Efficient and biocompatible new palladium-supported boehmite nanoparticles: synthesis, characterization and application in Suzuki–Miura and Mizoroki–Heck coupling reactions

Palladium complex-supported on boehmite (Pd(0)-SMTU-boehmite) nanoparticles were synthesized and characterized by using XRD, SEM, EDS, TGA, BET, ICP and FT-IR techniques. When applied as a new catalyst for C–C coupling reactions of Suzuki–Miyaura and Mizoroki–Heck in PEG-400 solvent, the Pd(0)-SMTU-...

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Detalles Bibliográficos
Autores principales: Hajighasemi, Zahra, Nahipour, Ali, Ghorbani-Choghamarani, Arash, Taherinia, Zahrra
Formato: Online Artículo Texto
Lenguaje:English
Publicado: RSC 2023
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10496902/
https://www.ncbi.nlm.nih.gov/pubmed/37705777
http://dx.doi.org/10.1039/d3na00403a
Descripción
Sumario:Palladium complex-supported on boehmite (Pd(0)-SMTU-boehmite) nanoparticles were synthesized and characterized by using XRD, SEM, EDS, TGA, BET, ICP and FT-IR techniques. When applied as a new catalyst for C–C coupling reactions of Suzuki–Miyaura and Mizoroki–Heck in PEG-400 solvent, the Pd(0)-SMTU-boehmite nanoparticles showed excellent activity and recyclability. The study of palladium leaching by the ICP-OES technique and hot filtration led to the catalyst exhibiting excellent stability and recyclability.

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