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Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method

Small-angle neutron scattering (SANS) is widely used as a powerful technique to study the higher-order structure of soft matter. To increase the reliability of SANS profile analysis for complex multi-component systems, combining different types of structural information obtained by other methods is...

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Detalles Bibliográficos
Autores principales: Kaneko, Fumitoshi, Radulescu, Aurel, Nakagawa, Hiroshi
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2023
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10543673/
https://www.ncbi.nlm.nih.gov/pubmed/37791361
http://dx.doi.org/10.1107/S1600576723007744
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author Kaneko, Fumitoshi
Radulescu, Aurel
Nakagawa, Hiroshi
author_facet Kaneko, Fumitoshi
Radulescu, Aurel
Nakagawa, Hiroshi
author_sort Kaneko, Fumitoshi
collection PubMed
description Small-angle neutron scattering (SANS) is widely used as a powerful technique to study the higher-order structure of soft matter. To increase the reliability of SANS profile analysis for complex multi-component systems, combining different types of structural information obtained by other methods is desirable. A simultaneous measurement system combining SANS and Fourier transform infrared (FTIR) spectroscopy meets this objective. It is beneficial for targets where matching the timing of structural changes between experiments is difficult, but the issue is that samples suitable for SANS are too thick for the typical transmission FTIR method. To overcome this problem, a new simultaneous measurement system that employs the attenuated total reflectance (ART) sampling method for FTIR spectroscopy has been developed.
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spelling pubmed-105436732023-10-03 Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method Kaneko, Fumitoshi Radulescu, Aurel Nakagawa, Hiroshi J Appl Crystallogr Research Papers Small-angle neutron scattering (SANS) is widely used as a powerful technique to study the higher-order structure of soft matter. To increase the reliability of SANS profile analysis for complex multi-component systems, combining different types of structural information obtained by other methods is desirable. A simultaneous measurement system combining SANS and Fourier transform infrared (FTIR) spectroscopy meets this objective. It is beneficial for targets where matching the timing of structural changes between experiments is difficult, but the issue is that samples suitable for SANS are too thick for the typical transmission FTIR method. To overcome this problem, a new simultaneous measurement system that employs the attenuated total reflectance (ART) sampling method for FTIR spectroscopy has been developed. International Union of Crystallography 2023-09-27 /pmc/articles/PMC10543673/ /pubmed/37791361 http://dx.doi.org/10.1107/S1600576723007744 Text en © Fumitoshi Kaneko et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Research Papers
Kaneko, Fumitoshi
Radulescu, Aurel
Nakagawa, Hiroshi
Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method
title Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method
title_full Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method
title_fullStr Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method
title_full_unstemmed Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method
title_short Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method
title_sort simultaneous sans/ftir measurement system incorporating the atr sampling method
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10543673/
https://www.ncbi.nlm.nih.gov/pubmed/37791361
http://dx.doi.org/10.1107/S1600576723007744
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