Cargando…

A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals

Titanate-based perovskite powders are the most widely used materials for fabrication of multilayered ceramic capacitors and thus are of significant importance. They have been synthesized by two approaches including solid-state and wet chemical processing methods. Synthesis temperature, cost of prepa...

Descripción completa

Detalles Bibliográficos
Autores principales: Mojed, Ali, Ashiri, Rouholah, Shafyei, Ali
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10480632/
https://www.ncbi.nlm.nih.gov/pubmed/37657368
http://dx.doi.org/10.1016/j.ultsonch.2023.106568
_version_ 1785101831849902080
author Mojed, Ali
Ashiri, Rouholah
Shafyei, Ali
author_facet Mojed, Ali
Ashiri, Rouholah
Shafyei, Ali
author_sort Mojed, Ali
collection PubMed
description Titanate-based perovskite powders are the most widely used materials for fabrication of multilayered ceramic capacitors and thus are of significant importance. They have been synthesized by two approaches including solid-state and wet chemical processing methods. Synthesis temperature, cost of preparation and quality of synthesized powders are key factors favoring the process. Here, a new ultrasound-assisted precipitation approach is introduced which is able to obtain the quality perovskite nanocrystals such as strontium titanate, barium titanate and so on at room temperature. The obtained powder products were characterized by DTA/TGA, FT-IR, XRD, SEM, EDAX and TEM. The results indicate the room temperature formation of highly pure monosized spherical nanoscale crystals which are loosely agglomerated in nature. It is tried to add the science, mechanism involved in the synthesis and its reaction pattern to the literature along with discussing the cause of low temperature obtainment of the perovskite powder products. The approach described in the current work has the capability to be a general strategy for the synthesis of perovskite materials and essential potentials for large-scale production purposes as it is facile, low temperature and cost-effective.
format Online
Article
Text
id pubmed-10480632
institution National Center for Biotechnology Information
language English
publishDate 2023
publisher Elsevier
record_format MEDLINE/PubMed
spelling pubmed-104806322023-09-07 A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals Mojed, Ali Ashiri, Rouholah Shafyei, Ali Ultrason Sonochem Original Research Article Titanate-based perovskite powders are the most widely used materials for fabrication of multilayered ceramic capacitors and thus are of significant importance. They have been synthesized by two approaches including solid-state and wet chemical processing methods. Synthesis temperature, cost of preparation and quality of synthesized powders are key factors favoring the process. Here, a new ultrasound-assisted precipitation approach is introduced which is able to obtain the quality perovskite nanocrystals such as strontium titanate, barium titanate and so on at room temperature. The obtained powder products were characterized by DTA/TGA, FT-IR, XRD, SEM, EDAX and TEM. The results indicate the room temperature formation of highly pure monosized spherical nanoscale crystals which are loosely agglomerated in nature. It is tried to add the science, mechanism involved in the synthesis and its reaction pattern to the literature along with discussing the cause of low temperature obtainment of the perovskite powder products. The approach described in the current work has the capability to be a general strategy for the synthesis of perovskite materials and essential potentials for large-scale production purposes as it is facile, low temperature and cost-effective. Elsevier 2023-08-25 /pmc/articles/PMC10480632/ /pubmed/37657368 http://dx.doi.org/10.1016/j.ultsonch.2023.106568 Text en © 2023 The Author(s) https://creativecommons.org/licenses/by-nc-nd/4.0/This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
spellingShingle Original Research Article
Mojed, Ali
Ashiri, Rouholah
Shafyei, Ali
A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals
title A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals
title_full A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals
title_fullStr A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals
title_full_unstemmed A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals
title_short A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals
title_sort mechanistic study on efficient room temperature sonocolloidal obtainment of srtio(3) nanocrystals
topic Original Research Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10480632/
https://www.ncbi.nlm.nih.gov/pubmed/37657368
http://dx.doi.org/10.1016/j.ultsonch.2023.106568
work_keys_str_mv AT mojedali amechanisticstudyonefficientroomtemperaturesonocolloidalobtainmentofsrtio3nanocrystals
AT ashirirouholah amechanisticstudyonefficientroomtemperaturesonocolloidalobtainmentofsrtio3nanocrystals
AT shafyeiali amechanisticstudyonefficientroomtemperaturesonocolloidalobtainmentofsrtio3nanocrystals
AT mojedali mechanisticstudyonefficientroomtemperaturesonocolloidalobtainmentofsrtio3nanocrystals
AT ashirirouholah mechanisticstudyonefficientroomtemperaturesonocolloidalobtainmentofsrtio3nanocrystals
AT shafyeiali mechanisticstudyonefficientroomtemperaturesonocolloidalobtainmentofsrtio3nanocrystals