Remote and automated high-throughput powder diffraction measurements enabled by a robotic sample changer at SSRL beamline 2-1

The general-purpose powder diffractometer beamline (BL2-1) at the Stanford Synchrotron Radiation Lightsource (SSRL) is described. The evolution of design and performance of BL2-1 are presented, in addition to current operating specifications, applications and measurement capabilities. Recent develop...

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Detalles Bibliográficos
Autores principales: Stone, Kevin H., Cosby, Monty R., Strange, Nicholas A., Thampy, Vivek, Walroth, Richard C., Troxel Jr, Charles
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Research Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10543666/
https://www.ncbi.nlm.nih.gov/pubmed/37791352
http://dx.doi.org/10.1107/S1600576723007148
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author Stone, Kevin H.
Cosby, Monty R.
Strange, Nicholas A.
Thampy, Vivek
Walroth, Richard C.
Troxel Jr, Charles
author_facet Stone, Kevin H.
Cosby, Monty R.
Strange, Nicholas A.
Thampy, Vivek
Walroth, Richard C.
Troxel Jr, Charles
author_sort Stone, Kevin H.
collection PubMed
description The general-purpose powder diffractometer beamline (BL2-1) at the Stanford Synchrotron Radiation Lightsource (SSRL) is described. The evolution of design and performance of BL2-1 are presented, in addition to current operating specifications, applications and measurement capabilities. Recent developments involve a robotic sample changer enabling high-throughput X-ray diffraction measurements, applicable to mail-in and remote operations. In situ and operando capabilities to measure samples with different form factors (e.g. capillary, flat plate or thin film, and transmission) and under variable experimental conditions are discussed. Several example datasets and accompanying Rietveld refinements are presented.
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spelling pubmed-105436662023-10-03 Remote and automated high-throughput powder diffraction measurements enabled by a robotic sample changer at SSRL beamline 2-1 Stone, Kevin H. Cosby, Monty R. Strange, Nicholas A. Thampy, Vivek Walroth, Richard C. Troxel Jr, Charles J Appl Crystallogr Research Papers The general-purpose powder diffractometer beamline (BL2-1) at the Stanford Synchrotron Radiation Lightsource (SSRL) is described. The evolution of design and performance of BL2-1 are presented, in addition to current operating specifications, applications and measurement capabilities. Recent developments involve a robotic sample changer enabling high-throughput X-ray diffraction measurements, applicable to mail-in and remote operations. In situ and operando capabilities to measure samples with different form factors (e.g. capillary, flat plate or thin film, and transmission) and under variable experimental conditions are discussed. Several example datasets and accompanying Rietveld refinements are presented. International Union of Crystallography 2023-09-20 /pmc/articles/PMC10543666/ /pubmed/37791352 http://dx.doi.org/10.1107/S1600576723007148 Text en © Kevin H. Stone et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Stone, Kevin H.
Cosby, Monty R.
Strange, Nicholas A.
Thampy, Vivek
Walroth, Richard C.
Troxel Jr, Charles
Remote and automated high-throughput powder diffraction measurements enabled by a robotic sample changer at SSRL beamline 2-1
title Remote and automated high-throughput powder diffraction measurements enabled by a robotic sample changer at SSRL beamline 2-1
title_full Remote and automated high-throughput powder diffraction measurements enabled by a robotic sample changer at SSRL beamline 2-1
title_fullStr Remote and automated high-throughput powder diffraction measurements enabled by a robotic sample changer at SSRL beamline 2-1
title_full_unstemmed Remote and automated high-throughput powder diffraction measurements enabled by a robotic sample changer at SSRL beamline 2-1
title_short Remote and automated high-throughput powder diffraction measurements enabled by a robotic sample changer at SSRL beamline 2-1
title_sort remote and automated high-throughput powder diffraction measurements enabled by a robotic sample changer at ssrl beamline 2-1
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10543666/
https://www.ncbi.nlm.nih.gov/pubmed/37791352
http://dx.doi.org/10.1107/S1600576723007148
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