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Efficient Reduction in Methylene Blue Using Palladium Nanoparticles Supported by Melamine-Based Polymer

In this work, palladium nanoparticles, supported by polyaminals (Pd@PAN-NA), were synthesized via a reverse double solvent approach and used as a nano catalyst. The thermogravimetric and the elemental analysis revealed that the catalyst had good dispersity and improved thermal stability. The catalyt...

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Autores principales: Alkayal, Nazeeha S., Ibrahim, Manal, Tashkandi, Nada, Alotaibi, Maha M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10488429/
https://www.ncbi.nlm.nih.gov/pubmed/37687576
http://dx.doi.org/10.3390/ma16175887
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author Alkayal, Nazeeha S.
Ibrahim, Manal
Tashkandi, Nada
Alotaibi, Maha M.
author_facet Alkayal, Nazeeha S.
Ibrahim, Manal
Tashkandi, Nada
Alotaibi, Maha M.
author_sort Alkayal, Nazeeha S.
collection PubMed
description In this work, palladium nanoparticles, supported by polyaminals (Pd@PAN-NA), were synthesized via a reverse double solvent approach and used as a nano catalyst. The thermogravimetric and the elemental analysis revealed that the catalyst had good dispersity and improved thermal stability. The catalytic activity of the prepared Pd@PAN-NA catalyst was studied for a methylene blue chemical reaction in the presence of NaBH(4) as a reducing agent. The effect of the catalyst dose, pH, and dye initial concentration were examined to optimize the chemical reduction conditions. The prepared catalyst Pd@PAN-NA removed 99.8% of methylene blue organic dye, indicating its potential effect for treating waste and contaminated water.
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spelling pubmed-104884292023-09-09 Efficient Reduction in Methylene Blue Using Palladium Nanoparticles Supported by Melamine-Based Polymer Alkayal, Nazeeha S. Ibrahim, Manal Tashkandi, Nada Alotaibi, Maha M. Materials (Basel) Article In this work, palladium nanoparticles, supported by polyaminals (Pd@PAN-NA), were synthesized via a reverse double solvent approach and used as a nano catalyst. The thermogravimetric and the elemental analysis revealed that the catalyst had good dispersity and improved thermal stability. The catalytic activity of the prepared Pd@PAN-NA catalyst was studied for a methylene blue chemical reaction in the presence of NaBH(4) as a reducing agent. The effect of the catalyst dose, pH, and dye initial concentration were examined to optimize the chemical reduction conditions. The prepared catalyst Pd@PAN-NA removed 99.8% of methylene blue organic dye, indicating its potential effect for treating waste and contaminated water. MDPI 2023-08-28 /pmc/articles/PMC10488429/ /pubmed/37687576 http://dx.doi.org/10.3390/ma16175887 Text en © 2023 by the authors. https://creativecommons.org/licenses/by/4.0/Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Alkayal, Nazeeha S.
Ibrahim, Manal
Tashkandi, Nada
Alotaibi, Maha M.
Efficient Reduction in Methylene Blue Using Palladium Nanoparticles Supported by Melamine-Based Polymer
title Efficient Reduction in Methylene Blue Using Palladium Nanoparticles Supported by Melamine-Based Polymer
title_full Efficient Reduction in Methylene Blue Using Palladium Nanoparticles Supported by Melamine-Based Polymer
title_fullStr Efficient Reduction in Methylene Blue Using Palladium Nanoparticles Supported by Melamine-Based Polymer
title_full_unstemmed Efficient Reduction in Methylene Blue Using Palladium Nanoparticles Supported by Melamine-Based Polymer
title_short Efficient Reduction in Methylene Blue Using Palladium Nanoparticles Supported by Melamine-Based Polymer
title_sort efficient reduction in methylene blue using palladium nanoparticles supported by melamine-based polymer
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10488429/
https://www.ncbi.nlm.nih.gov/pubmed/37687576
http://dx.doi.org/10.3390/ma16175887
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