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Spectroscopic, crystallographic, and Hirshfeld surface characterization of nine-membered-ring-containing 9-methoxy-3,4,5,6-tetrahydro-1H-benzo[b]azonine-2,7-dione and its parent tetrahydrocarbazole
9-Methoxy-3,4,5,6-tetrahydro-1H-benzo[b]azonine-2,7-dione, C(13)H(15)NO(3), (I), and 6-methoxy-1,2,3,4-tetrahydrocarbazole, C(13)H(15)NO, (II), represent the structures of a benzoazonine that contains a nine-membered ring and its parent tetrahydrocarbazole. The molecules of (I) pack toge...
| Autores principales: | , , |
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| Formato: | Online Artículo Texto |
| Lenguaje: | English |
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International Union of Crystallography
2023
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| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10483559/ https://www.ncbi.nlm.nih.gov/pubmed/37693673 http://dx.doi.org/10.1107/S2056989023007259 |
| _version_ | 1785102413540098048 |
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| author | Flores, Maritza J. Mai, Brandon Tanski, Joseph M. |
| author_facet | Flores, Maritza J. Mai, Brandon Tanski, Joseph M. |
| author_sort | Flores, Maritza J. |
| collection | PubMed |
| description | 9-Methoxy-3,4,5,6-tetrahydro-1H-benzo[b]azonine-2,7-dione, C(13)H(15)NO(3), (I), and 6-methoxy-1,2,3,4-tetrahydrocarbazole, C(13)H(15)NO, (II), represent the structures of a benzoazonine that contains a nine-membered ring and its parent tetrahydrocarbazole. The molecules of (I) pack together via strong amide N—H⋯O hydrogen bonding and weak C—H⋯O interactions, whereas the parent tetrahydrocarbazole (II) packs with C/N—H⋯π interactions, as visualized by Hirshfeld surface characterization. |
| format | Online Article Text |
| id | pubmed-10483559 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2023 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-104835592023-09-08 Spectroscopic, crystallographic, and Hirshfeld surface characterization of nine-membered-ring-containing 9-methoxy-3,4,5,6-tetrahydro-1H-benzo[b]azonine-2,7-dione and its parent tetrahydrocarbazole Flores, Maritza J. Mai, Brandon Tanski, Joseph M. Acta Crystallogr E Crystallogr Commun Research Communications 9-Methoxy-3,4,5,6-tetrahydro-1H-benzo[b]azonine-2,7-dione, C(13)H(15)NO(3), (I), and 6-methoxy-1,2,3,4-tetrahydrocarbazole, C(13)H(15)NO, (II), represent the structures of a benzoazonine that contains a nine-membered ring and its parent tetrahydrocarbazole. The molecules of (I) pack together via strong amide N—H⋯O hydrogen bonding and weak C—H⋯O interactions, whereas the parent tetrahydrocarbazole (II) packs with C/N—H⋯π interactions, as visualized by Hirshfeld surface characterization. International Union of Crystallography 2023-08-23 /pmc/articles/PMC10483559/ /pubmed/37693673 http://dx.doi.org/10.1107/S2056989023007259 Text en © Flores et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Research Communications Flores, Maritza J. Mai, Brandon Tanski, Joseph M. Spectroscopic, crystallographic, and Hirshfeld surface characterization of nine-membered-ring-containing 9-methoxy-3,4,5,6-tetrahydro-1H-benzo[b]azonine-2,7-dione and its parent tetrahydrocarbazole |
| title | Spectroscopic, crystallographic, and Hirshfeld surface characterization of nine-membered-ring-containing 9-methoxy-3,4,5,6-tetrahydro-1H-benzo[b]azonine-2,7-dione and its parent tetrahydrocarbazole |
| title_full | Spectroscopic, crystallographic, and Hirshfeld surface characterization of nine-membered-ring-containing 9-methoxy-3,4,5,6-tetrahydro-1H-benzo[b]azonine-2,7-dione and its parent tetrahydrocarbazole |
| title_fullStr | Spectroscopic, crystallographic, and Hirshfeld surface characterization of nine-membered-ring-containing 9-methoxy-3,4,5,6-tetrahydro-1H-benzo[b]azonine-2,7-dione and its parent tetrahydrocarbazole |
| title_full_unstemmed | Spectroscopic, crystallographic, and Hirshfeld surface characterization of nine-membered-ring-containing 9-methoxy-3,4,5,6-tetrahydro-1H-benzo[b]azonine-2,7-dione and its parent tetrahydrocarbazole |
| title_short | Spectroscopic, crystallographic, and Hirshfeld surface characterization of nine-membered-ring-containing 9-methoxy-3,4,5,6-tetrahydro-1H-benzo[b]azonine-2,7-dione and its parent tetrahydrocarbazole |
| title_sort | spectroscopic, crystallographic, and hirshfeld surface characterization of nine-membered-ring-containing 9-methoxy-3,4,5,6-tetrahydro-1h-benzo[b]azonine-2,7-dione and its parent tetrahydrocarbazole |
| topic | Research Communications |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10483559/ https://www.ncbi.nlm.nih.gov/pubmed/37693673 http://dx.doi.org/10.1107/S2056989023007259 |
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