Cargando…

Synthesis of Composites for the Removal of F(-) Anions

This work presents the synthesis of amine and ferrihydrite functionalized graphene oxide for the removal of fluoride from water. The synthesis of the graphene oxide and the modified with amine groups is developed by following the modified Hummer’s method. Fourier transform infrared spectrometry, X-r...

Descripción completa

Detalles Bibliográficos
Autores principales: Saldaña-Robles, Adriana, Arcibar-Orozco, Javier Antonio, Guerrero-Mosqueda, Luz Rocío, Damián-Ascencio, César Eduardo, Marquez-Herrera, Alfredo, Corona, Miguel, Gallegos-Muñoz, Armando, Cano-Andrade, Sergio
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10458539/
https://www.ncbi.nlm.nih.gov/pubmed/37630861
http://dx.doi.org/10.3390/nano13162277
_version_ 1785097189898321920
author Saldaña-Robles, Adriana
Arcibar-Orozco, Javier Antonio
Guerrero-Mosqueda, Luz Rocío
Damián-Ascencio, César Eduardo
Marquez-Herrera, Alfredo
Corona, Miguel
Gallegos-Muñoz, Armando
Cano-Andrade, Sergio
author_facet Saldaña-Robles, Adriana
Arcibar-Orozco, Javier Antonio
Guerrero-Mosqueda, Luz Rocío
Damián-Ascencio, César Eduardo
Marquez-Herrera, Alfredo
Corona, Miguel
Gallegos-Muñoz, Armando
Cano-Andrade, Sergio
author_sort Saldaña-Robles, Adriana
collection PubMed
description This work presents the synthesis of amine and ferrihydrite functionalized graphene oxide for the removal of fluoride from water. The synthesis of the graphene oxide and the modified with amine groups is developed by following the modified Hummer’s method. Fourier transform infrared spectrometry, X-ray, Raman spectroscopy, thermogravimetric analysis, surface charge distribution, specific surface area and porosity, adsorption isotherms, and the van’t Hoff equation are used for the characterization of the synthesized materials. Results show that the addition of amines with ferrihydrite generates wrinkles on the surface layers, suggesting a successful incorporation of nitrogen onto the graphene oxide; and as a consequence, the adsorption capacity per unit area of the materials is increased.
format Online
Article
Text
id pubmed-10458539
institution National Center for Biotechnology Information
language English
publishDate 2023
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-104585392023-08-27 Synthesis of Composites for the Removal of F(-) Anions Saldaña-Robles, Adriana Arcibar-Orozco, Javier Antonio Guerrero-Mosqueda, Luz Rocío Damián-Ascencio, César Eduardo Marquez-Herrera, Alfredo Corona, Miguel Gallegos-Muñoz, Armando Cano-Andrade, Sergio Nanomaterials (Basel) Article This work presents the synthesis of amine and ferrihydrite functionalized graphene oxide for the removal of fluoride from water. The synthesis of the graphene oxide and the modified with amine groups is developed by following the modified Hummer’s method. Fourier transform infrared spectrometry, X-ray, Raman spectroscopy, thermogravimetric analysis, surface charge distribution, specific surface area and porosity, adsorption isotherms, and the van’t Hoff equation are used for the characterization of the synthesized materials. Results show that the addition of amines with ferrihydrite generates wrinkles on the surface layers, suggesting a successful incorporation of nitrogen onto the graphene oxide; and as a consequence, the adsorption capacity per unit area of the materials is increased. MDPI 2023-08-08 /pmc/articles/PMC10458539/ /pubmed/37630861 http://dx.doi.org/10.3390/nano13162277 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Saldaña-Robles, Adriana
Arcibar-Orozco, Javier Antonio
Guerrero-Mosqueda, Luz Rocío
Damián-Ascencio, César Eduardo
Marquez-Herrera, Alfredo
Corona, Miguel
Gallegos-Muñoz, Armando
Cano-Andrade, Sergio
Synthesis of Composites for the Removal of F(-) Anions
title Synthesis of Composites for the Removal of F(-) Anions
title_full Synthesis of Composites for the Removal of F(-) Anions
title_fullStr Synthesis of Composites for the Removal of F(-) Anions
title_full_unstemmed Synthesis of Composites for the Removal of F(-) Anions
title_short Synthesis of Composites for the Removal of F(-) Anions
title_sort synthesis of composites for the removal of f(-) anions
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10458539/
https://www.ncbi.nlm.nih.gov/pubmed/37630861
http://dx.doi.org/10.3390/nano13162277
work_keys_str_mv AT saldanaroblesadriana synthesisofcompositesfortheremovaloffanions
AT arcibarorozcojavierantonio synthesisofcompositesfortheremovaloffanions
AT guerreromosquedaluzrocio synthesisofcompositesfortheremovaloffanions
AT damianascenciocesareduardo synthesisofcompositesfortheremovaloffanions
AT marquezherreraalfredo synthesisofcompositesfortheremovaloffanions
AT coronamiguel synthesisofcompositesfortheremovaloffanions
AT gallegosmunozarmando synthesisofcompositesfortheremovaloffanions
AT canoandradesergio synthesisofcompositesfortheremovaloffanions