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A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals
Titanate-based perovskite powders are the most widely used materials for fabrication of multilayered ceramic capacitors and thus are of significant importance. They have been synthesized by two approaches including solid-state and wet chemical processing methods. Synthesis temperature, cost of prepa...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Elsevier
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10480632/ https://www.ncbi.nlm.nih.gov/pubmed/37657368 http://dx.doi.org/10.1016/j.ultsonch.2023.106568 |
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author | Mojed, Ali Ashiri, Rouholah Shafyei, Ali |
author_facet | Mojed, Ali Ashiri, Rouholah Shafyei, Ali |
author_sort | Mojed, Ali |
collection | PubMed |
description | Titanate-based perovskite powders are the most widely used materials for fabrication of multilayered ceramic capacitors and thus are of significant importance. They have been synthesized by two approaches including solid-state and wet chemical processing methods. Synthesis temperature, cost of preparation and quality of synthesized powders are key factors favoring the process. Here, a new ultrasound-assisted precipitation approach is introduced which is able to obtain the quality perovskite nanocrystals such as strontium titanate, barium titanate and so on at room temperature. The obtained powder products were characterized by DTA/TGA, FT-IR, XRD, SEM, EDAX and TEM. The results indicate the room temperature formation of highly pure monosized spherical nanoscale crystals which are loosely agglomerated in nature. It is tried to add the science, mechanism involved in the synthesis and its reaction pattern to the literature along with discussing the cause of low temperature obtainment of the perovskite powder products. The approach described in the current work has the capability to be a general strategy for the synthesis of perovskite materials and essential potentials for large-scale production purposes as it is facile, low temperature and cost-effective. |
format | Online Article Text |
id | pubmed-10480632 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | Elsevier |
record_format | MEDLINE/PubMed |
spelling | pubmed-104806322023-09-07 A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals Mojed, Ali Ashiri, Rouholah Shafyei, Ali Ultrason Sonochem Original Research Article Titanate-based perovskite powders are the most widely used materials for fabrication of multilayered ceramic capacitors and thus are of significant importance. They have been synthesized by two approaches including solid-state and wet chemical processing methods. Synthesis temperature, cost of preparation and quality of synthesized powders are key factors favoring the process. Here, a new ultrasound-assisted precipitation approach is introduced which is able to obtain the quality perovskite nanocrystals such as strontium titanate, barium titanate and so on at room temperature. The obtained powder products were characterized by DTA/TGA, FT-IR, XRD, SEM, EDAX and TEM. The results indicate the room temperature formation of highly pure monosized spherical nanoscale crystals which are loosely agglomerated in nature. It is tried to add the science, mechanism involved in the synthesis and its reaction pattern to the literature along with discussing the cause of low temperature obtainment of the perovskite powder products. The approach described in the current work has the capability to be a general strategy for the synthesis of perovskite materials and essential potentials for large-scale production purposes as it is facile, low temperature and cost-effective. Elsevier 2023-08-25 /pmc/articles/PMC10480632/ /pubmed/37657368 http://dx.doi.org/10.1016/j.ultsonch.2023.106568 Text en © 2023 The Author(s) https://creativecommons.org/licenses/by-nc-nd/4.0/This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/). |
spellingShingle | Original Research Article Mojed, Ali Ashiri, Rouholah Shafyei, Ali A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals |
title | A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals |
title_full | A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals |
title_fullStr | A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals |
title_full_unstemmed | A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals |
title_short | A mechanistic study on efficient room temperature sonocolloidal obtainment of SrTiO(3) nanocrystals |
title_sort | mechanistic study on efficient room temperature sonocolloidal obtainment of srtio(3) nanocrystals |
topic | Original Research Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10480632/ https://www.ncbi.nlm.nih.gov/pubmed/37657368 http://dx.doi.org/10.1016/j.ultsonch.2023.106568 |
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