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Modification of kitchen blenders into controllable laboratory mixers for mechanochemical synthesis of atomically thin materials

Graphene and related two-dimensional materials (2DMs) have shown promise across numerous technology areas including flexible electronics, energy storage and pollution remediation. Research into novel applications of these atomically thin materials relies on access to synthesis techniques for produci...

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Detalles Bibliográficos
Autores principales: Pérez-Álvarez, Diego T., Brown, Jacob, Stafford, Jason
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Elsevier 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10523276/
https://www.ncbi.nlm.nih.gov/pubmed/37771323
http://dx.doi.org/10.1016/j.ohx.2023.e00471
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author Pérez-Álvarez, Diego T.
Brown, Jacob
Stafford, Jason
author_facet Pérez-Álvarez, Diego T.
Brown, Jacob
Stafford, Jason
author_sort Pérez-Álvarez, Diego T.
collection PubMed
description Graphene and related two-dimensional materials (2DMs) have shown promise across numerous technology areas including flexible electronics, energy storage and pollution remediation. Research into novel applications of these atomically thin materials relies on access to synthesis techniques for producing 2DMs with suitable quality and quantity. Liquid-phase exfoliation is a mechanochemical approach that can achieve this and produce defect-free nanomaterial dispersions which are compatible for downstream use (e.g. inkjet printing, coatings). Here, using kitchen blenders to deliver shear-driven exfoliation, we develop a range of inexpensive hardware solutions that can allow researchers to synthesise 2DMs using a controllable, sustainable and scalable process. Extensive modifications were necessary as the onboard electronics lack the experimental controls (temperature, speed, characterisation) for scientific research and precision synthesis. The technical aspects (including the many lessons learned) of the modifications are discussed and a simple selection process is proposed for creating bespoke mechanochemical processors for any application in the hope that this encourages experimentation. Specific builds with detailed notes, cost breakdown and associated files are provided in the Open Science Framework (OSF) repository, OpenLPE associated with this article.
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spelling pubmed-105232762023-09-28 Modification of kitchen blenders into controllable laboratory mixers for mechanochemical synthesis of atomically thin materials Pérez-Álvarez, Diego T. Brown, Jacob Stafford, Jason HardwareX Hardware Article Graphene and related two-dimensional materials (2DMs) have shown promise across numerous technology areas including flexible electronics, energy storage and pollution remediation. Research into novel applications of these atomically thin materials relies on access to synthesis techniques for producing 2DMs with suitable quality and quantity. Liquid-phase exfoliation is a mechanochemical approach that can achieve this and produce defect-free nanomaterial dispersions which are compatible for downstream use (e.g. inkjet printing, coatings). Here, using kitchen blenders to deliver shear-driven exfoliation, we develop a range of inexpensive hardware solutions that can allow researchers to synthesise 2DMs using a controllable, sustainable and scalable process. Extensive modifications were necessary as the onboard electronics lack the experimental controls (temperature, speed, characterisation) for scientific research and precision synthesis. The technical aspects (including the many lessons learned) of the modifications are discussed and a simple selection process is proposed for creating bespoke mechanochemical processors for any application in the hope that this encourages experimentation. Specific builds with detailed notes, cost breakdown and associated files are provided in the Open Science Framework (OSF) repository, OpenLPE associated with this article. Elsevier 2023-09-11 /pmc/articles/PMC10523276/ /pubmed/37771323 http://dx.doi.org/10.1016/j.ohx.2023.e00471 Text en © 2023 The Authors https://creativecommons.org/licenses/by/4.0/This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Hardware Article
Pérez-Álvarez, Diego T.
Brown, Jacob
Stafford, Jason
Modification of kitchen blenders into controllable laboratory mixers for mechanochemical synthesis of atomically thin materials
title Modification of kitchen blenders into controllable laboratory mixers for mechanochemical synthesis of atomically thin materials
title_full Modification of kitchen blenders into controllable laboratory mixers for mechanochemical synthesis of atomically thin materials
title_fullStr Modification of kitchen blenders into controllable laboratory mixers for mechanochemical synthesis of atomically thin materials
title_full_unstemmed Modification of kitchen blenders into controllable laboratory mixers for mechanochemical synthesis of atomically thin materials
title_short Modification of kitchen blenders into controllable laboratory mixers for mechanochemical synthesis of atomically thin materials
title_sort modification of kitchen blenders into controllable laboratory mixers for mechanochemical synthesis of atomically thin materials
topic Hardware Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10523276/
https://www.ncbi.nlm.nih.gov/pubmed/37771323
http://dx.doi.org/10.1016/j.ohx.2023.e00471
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