http://dx.doi.org/10.1021/acsomega.3c03869
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author Flores-Valenzuela, J.
Leal-Perez, J. E.
Almaral-Sanchez, J. L.
Hurtado-Macias, A.
Borquez-Mendivil, A.
Vargas-Ortiz, R. A.
Garcia-Grajeda, B. A.
Duran-Perez, S. A.
Cortez-Valadez, Manuel
author_facet Flores-Valenzuela, J.
Leal-Perez, J. E.
Almaral-Sanchez, J. L.
Hurtado-Macias, A.
Borquez-Mendivil, A.
Vargas-Ortiz, R. A.
Garcia-Grajeda, B. A.
Duran-Perez, S. A.
Cortez-Valadez, Manuel
author_sort Flores-Valenzuela, J.
collection PubMed
description [Image: see text] In this work, we report the structural analysis of Cu(+) and Cu(2+) ions in zeolite as a nanoreactor with antibacterial applications. A simple one-step process was implemented to obtain Cu ions in zeolite A (ZA4) by controlling the temperature in the solutions to guarantee the ions’ stability. Samples were characterized by scanning electron microscopy, energy-dispersive X-ray spectroscopy, and Fourier transform infrared (FT-IR) spectroscopy, showing the characteristic zeolite elements as well as the characteristic bands with slight modifications in the chemical environment of the zeolite nanoreactor attributed to Cu ions by FT-IR spectroscopy. In addition, a shift of the characteristic peaks of ZA4 in X-ray diffraction was observed as well as a decrease in relative peak intensity. On the other hand, the antibacterial activity of Cu ions in the zeolite nanoreactor was evaluated.
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spelling pubmed-104486752023-08-25 Structural Analysis of Cu(+) and Cu(2+) Ions in Zeolite as a Nanoreactor with Antibacterial Applications Flores-Valenzuela, J. Leal-Perez, J. E. Almaral-Sanchez, J. L. Hurtado-Macias, A. Borquez-Mendivil, A. Vargas-Ortiz, R. A. Garcia-Grajeda, B. A. Duran-Perez, S. A. Cortez-Valadez, Manuel ACS Omega [Image: see text] In this work, we report the structural analysis of Cu(+) and Cu(2+) ions in zeolite as a nanoreactor with antibacterial applications. A simple one-step process was implemented to obtain Cu ions in zeolite A (ZA4) by controlling the temperature in the solutions to guarantee the ions’ stability. Samples were characterized by scanning electron microscopy, energy-dispersive X-ray spectroscopy, and Fourier transform infrared (FT-IR) spectroscopy, showing the characteristic zeolite elements as well as the characteristic bands with slight modifications in the chemical environment of the zeolite nanoreactor attributed to Cu ions by FT-IR spectroscopy. In addition, a shift of the characteristic peaks of ZA4 in X-ray diffraction was observed as well as a decrease in relative peak intensity. On the other hand, the antibacterial activity of Cu ions in the zeolite nanoreactor was evaluated. American Chemical Society 2023-08-08 /pmc/articles/PMC10448675/ /pubmed/37636981 http://dx.doi.org/10.1021/acsomega.3c03869 Text en © 2023 The Authors. Published by American Chemical Society https://creativecommons.org/licenses/by/4.0/Permits the broadest form of re-use including for commercial purposes, provided that author attribution and integrity are maintained (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Flores-Valenzuela, J.
Leal-Perez, J. E.
Almaral-Sanchez, J. L.
Hurtado-Macias, A.
Borquez-Mendivil, A.
Vargas-Ortiz, R. A.
Garcia-Grajeda, B. A.
Duran-Perez, S. A.
Cortez-Valadez, Manuel
Structural Analysis of Cu(+) and Cu(2+) Ions in Zeolite as a Nanoreactor with Antibacterial Applications
title Structural Analysis of Cu(+) and Cu(2+) Ions in Zeolite as a Nanoreactor with Antibacterial Applications
title_full Structural Analysis of Cu(+) and Cu(2+) Ions in Zeolite as a Nanoreactor with Antibacterial Applications
title_fullStr Structural Analysis of Cu(+) and Cu(2+) Ions in Zeolite as a Nanoreactor with Antibacterial Applications
title_full_unstemmed Structural Analysis of Cu(+) and Cu(2+) Ions in Zeolite as a Nanoreactor with Antibacterial Applications
title_short Structural Analysis of Cu(+) and Cu(2+) Ions in Zeolite as a Nanoreactor with Antibacterial Applications
title_sort structural analysis of cu(+) and cu(2+) ions in zeolite as a nanoreactor with antibacterial applications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10448675/
https://www.ncbi.nlm.nih.gov/pubmed/37636981
http://dx.doi.org/10.1021/acsomega.3c03869
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