Indium Kα radiation from a MetalJet X-ray source: the long way to a successful charge-density investigation

The MetalJet X-ray source provides indium Kα radiation with a wavelength even shorter than Ag radiation. This paper reports on problematic spectral impurities and presents possible countermeasures so that collection of data with excellent quality up to a high resolution is possible. It is demonstrat...

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Detalles Bibliográficos
Autores principales: Graw, Nico, Ruth, Paul Niklas, Ernemann, Tobias, Herbst-Irmer, Regine, Stalke, Dietmar
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Research Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10543667/
https://www.ncbi.nlm.nih.gov/pubmed/37791365
http://dx.doi.org/10.1107/S1600576723007203
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author Graw, Nico
Ruth, Paul Niklas
Ernemann, Tobias
Herbst-Irmer, Regine
Stalke, Dietmar
author_facet Graw, Nico
Ruth, Paul Niklas
Ernemann, Tobias
Herbst-Irmer, Regine
Stalke, Dietmar
author_sort Graw, Nico
collection PubMed
description The MetalJet X-ray source provides indium Kα radiation with a wavelength even shorter than Ag radiation. This paper reports on problematic spectral impurities and presents possible countermeasures so that collection of data with excellent quality up to a high resolution is possible. It is demonstrated that these data can be used in the refinement of a multipole model, the results of which are used for a topological analysis to assess the bonding situation in a sulfur ylide compound.
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spelling pubmed-105436672023-10-03 Indium Kα radiation from a MetalJet X-ray source: the long way to a successful charge-density investigation Graw, Nico Ruth, Paul Niklas Ernemann, Tobias Herbst-Irmer, Regine Stalke, Dietmar J Appl Crystallogr Research Papers The MetalJet X-ray source provides indium Kα radiation with a wavelength even shorter than Ag radiation. This paper reports on problematic spectral impurities and presents possible countermeasures so that collection of data with excellent quality up to a high resolution is possible. It is demonstrated that these data can be used in the refinement of a multipole model, the results of which are used for a topological analysis to assess the bonding situation in a sulfur ylide compound. International Union of Crystallography 2023-09-05 /pmc/articles/PMC10543667/ /pubmed/37791365 http://dx.doi.org/10.1107/S1600576723007203 Text en © Nico Graw et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Graw, Nico
Ruth, Paul Niklas
Ernemann, Tobias
Herbst-Irmer, Regine
Stalke, Dietmar
Indium Kα radiation from a MetalJet X-ray source: the long way to a successful charge-density investigation
title Indium Kα radiation from a MetalJet X-ray source: the long way to a successful charge-density investigation
title_full Indium Kα radiation from a MetalJet X-ray source: the long way to a successful charge-density investigation
title_fullStr Indium Kα radiation from a MetalJet X-ray source: the long way to a successful charge-density investigation
title_full_unstemmed Indium Kα radiation from a MetalJet X-ray source: the long way to a successful charge-density investigation
title_short Indium Kα radiation from a MetalJet X-ray source: the long way to a successful charge-density investigation
title_sort indium kα radiation from a metaljet x-ray source: the long way to a successful charge-density investigation
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10543667/
https://www.ncbi.nlm.nih.gov/pubmed/37791365
http://dx.doi.org/10.1107/S1600576723007203
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