Efficient and biocompatible new palladium-supported boehmite nanoparticles: synthesis, characterization and application in Suzuki–Miura and Mizoroki–Heck coupling reactions

Palladium complex-supported on boehmite (Pd(0)-SMTU-boehmite) nanoparticles were synthesized and characterized by using XRD, SEM, EDS, TGA, BET, ICP and FT-IR techniques. When applied as a new catalyst for C–C coupling reactions of Suzuki–Miyaura and Mizoroki–Heck in PEG-400 solvent, the Pd(0)-SMTU-...

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Autores principales: Hajighasemi, Zahra, Nahipour, Ali, Ghorbani-Choghamarani, Arash, Taherinia, Zahrra
Formato: Online Artículo Texto
Lenguaje:English
Publicado: RSC 2023
Materias:
Chemistry
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10496902/
https://www.ncbi.nlm.nih.gov/pubmed/37705777
http://dx.doi.org/10.1039/d3na00403a
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author Hajighasemi, Zahra
Nahipour, Ali
Ghorbani-Choghamarani, Arash
Taherinia, Zahrra
author_facet Hajighasemi, Zahra
Nahipour, Ali
Ghorbani-Choghamarani, Arash
Taherinia, Zahrra
author_sort Hajighasemi, Zahra
collection PubMed
description Palladium complex-supported on boehmite (Pd(0)-SMTU-boehmite) nanoparticles were synthesized and characterized by using XRD, SEM, EDS, TGA, BET, ICP and FT-IR techniques. When applied as a new catalyst for C–C coupling reactions of Suzuki–Miyaura and Mizoroki–Heck in PEG-400 solvent, the Pd(0)-SMTU-boehmite nanoparticles showed excellent activity and recyclability. The study of palladium leaching by the ICP-OES technique and hot filtration led to the catalyst exhibiting excellent stability and recyclability.
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spelling pubmed-104969022023-09-13 Efficient and biocompatible new palladium-supported boehmite nanoparticles: synthesis, characterization and application in Suzuki–Miura and Mizoroki–Heck coupling reactions Hajighasemi, Zahra Nahipour, Ali Ghorbani-Choghamarani, Arash Taherinia, Zahrra Nanoscale Adv Chemistry Palladium complex-supported on boehmite (Pd(0)-SMTU-boehmite) nanoparticles were synthesized and characterized by using XRD, SEM, EDS, TGA, BET, ICP and FT-IR techniques. When applied as a new catalyst for C–C coupling reactions of Suzuki–Miyaura and Mizoroki–Heck in PEG-400 solvent, the Pd(0)-SMTU-boehmite nanoparticles showed excellent activity and recyclability. The study of palladium leaching by the ICP-OES technique and hot filtration led to the catalyst exhibiting excellent stability and recyclability. RSC 2023-08-14 /pmc/articles/PMC10496902/ /pubmed/37705777 http://dx.doi.org/10.1039/d3na00403a Text en This journal is © The Royal Society of Chemistry https://creativecommons.org/licenses/by/3.0/
spellingShingle Chemistry
Hajighasemi, Zahra
Nahipour, Ali
Ghorbani-Choghamarani, Arash
Taherinia, Zahrra
Efficient and biocompatible new palladium-supported boehmite nanoparticles: synthesis, characterization and application in Suzuki–Miura and Mizoroki–Heck coupling reactions
title Efficient and biocompatible new palladium-supported boehmite nanoparticles: synthesis, characterization and application in Suzuki–Miura and Mizoroki–Heck coupling reactions
title_full Efficient and biocompatible new palladium-supported boehmite nanoparticles: synthesis, characterization and application in Suzuki–Miura and Mizoroki–Heck coupling reactions
title_fullStr Efficient and biocompatible new palladium-supported boehmite nanoparticles: synthesis, characterization and application in Suzuki–Miura and Mizoroki–Heck coupling reactions
title_full_unstemmed Efficient and biocompatible new palladium-supported boehmite nanoparticles: synthesis, characterization and application in Suzuki–Miura and Mizoroki–Heck coupling reactions
title_short Efficient and biocompatible new palladium-supported boehmite nanoparticles: synthesis, characterization and application in Suzuki–Miura and Mizoroki–Heck coupling reactions
title_sort efficient and biocompatible new palladium-supported boehmite nanoparticles: synthesis, characterization and application in suzuki–miura and mizoroki–heck coupling reactions
topic Chemistry
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10496902/
https://www.ncbi.nlm.nih.gov/pubmed/37705777
http://dx.doi.org/10.1039/d3na00403a
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