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Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method
Small-angle neutron scattering (SANS) is widely used as a powerful technique to study the higher-order structure of soft matter. To increase the reliability of SANS profile analysis for complex multi-component systems, combining different types of structural information obtained by other methods is...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2023
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10543673/ https://www.ncbi.nlm.nih.gov/pubmed/37791361 http://dx.doi.org/10.1107/S1600576723007744 |
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author | Kaneko, Fumitoshi Radulescu, Aurel Nakagawa, Hiroshi |
author_facet | Kaneko, Fumitoshi Radulescu, Aurel Nakagawa, Hiroshi |
author_sort | Kaneko, Fumitoshi |
collection | PubMed |
description | Small-angle neutron scattering (SANS) is widely used as a powerful technique to study the higher-order structure of soft matter. To increase the reliability of SANS profile analysis for complex multi-component systems, combining different types of structural information obtained by other methods is desirable. A simultaneous measurement system combining SANS and Fourier transform infrared (FTIR) spectroscopy meets this objective. It is beneficial for targets where matching the timing of structural changes between experiments is difficult, but the issue is that samples suitable for SANS are too thick for the typical transmission FTIR method. To overcome this problem, a new simultaneous measurement system that employs the attenuated total reflectance (ART) sampling method for FTIR spectroscopy has been developed. |
format | Online Article Text |
id | pubmed-10543673 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2023 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-105436732023-10-03 Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method Kaneko, Fumitoshi Radulescu, Aurel Nakagawa, Hiroshi J Appl Crystallogr Research Papers Small-angle neutron scattering (SANS) is widely used as a powerful technique to study the higher-order structure of soft matter. To increase the reliability of SANS profile analysis for complex multi-component systems, combining different types of structural information obtained by other methods is desirable. A simultaneous measurement system combining SANS and Fourier transform infrared (FTIR) spectroscopy meets this objective. It is beneficial for targets where matching the timing of structural changes between experiments is difficult, but the issue is that samples suitable for SANS are too thick for the typical transmission FTIR method. To overcome this problem, a new simultaneous measurement system that employs the attenuated total reflectance (ART) sampling method for FTIR spectroscopy has been developed. International Union of Crystallography 2023-09-27 /pmc/articles/PMC10543673/ /pubmed/37791361 http://dx.doi.org/10.1107/S1600576723007744 Text en © Fumitoshi Kaneko et al. 2023 https://creativecommons.org/licenses/by/4.0/This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Research Papers Kaneko, Fumitoshi Radulescu, Aurel Nakagawa, Hiroshi Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method |
title | Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method |
title_full | Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method |
title_fullStr | Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method |
title_full_unstemmed | Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method |
title_short | Simultaneous SANS/FTIR measurement system incorporating the ATR sampling method |
title_sort | simultaneous sans/ftir measurement system incorporating the atr sampling method |
topic | Research Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10543673/ https://www.ncbi.nlm.nih.gov/pubmed/37791361 http://dx.doi.org/10.1107/S1600576723007744 |
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